JP6354539B2 - 基板処理装置、基板処理方法、記憶媒体 - Google Patents
基板処理装置、基板処理方法、記憶媒体 Download PDFInfo
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- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
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- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
- C23C16/45523—Pulsed gas flow or change of composition over time
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- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02107—Forming insulating materials on a substrate
- H01L21/02109—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates
- H01L21/02205—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates the layer being characterised by the precursor material for deposition
- H01L21/02208—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates the layer being characterised by the precursor material for deposition the precursor containing a compound comprising Si
- H01L21/02211—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates the layer being characterised by the precursor material for deposition the precursor containing a compound comprising Si the compound being a silane, e.g. disilane, methylsilane or chlorosilane
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- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02107—Forming insulating materials on a substrate
- H01L21/02109—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates
- H01L21/02205—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates the layer being characterised by the precursor material for deposition
- H01L21/02208—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates the layer being characterised by the precursor material for deposition the precursor containing a compound comprising Si
- H01L21/02219—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates the layer being characterised by the precursor material for deposition the precursor containing a compound comprising Si the compound comprising silicon and nitrogen
Description
前記真空容器内に連鎖分解反応を起こす濃度以上の濃度のオゾンと、水素供与体と、からなる処理雰囲気を形成するための雰囲気ガスを供給する雰囲気ガス供給部と、
前記処理雰囲気にエネルギーを供給し、前記オゾンを強制的に分解させて生じた活性種と、前記水素供与体とが反応して生成したヒドロキシルラジカルにより基板の表面を酸化するためのエネルギー供給部と、
不活性ガスが供給されると共に、前記オゾンの分解による真空容器内の圧力上昇を緩和するために、少なくとも前記エネルギーの供給時に真空容器内に連通するバッファ領域と、
を備えることを特徴とする。
本発明の第1の実施形態に係る成膜装置1について、図1の縦断側面図及び図2の横断平面図を参照しながら説明する。この成膜装置1はALDにより、基板であるウエハWに酸化シリコン膜を形成する。図中11は水平な円形のステージであり、その表面にウエハWを水平に載置する。ステージ11の下方には垂直な支柱12が設けられ、支柱12の下端は昇降機構13に接続されており、当該昇降機構13を介してステージ11は鉛直方向に昇降することができる。図1では成膜処理を行うための上昇位置に位置したステージ11を実線で、図示しない搬送機構との間でウエハWを受け渡すための下降位置に位置したステージ11を鎖線で、夫々示している。
H2+2O・→2OH・(式1)
続いて第2の実施形態に係る成膜装置7について、図17を参照しながら成膜装置1との差異点を中心に説明する。この成膜装置7においてはガス供給路41A〜43A及び排気路17が、フード21に設けられる代わりにステージ11に設けられており、ステージ11の表面において、ウエハWの載置領域の外側に開口している。従って、この成膜装置7では、ガス供給管41〜43及び排気管18は、フード21に接続される代わりにステージ11に接続されている。
H2O+O・→2OH・(式2)
H2O2+O・→2OH・+O・(式3)
本発明に関連して行われた評価試験について説明する。評価試験1として、実施の形態で説明したように、処理空間22に連鎖分解反応が起きる限界濃度以上の濃度になるように一定の量のオゾンガスを封入すると共に、H2ガスを封入した。然る後、処理空間22にNOガスを供給して連鎖分解反応を起こして、OHラジカルを発生させる処理を行った。H2ガスの供給流量はこの処理を行う度に変更した。
1 成膜装置
10 制御部
22 処理空間
23 処理容器
25 外側容器
26 バッファ領域
51 アミノシランガス供給源
54 O3ガス供給源
53 NOガス供給源
Claims (17)
- 真空容器内に形成された真空雰囲気で基板の表面を酸化する基板処理装置において、
前記真空容器内に連鎖分解反応を起こす濃度以上の濃度のオゾンと、水素供与体と、からなる処理雰囲気を形成するための雰囲気ガスを供給する雰囲気ガス供給部と、
前記処理雰囲気にエネルギーを供給し、前記オゾンを強制的に分解させて生じた活性種と、前記水素供与体とが反応して生成したヒドロキシルラジカルにより基板の表面を酸化するためのエネルギー供給部と、
不活性ガスが供給されると共に、前記オゾンの分解による真空容器内の圧力上昇を緩和するために、少なくとも前記エネルギーの供給時に真空容器内に連通するバッファ領域と、
を備えることを特徴とする基板処理装置。 - 前記バッファ領域は真空容器の外側を囲む外側容器の内部空間により構成され、
前記真空容器にはバッファ領域と真空容器内とを連通させるガス流路が設けられることを特徴とする請求項1記載の基板処理装置。 - 前記真空容器は、基板を載置するステージと、ステージを覆うフードと、を備え、前記ガス流路は前記ステージと前記フードとの間に形成される隙間であることを特徴とする請求項2記載の基板処理装置。
- 前記雰囲気ガスが前記真空容器内に供給されるときには前記隙間を閉塞して前記真空容器内と前記バッファ領域とを区画し、前記エネルギーが供給されるときには前記隙間を開放して前記真空容器内と前記バッファ領域とを連通させる区画機構が設けられることを特徴とする請求項3記載の基板処理装置。
- 前記雰囲気ガス供給部は、
液体状態の前記水素供与体が貯留されたタンクと、
前記タンク内の液面下にオゾンガスを供給してバブリングを行い、水素供与体を気化させるオゾンガス供給部と、
前記オゾンガスをキャリアガスとして気化した水素供与体を真空容器内に供給するためのガス供給路と、
を備えたことを特徴とする請求項1ないし4のいずれか一つに記載の基板処理装置。 - 前記水素供与体は、水素、水または過酸化水素であることを特徴とする請求項1ないし5のいずれか一つに記載の基板処理装置。
- 前記エネルギー供給部は、オゾンと化学反応して前記強制的な分解を起こすための反応ガスを前記処理雰囲気に供給する反応ガス供給部により構成されることを特徴とする請求項1ないし6のいずれか一つに記載の基板処理装置。
- 前記反応ガスは一酸化窒素であることを特徴とする請求項7記載の基板処理装置。
- 前記真空容器は、前記反応ガスを前記真空雰囲気に供給するための供給口を備え、
前記供給口は、真空容器内に載置される基板の中心部に向かって開口することを特徴とする請求項7または8記載の基板処理装置。 - 前記真空容器内の基板に原料を吸着させるために、当該基板に前記原料を含む原料ガスを供給する原料ガス供給部と、
この原料ガスの供給と、次いで行われる前記処理雰囲気の形成と、続いて行われるエネルギー供給とからなるサイクルが複数回繰り返し行われ、基板の表面に酸化物の分子層が積層されるように制御信号を出力する制御部と、
を含む成膜装置として構成されることを特徴とする請求項1ないし9のいずれか一つに記載の基板処理装置。 - 真空容器内に形成された真空雰囲気で基板の表面を酸化する基板処理方法において、
前記真空容器内に連鎖分解反応を起こす濃度以上の濃度のオゾンと、水素供与体と、からなる処理雰囲気を形成するための雰囲気ガスを供給する工程と、
前記処理雰囲気にエネルギーを供給し、前記オゾンを強制的に分解させて生じた活性種と、前記水素供与体とが反応して生成したヒドロキシルラジカルにより基板の表面を酸化するためのエネルギー供給工程と、
前記オゾンの分解による真空容器内の圧力上昇を緩和するために、不活性ガスが供給されるバッファ領域を、少なくとも前記エネルギーの供給時に真空容器内に連通させる工程と、
を備えることを特徴とする基板処理方法。 - 前記雰囲気ガスを供給する工程は、
液体状態の前記水素供与体が貯留されたタンク内の液面下にオゾンガスを供給してバブリングを行い、当該水素供与体を気化させる工程と、
前記オゾンガスをキャリアガスとして、気化した前記水素供与体をガス供給路を介して前記真空容器内に供給する工程と、
を備えたことを特徴とする請求項11記載の基板処理方法。 - 前記エネルギー供給工程は、オゾンと化学反応して前記強制的な分解を起こすための反応ガスを前記処理雰囲気に供給する工程を含むことを特徴とする請求項11または12記載の基板処理方法。
- 前記反応ガスは一酸化窒素であることを特徴とする請求項13記載の基板処理方法。
- 前記反応ガスを処理雰囲気に供給する工程は、
前記真空容器内に載置される基板の中心部に向かって開口するように当該真空容器に設けられた供給口から、前記反応ガスを前記処理雰囲気に供給する工程であることを特徴とする請求項13または14記載の基板処理方法。 - 前記真空容器内の基板に原料を吸着させるために、当該基板に前記原料を含む原料ガスを供給する原料ガス供給工程と、
この原料ガス供給工程と、次いで行われる前記雰囲気ガスの供給工程と、続いて行われるエネルギー供給工程とからなるサイクルを複数回繰り返し行い、基板の表面に酸化物の分子層を積層して薄膜を形成する工程と、
を含むことを特徴とする請求項11ないし15のいずれか一つに記載の基板処理方法。 - 真空容器内に形成された真空雰囲気で、基板の表面を酸化する基板処理装置において用いられるコンピュータプログラムを格納した記憶媒体において、
前記コンピュータプログラムは、請求項11ないし16のいずれか一つに記載の基板処理方法を実施するようにステップが組まれていることを特徴とする記憶媒体。
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