JP4827354B2 - ポリ(アリーレンスルフィド)の製法 - Google Patents

ポリ(アリーレンスルフィド)の製法 Download PDF

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Publication number
JP4827354B2
JP4827354B2 JP2001523673A JP2001523673A JP4827354B2 JP 4827354 B2 JP4827354 B2 JP 4827354B2 JP 2001523673 A JP2001523673 A JP 2001523673A JP 2001523673 A JP2001523673 A JP 2001523673A JP 4827354 B2 JP4827354 B2 JP 4827354B2
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JP
Japan
Prior art keywords
molecular weight
arylene sulfide
methanol
mixture
alkali metal
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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JP2001523673A
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English (en)
Japanese (ja)
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JP2003509556A (ja
Inventor
ヴィドーリ、フェルナンド、シー、ジュニア
ゲイベル、ジョン、エフ
ウォーターマン、ジェイムズ、ダブリュ
チャフィン、ジェイ、エム
サウス、オーブリー、ジュニア
フォードア、ジェフリー、エス
カイル、グレン、エフ
Original Assignee
コノコフィリップス カンパニー
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Publication of JP2003509556A publication Critical patent/JP2003509556A/ja
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/14Polysulfides
    • C08G75/16Polysulfides by polycondensation of organic compounds with inorganic polysulfides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D207/00Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
    • C07D207/02Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D207/18Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D207/22Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D207/24Oxygen or sulfur atoms
    • C07D207/262-Pyrrolidones
    • C07D207/2632-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms
    • C07D207/2672-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to the ring nitrogen atom
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02Polythioethers
    • C08G75/0204Polyarylenethioethers
    • C08G75/0277Post-polymerisation treatment
    • C08G75/0281Recovery or purification

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
JP2001523673A 1999-09-13 2000-09-11 ポリ(アリーレンスルフィド)の製法 Expired - Fee Related JP4827354B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US09/394,790 US6331608B1 (en) 1999-09-13 1999-09-13 Process for producing poly(arylene sulfide)
US09/394,790 1999-09-13
PCT/US2000/040865 WO2001019898A1 (en) 1999-09-13 2000-09-11 A process for producing poly(arylene sulfide)

Publications (2)

Publication Number Publication Date
JP2003509556A JP2003509556A (ja) 2003-03-11
JP4827354B2 true JP4827354B2 (ja) 2011-11-30

Family

ID=23560436

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2001523673A Expired - Fee Related JP4827354B2 (ja) 1999-09-13 2000-09-11 ポリ(アリーレンスルフィド)の製法

Country Status (11)

Country Link
US (1) US6331608B1 (pt)
EP (1) EP1228123B1 (pt)
JP (1) JP4827354B2 (pt)
KR (1) KR100737542B1 (pt)
CN (1) CN1261488C (pt)
AT (1) ATE299159T1 (pt)
AU (1) AU1251401A (pt)
BR (1) BR0013956A (pt)
DE (1) DE60021198T2 (pt)
ES (1) ES2243318T3 (pt)
WO (1) WO2001019898A1 (pt)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6437024B1 (en) * 1999-09-13 2002-08-20 Phillips Petroleum Company Menthanol extraction of polar organic compounds and modifier compounds from poly(arylene sulfide) polymer and oligomer streams
US6307011B1 (en) * 1999-09-13 2001-10-23 Phillips Petroleum Company Recovery of modifier compounds and polar organic compounds from a poly(arylene sulfide) recycle mixture
ATE433472T1 (de) * 2001-12-03 2009-06-15 Kureha Corp Verfahren zur kontinuierlichen reinigung von polyarylensulfid
JP2003252610A (ja) * 2001-12-27 2003-09-10 Idemitsu Petrochem Co Ltd 硫化リチウムの再生方法及びポリアリーレンスルフィドの製造方法
US8263734B2 (en) * 2009-02-13 2012-09-11 Chevron Phillips Chemical Company Lp System and method for reducing off-gassing of polyphenylene sulfide
JP2016536377A (ja) 2013-09-25 2016-11-24 ティコナ・エルエルシー ポリアリーレンスルフィドを形成するためのスクラビングプロセス
JP6797687B2 (ja) 2013-09-25 2020-12-09 ティコナ・エルエルシー ポリアリーレンスルフィド結晶化方法
WO2015047717A1 (en) 2013-09-25 2015-04-02 Ticona Llc Method and system for separation of a polymer from multiple compounds
JP6684206B2 (ja) 2013-09-25 2020-04-22 ティコナ・エルエルシー ポリアリーレンスルフィドの形成中における塩副生成物の分離
JP2016536376A (ja) 2013-09-25 2016-11-24 ティコナ・エルエルシー 低ハロゲン含量のポリアリーレンスルフィドを形成する方法
JP6797686B2 (ja) 2013-09-25 2020-12-09 ティコナ・エルエルシー ポリアリーレンスルフィドを形成するための多段階プロセス
JP6803844B2 (ja) 2015-02-19 2020-12-23 ティコナ・エルエルシー 低粘度のポリアリーレンスルフィドを形成する方法
WO2016133739A1 (en) 2015-02-19 2016-08-25 Ticona Llc Method for forming a high molecular weight polyarylene sulfide
WO2016133740A1 (en) 2015-02-19 2016-08-25 Ticona Llc Method of polyarylene sulfide precipitation
JP6783242B2 (ja) 2015-03-25 2020-11-11 ティコナ・エルエルシー 高溶融粘度のポリアリーレンスルフィドを形成する方法
CN108948355B (zh) * 2018-07-26 2020-12-08 四川中科兴业高新材料有限公司 一种以苯和硫磺为原料制备聚苯硫醚的方法
US11407861B2 (en) 2019-06-28 2022-08-09 Ticona Llc Method for forming a polyarylene sulfide
CN115279734A (zh) 2019-12-20 2022-11-01 提克纳有限责任公司 形成聚芳硫醚的方法
US12018129B2 (en) 2021-09-08 2024-06-25 Ticona Llc Extraction technique for recovering an organic solvent from a polyarylene sulfide waste sludge

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61255933A (ja) * 1985-05-08 1986-11-13 Kureha Chem Ind Co Ltd 重合体スラリ−の処理法
JPS62177028A (ja) * 1986-01-31 1987-08-03 Dainippon Ink & Chem Inc ポリアリ−レンスルフイド製造時の重合助剤の回収方法
JPS63132941A (ja) * 1986-11-25 1988-06-04 Tosoh Corp ポリアリ−レンサルフアイドの回収方法
JPS6431832A (en) * 1987-07-11 1989-02-02 Bayer Ag Isolation of polyarylene sulfide
JPH04275334A (ja) * 1990-11-29 1992-09-30 Phillips Petroleum Co フェニレンスルフィドポリマーの製造法
JPH07118389A (ja) * 1993-10-19 1995-05-09 Kureha Chem Ind Co Ltd 低腐食性ポリアリーレンスルフィドの製造方法
JPH09328551A (ja) * 1996-03-11 1997-12-22 Idemitsu Petrochem Co Ltd ポリアリーレンスルフィドの連続式製造方法
JPH1180355A (ja) * 1997-09-12 1999-03-26 Dainippon Ink & Chem Inc ポリアリーレンスルフィドの精製方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3800845A (en) 1971-12-14 1974-04-02 Phillips Petroleum Co Solvent removal from poly(arylene sulfide) reaction slurry
US4415729A (en) 1982-06-04 1983-11-15 Phillips Petroleum Company Recovering granular poly(arylene sulfide) particles from a poly(arylene sulfide) reaction mixture
DE3243189A1 (de) 1982-11-23 1984-05-24 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von hochmolekularen gegebenenfalls verzweigten polyarylensulfiden
JPS62232437A (ja) 1986-04-02 1987-10-12 Toto Kasei Kk ポリフエニレンスルフイド樹脂の製造方法
ATE104999T1 (de) * 1987-10-05 1994-05-15 Phillips Petroleum Co Verfahren zur gewinnung von polyarylensulfiden mit vaporisierten fluessigkeiten.
US5231163A (en) 1988-08-05 1993-07-27 Idemitsu Petrochemical Company, Ltd. Polyarylene sulfide from aromatic compound having at least three functional groups
US5278283A (en) 1989-06-30 1994-01-11 Idemitsu Petrochemical Company, Limited Process for preparing polyarylene sulfides of increased molecular weight
JPH0672186B2 (ja) 1989-12-25 1994-09-14 出光石油化学株式会社 粒状の高分子量ポリアリーレンスルフィドの製造方法
US5128445A (en) 1990-06-14 1992-07-07 Phillips Petroleum Company Method to recover poly(arylene sulfide) polymers with water-polar organic compound
US5334701A (en) * 1992-10-23 1994-08-02 Phillips Petroleum Company Process for the removal of lower molecular weight fractions of poly(arylene sulfide) polymers

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61255933A (ja) * 1985-05-08 1986-11-13 Kureha Chem Ind Co Ltd 重合体スラリ−の処理法
JPS62177028A (ja) * 1986-01-31 1987-08-03 Dainippon Ink & Chem Inc ポリアリ−レンスルフイド製造時の重合助剤の回収方法
JPS63132941A (ja) * 1986-11-25 1988-06-04 Tosoh Corp ポリアリ−レンサルフアイドの回収方法
JPS6431832A (en) * 1987-07-11 1989-02-02 Bayer Ag Isolation of polyarylene sulfide
JPH04275334A (ja) * 1990-11-29 1992-09-30 Phillips Petroleum Co フェニレンスルフィドポリマーの製造法
JPH07118389A (ja) * 1993-10-19 1995-05-09 Kureha Chem Ind Co Ltd 低腐食性ポリアリーレンスルフィドの製造方法
JPH09328551A (ja) * 1996-03-11 1997-12-22 Idemitsu Petrochem Co Ltd ポリアリーレンスルフィドの連続式製造方法
JPH1180355A (ja) * 1997-09-12 1999-03-26 Dainippon Ink & Chem Inc ポリアリーレンスルフィドの精製方法

Also Published As

Publication number Publication date
BR0013956A (pt) 2002-07-23
US6331608B1 (en) 2001-12-18
AU1251401A (en) 2001-04-17
ATE299159T1 (de) 2005-07-15
EP1228123B1 (en) 2005-07-06
EP1228123A4 (en) 2003-01-02
ES2243318T3 (es) 2005-12-01
KR20020030817A (ko) 2002-04-25
KR100737542B1 (ko) 2007-07-10
DE60021198D1 (de) 2005-08-11
JP2003509556A (ja) 2003-03-11
CN1261488C (zh) 2006-06-28
DE60021198T2 (de) 2006-05-11
WO2001019898A1 (en) 2001-03-22
CN1377381A (zh) 2002-10-30
EP1228123A1 (en) 2002-08-07

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