JP2010513609A - レーザーマーキングまたはレーザー溶着化剤としての球体金属粒子の使用、ならびにレーザーマーク可能および/またはレーザー溶着可能なプラスチック - Google Patents
レーザーマーキングまたはレーザー溶着化剤としての球体金属粒子の使用、ならびにレーザーマーク可能および/またはレーザー溶着可能なプラスチック Download PDFInfo
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Classifications
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Abstract
本発明は、さらに、レーザーマーキング剤が、アンチモンおよび/またはアンチモン含有化合物を含まない、球体金属粒子からなる、レーザーマーク可能および/またはレーザー溶着可能なプラスチックにも関するが、ここで、その球体金属粒子の粒子サイズ分布は、レーザー粒度測定法によって求めて、体積平均累積篩下粒子サイズ分布の形で、D99値が<110μm、D90値が<75μm、そしてD50が<45μmである。
Description
−たとえばブタジエンまたはイソプレンのようなジエンを基とするジエンゴム(ABS);
−アクリル酸のアルキルエステル、たとえば、アクリル酸n−ブチルおよびアクリル酸2−エチルヘキシルを基とするアクリル酸アルキルゴム(ASA);
−エチレン、プロピレンおよびジエンを基とするEPDMゴム(AES);
または、これらのゴムおよび/またはゴムモノマーの混合物。
例:Hostanox(Clariant、Frankfurt)、Irganox(Ciba Geigy、Basel)、Naugard(Uniroyal、GB)。
例:Chimasorb、Tinuvin(いずれもCiba−Geigy、Basel)、Cyasorb(American Cyanamid)、Hostavin(Clariant、Frankfurt)、Uvinul(BASF、Ludwigshafen)。
例:Carbowax(DOW、Belgium)、Cetamoll(BASF、Ludwigshafen)、Edenol(Henkel、Dusseldorf)、Elvaloy(DuPont de Nemours、USA)、Lankroflex(Lankro、GB)、Palamoll、Palatinol(いずれもBASF、Ludwigshafen)。
例:Licowax、Ceridust、Licolub、Licomont(すべてClariant、Frankfurt)、Irgawax(Ciba−Geigy、Basel)、Loxiol(Henkel、Dusseldorf)、Baerolub(Baerlocher、Munich)。
例:Fire Fighters(Great Lakes Chemicals)、Fyrol(Dead Sea Bromine、Israel)、Martinal(Martinswerk、Bergheim)、Reofos(Ciba−Geigy、Basel)、Phosflex(Akzo Chemicals、USA)。
例:Baerostat(Baerlocher、Munich)、Dehydat(Henkel、Dusseldorf)、Hostastat(Clariant、Frankfurt)、Irgastat(Ciba−Geigy、Basel)。
例:Hostalux(Clariant、Frankfurt)、Uvitex(Ciba−Geigy、Basel)。
例:Cunilate(Ventron、B)、Preventol(Bayer、Leverkusen)、Fungitrol(Tenneco、USA)。
例:Hydrocerol 8(Boehringer、Ingelheim)、Porofor(Bayer、Leverkusen)、Genitron(Schering、GB)。
例:Interox(Peroxidchemie、Hoellriegelskreuth)、Luperco、Luperox(Luperox、Guenzburg)。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(Sympatec、Germanyから供給されるHelos装置を使用したレーザー粒度測定法により決定)である、球体アルミニウム粒子の粉体(ECKART GmbH & Co.KG、Fuerth、Germany)を、熱可塑性ポリプロピレン(PP)(R771−10;DOW、Germany、Wesseling)との混合物の形で、射出成形により加工して、板(面積42×60mm、厚み2mm)を形成させた。
D50値が2.50μm、D90値が5.46μm、D99値が11.6μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子(ECKART)を、実施例1にならって、PPと共に加工した。
D50値が2.27μm、D90値が3.83μm、D99値が5.28μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子(ECKART)を、実施例1にならって、PPと共に加工した。
D50値が17.5μm、D90値が34.5μm、D99値が62.0μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子(ECKART)を、実施例1にならって、PPと共に加工した。
D50値が39.3μm、D90値が69.1μm、D99値が104μm(実施例1の同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子(ECKART)を、実施例1にならって、PPと共に加工した。
D50値が140μm、D90値が230μm(D99値:決定不能)(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子(ECKART)を、実施例1にならって、PPと共に加工した。
D10値が1.51μm、D50値が4.02μm、D90値が10.0μm(実施例1と同様にしてHelos装置を用いて決定)である、微細な、微小板形状のアルミニウム効果顔料(PC200、Eckart GmbH & Co.KG、Fuerth、Germany)を、実施例1にならって、PPと共に加工した。
アンチモンをドープさせた酸化スズ粒子(Mark−it(商標)顔料、Engelhard Corporation、USA)を、実施例1に従って、PPと共に加工した。
アンチモンをドープさせた酸化スズのコーティングを含むマイカフレーク(Lazerflair(登録商標)825、E.Merck KGaA、Germany)を、実施例1に従って、PPと共に加工した。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子の粉体(ECKART)を、熱可塑性ポリスチレン(PS)(Styron 678−E、DOW、USA)との混合物の形で、実施例1にならって射出成形により加工して、板(面積42×60mm、厚み2mm)を形成させた。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子の粉体(ECKART)を、熱可塑性ポリカーボネート(PC)(Calibre 201 TNT、DOW、USA)との混合物の形で、実施例1にならって射出成形により加工して、板(面積42×60mm、厚み2mm)を形成させた。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子の粉体(ECKART)を、熱可塑性ポリエチレンテレフタレート(PET)(Suka 5141、Du Pont、USA)との混合物の形で、実施例1にならって射出成形により加工して、板(面積42×60mm、厚み2mm)を形成させた。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子の粉体(ECKART)を、熱可塑性スチレン−アクリロニトリル(SAN)(Tyril 867、DOW、USA)との混合物の形で、実施例1にならって射出成形により加工して、板(面積42×60mm、厚み2mm)を形成させた。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子の粉体(ECKART)を、熱可塑性アクリル−ブタジエン−スチレン・コポリマー(ABS)(Magnum 8433、DOW、USA)との混合物の形で、実施例1と同様にして射出成形により加工して、板(面積42×60mm、厚み2mm)を形成させた。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子の粉体(ECKART)を、低密度ポリエチレン(LDPE)(LDPE 410−E、DOW、USA)との混合物の形で、サイエンティフィックフィルム押し出し機(LabTech、Thiland)を使用して加工して、100μmの厚みを有するインフレートフィルムを得た。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子の粉体(ECKART)を、熱可塑性ポリアミドPA6(Gerstamid R 200 S、Resin Express、Germany)との混合物の形で、実施例1と同様にして射出成形により加工して、板(面積42×60mm、厚み2mm)を形成させた。
実施例1と同様にして、銀色の真珠光沢顔料(PX1001、ECKART)を、ポリプロピレン(PP)中、濃度0.49重量%で加工した。この場合、満足ないしは十分なエッジ解像力およびドット精度を示す、高コントラストで、黒く耐摩耗性のマークを得ることが可能であった。しかしながら、この場合においては、そのPP板が真珠光的な光沢を有していて、また不透明であった。PP板の中に流れ筋が形成されたことが、極めて明瞭に観察できた。
実施例1と同様にして、銀色の真珠光沢顔料(PX1001、ECKART)を、ポリプロピレン(PP)中、濃度0.49重量%で、さらに、D10=1.9μm、D50=3.4μm、D90=6μmの粒子サイズ分布を有する亜鉛粉体(亜鉛末17640、製造業者:Norzinko GmbH、Gosslar、Germany)を0.0098重量%で、PPと共に加工した。
実施例1と同様にして、亜鉛粉体(亜鉛末17640、Norzinko GmbH、Gosslar、Germany)を、ポリプロピレン(PP)と共に加工した。
実施例1と同様にして、銀色の真珠光沢顔料(PX1001、ECKART)を濃度0.05重量%で、さらに、亜鉛粉体(亜鉛末17640、Norzinko GmbH、Gosslar、Germany)を0.25重量%および0.05重量%の濃度で、PPと共に加工した。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて決定)である、球体アルミニウム粒子の粉体を、0.05重量%で、熱可塑性ポリプロピレン(R 771−10;DOW、USA)との混合物の形で、射出成形プロセスにおいて加工して、板とした(実施例1と同様、面積42×60mm、厚み1mm)。
実施例20と同様にして、その手順を、熱可塑性ポリプロピレン(R 771−10;DOW、USA)製の2枚の顔料無添加の板を用いて実施した。この結果としては、プラスチック板の溶融を誘導することはできなかった。
D50値が1.57μm、D90値が3.37μm、D99値が7.55μm(実施例1と同様にしてHelos装置を用いて測定)である、球体アルミニウム粒子の粉体を、0.5重量%で、低密度ポリエチレン(LDPE)(LDPE 410−E、DOW、USA)との混合物の形で、フィルム押し出し機(タイプ:Scientific、LabTech、Thiland)により加工して、100μmの厚みを有するインフレートフィルムとした。フィルムの一部(110×70mm)を、相当する顔料無添加のLDPEフィルムを用いて覆い、実施例20と同様にして処理した。この結果として、照射した領域において、フィルムとフィルムの接触範囲でそれらの溶融を誘導することが可能であった。その溶着は、力を加えたときにだけ、再分離させることが可能であり、その溶着の部分ではフィルムの破損を伴った。
低密度ポリエチレン(LDPE)(LDPE 410−E、DOW、USA)の2枚の顔料無添加のフィルムを使用して、実施例22の手順を繰り返した。この結果として、ポリマーフィルムの溶着を誘導することはできなかった。
Claims (21)
- プラスチック中のレーザーマーキング剤またはレーザー溶着化剤としての、アンチモンおよび/またはアンチモン含有化合物を含まない球体金属粒子の使用であって、前記球体金属粒子の粒子サイズ分布が、レーザー粒度測定法によって求めて、体積平均累積篩下粒子サイズ分布の形で、D99値が<110μm、D90値が<75μm、そしてD50が<45μmである、球体金属粒子の使用。
- 前記球体金属粒子の累積篩下粒子サイズ分布が、D99値が<70μmであり、そしてD90値が<40μmであることを特徴とする、請求項1に記載のレーザーマーキング剤またはレーザー溶着化剤としての球体金属粒子の使用。
- 前記球体金属粒子の累積篩下粒子サイズ分布が、D99値が<65μmであり、そしてD90値が<36μmであることを特徴とする、請求項1または2に記載のレーザーマーキング剤またはレーザー溶着化剤としての球体金属粒子の使用。
- 前記金属粒子が、アルミニウム、銅、銀、金、亜鉛、スズ、鉄、チタン、バナジウム、マグネシウム、およびそれらの合金からなる群より選択される金属を含むか、またはそれらからなることを特徴とする、先行する請求項のいずれかに記載のレーザーマーキング剤またはレーザー溶着化剤としての球体金属粒子の使用。
- 前記金属粒子が、前記金属粒子の全重量を基準にして、10重量%以下の金属酸化物含量を有することを特徴とする、先行する請求項のいずれかに記載のレーザーマーキング剤またはレーザー溶着化剤としての球体金属粒子の使用。
- 前記金属粒子が、少なくとも1層の無機金属酸化物層を備えていることを特徴とする、先行する請求項のいずれかに記載のレーザーマーキング剤またはレーザー溶着化剤としての球体金属粒子の使用。
- 前記金属酸化物層が、SiO2を含むか、またはSiO2からなることを特徴とする、請求項6に記載のレーザーマーキング剤またはレーザー溶着化剤としての球体金属粒子の使用。
- マスターバッチであって、
前記マスターバッチが、請求項1〜7に記載の使用のための前記球体金属顔料と、さらに少なくとも1種の分散担体を含むことを特徴とする、マスターバッチ。 - 前記分散担体が、プラスチック成分、ワックス、樹脂、添加剤、またはそれらの混合物からなる群より選択されることを特徴とする、請求項8に記載のマスターバッチ。
- 前記マスターバッチ中の球体金属粒子の量が、前記マスターバッチの全重量を基準にして、80%〜99重量%であることを特徴とする、請求項8または9に記載のマスターバッチ。
- 前記マスターバッチ中の球体金属粒子の量が、前記マスターバッチの全重量を基準にして、0.001%〜5重量%であることを特徴とする、請求項8に記載のマスターバッチ。
- レーザーマーク可能および/またはレーザー溶着可能なプラスチックを製造するための、請求項8〜11のいずれかに記載のマスターバッチの使用。
- レーザーマーク可能および/またはレーザー溶着可能なプラスチックであって、
前記プラスチックが、請求項1〜7のいずれかに記載のレーザーマーキング剤、または請求項8〜11のいずれかに記載のマスターバッチを含むことを特徴とする、レーザーマーク可能および/またはレーザー溶着可能なプラスチック。 - 前記プラスチック中の前記金属粒子の割合が、それぞれの場合において、前記プラスチックの全重量を基準にして、0.0005%〜0.8重量%、好ましくは0.001%〜0.5重量%であることを特徴とする、請求項13に記載のレーザーマーク可能および/またはレーザー溶着可能なプラスチック。
- 前記プラスチック中の前記金属粒子の割合が、それぞれの場合において、前記レーザーマーク可能なプラスチックの全重量を基準にして、0.005%〜0.5重量%、好ましくは0.01%〜0.1重量%であることを特徴とする、請求項13および14のいずれかに記載のレーザーマーク可能および/またはレーザー溶着可能なプラスチック。
- 前記プラスチックが、プラスチックフィルムまたはラベルであることを特徴とする、請求項13に記載のレーザーマーク可能および/またはレーザー溶着可能なプラスチック。
- 前記プラスチックが、それぞれの場合において、前記レーザーマーク可能なプラスチックフィルムの全重量を基準にして、0.01%〜1.0重量%、好ましくは0.02%〜0.5重量%の金属粒子の割合を有するプラスチックフィルムであることを特徴とする、請求項16に記載のレーザーマーク可能および/またはレーザー溶着可能なプラスチック。
- 前記プラスチックが、三次元プラスチック体であることを特徴とする、請求項13〜15のいずれかに記載のレーザーマーク可能および/またはレーザー溶着可能なプラスチック。
- 前記レーザーマーク可能および/またはレーザー溶着可能なプラスチックが、それ自体はレーザーマーク可能および/またはレーザー溶着可能である必要がない物品の構成要素であることを特徴とする、請求項13〜18のいずれかに記載のレーザーマーク可能および/またはレーザー溶着可能なプラスチック。
- 前記プラスチックが、熱可塑性プラスチック、熱硬化性プラスチック、エラストマー、またはゴムを含むことを特徴とする、請求項13〜19のいずれかに記載のレーザーマーク可能なプラスチック。
- 前記プラスチックが、熱可塑性プラスチックを含むことを特徴とする、請求項13〜19のいずれかに記載のレーザー溶着可能なプラスチック。
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KR20100108542A (ko) * | 2007-11-30 | 2010-10-07 | 엑카르트 게엠베하 | 레이저 마킹제 또는 레이저 용접제로서 구형 금속 입자 및 금속 플레이크를 포함하는 혼합물의 용도, 및 레이저 마킹가능한 및/또는 레이저 용접가능한 플라스틱 |
JP2011506124A (ja) * | 2007-11-30 | 2011-03-03 | エッカルト ゲゼルシャフト ミット ベシュレンクテル ハフツング | レーザーマーキング剤またはレーザー溶着化剤としての球状金属粒子および金属フレークを含む混合物の使用、ならびにレーザーマーク可能および/またはレーザー溶着可能なプラスチック |
US8877332B2 (en) | 2007-11-30 | 2014-11-04 | Eckart Gmbh | Use of a mixture comprising spherical metal particles and metal flakes as laser-marking or laser-weldability agents and laser markable and/or laser weldable plastic |
KR101595582B1 (ko) | 2007-11-30 | 2016-02-18 | 엑카르트 게엠베하 | 레이저 마킹제 또는 레이저 용접제로서 구형 금속 입자 및 금속 플레이크를 포함하는 혼합물의 용도, 및 레이저 마킹가능한 및/또는 레이저 용접가능한 플라스틱 |
JP2010189504A (ja) * | 2009-02-17 | 2010-09-02 | Mitsubishi Plastics Inc | ポリエステルフィルム |
JP2020185614A (ja) * | 2020-08-21 | 2020-11-19 | 三信化工株式会社 | レーザーマーキングされた樹脂製成形体およびその製造方法 |
JP6997475B2 (ja) | 2020-08-21 | 2022-01-17 | 三信化工株式会社 | レーザーマーキングされた樹脂製成形体およびその製造方法 |
WO2023149503A1 (ja) * | 2022-02-04 | 2023-08-10 | 三菱ケミカル株式会社 | 樹脂組成物、成形体、ペレット、および、レーザー溶着体 |
Also Published As
Publication number | Publication date |
---|---|
CN101610894A (zh) | 2009-12-23 |
DE502007000647D1 (de) | 2009-06-04 |
EP1968781B1 (de) | 2009-04-22 |
DE102006062269A1 (de) | 2008-06-26 |
CN101610894B (zh) | 2013-04-17 |
ATE429322T1 (de) | 2009-05-15 |
US20100009171A1 (en) | 2010-01-14 |
JP5043125B2 (ja) | 2012-10-10 |
EP1968781A1 (de) | 2008-09-17 |
WO2008083726A1 (de) | 2008-07-17 |
US8318262B2 (en) | 2012-11-27 |
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