FR2384734A1 - Procede de preparation d'octafluoropropane - Google Patents
Procede de preparation d'octafluoropropaneInfo
- Publication number
- FR2384734A1 FR2384734A1 FR7808493A FR7808493A FR2384734A1 FR 2384734 A1 FR2384734 A1 FR 2384734A1 FR 7808493 A FR7808493 A FR 7808493A FR 7808493 A FR7808493 A FR 7808493A FR 2384734 A1 FR2384734 A1 FR 2384734A1
- Authority
- FR
- France
- Prior art keywords
- octafluoropropane
- hexafluoropropene
- reacted
- temperatures
- degrees
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/07—Preparation of halogenated hydrocarbons by addition of hydrogen halides
- C07C17/08—Preparation of halogenated hydrocarbons by addition of hydrogen halides to unsaturated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/07—Preparation of halogenated hydrocarbons by addition of hydrogen halides
- C07C17/087—Preparation of halogenated hydrocarbons by addition of hydrogen halides to unsaturated halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Procédé de préparation d'octafluoropropane à partir d'hexafluoropropène. On fait réagir, dans une première étape, l'hexafluoropropène avec du fluorure d'hydrogène, à des températures de 100 à 350 degrés C, en présence d'un catalyseur d'oxyfluorure de chrome 3, pour former le 2H-heptafluoropropane, puis, dans une seconde étape, on fait réagir le gaz réactionnel obtenu, à des températures de 100 à 350 degrés C, en présence d'un catalyseur 6 contenant un élément de sous-groupes du tableau periodique sous la forme de fluorure ou de métal, avec du fluor élémentaire pour obtenir l'octafluoropropane, et on sépare de celui-ci le fluorure d'hydrogène formé. L'octafluoropropane a de nombreuses applications : milieu réactionnel inerte, diélectrique, propulseur, liquide caloporteur, etc.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2712732A DE2712732C2 (de) | 1977-03-23 | 1977-03-23 | Verfahren zur Herstellung von Oktafluorpropan |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2384734A1 true FR2384734A1 (fr) | 1978-10-20 |
Family
ID=6004433
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7808493A Pending FR2384734A1 (fr) | 1977-03-23 | 1978-03-23 | Procede de preparation d'octafluoropropane |
Country Status (9)
Country | Link |
---|---|
US (1) | US4158023A (fr) |
JP (1) | JPS53119802A (fr) |
BE (1) | BE865260A (fr) |
CA (1) | CA1107766A (fr) |
DE (1) | DE2712732C2 (fr) |
FR (1) | FR2384734A1 (fr) |
GB (1) | GB1568020A (fr) |
IT (1) | IT1093902B (fr) |
NL (1) | NL189085C (fr) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1995032935A1 (fr) * | 1994-05-26 | 1995-12-07 | E.I. Du Pont De Nemours And Company | Production de 1,2-dihydro et 2,2-dihydro hexafluoropropanes et d'azeotropes de ces derniers a l'aide de fluorure d'hydrogene |
WO1998028247A1 (fr) * | 1996-12-23 | 1998-07-02 | Alliedsignal Inc. | Procede de production de 1,1,1,2,3,3,3-heptafluoropropane |
WO1999006342A1 (fr) * | 1997-07-31 | 1999-02-11 | Imperial Chemical Industries Plc | Preparation de 1,1,1,2,3,3,3-heptafluoropropane en phase vapeur |
US6472574B2 (en) | 1999-12-10 | 2002-10-29 | E. I. Du Pont Nemours And Company | Production of 1,2-dihydro and 2,2-dihydro hexafluoropropanes and azeotropes thereof with HF |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4377715A (en) * | 1979-12-26 | 1983-03-22 | Allied Corporation | Production of perfluoropropane |
DE3009760A1 (de) * | 1980-03-14 | 1981-09-24 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von hochreinen teilfluorierten aethanen |
JP2513758B2 (ja) * | 1988-01-08 | 1996-07-03 | 関東電化工業株式会社 | トリフルオロメチル基を有する炭化水素化合物のフッ素化方法 |
DE3905726A1 (de) * | 1989-02-24 | 1990-08-30 | Hoechst Ag | Druckgaspackung und treibmittel fuer aerosole |
DE3908551A1 (de) * | 1989-03-16 | 1990-09-20 | Hoechst Ag | Fuellmedium fuer fuehlersysteme von temperatur-weg-gebern |
US5406008A (en) * | 1989-12-28 | 1995-04-11 | E. I. Du Pont De Nemours And Company | Process for the manufacture of hydrofluorocarbons |
US5387323A (en) * | 1993-08-31 | 1995-02-07 | Minnesota Mining And Manufacturing Company | Process for preparing fluorochemicals |
JP3213929B2 (ja) * | 1994-07-14 | 2001-10-02 | ダイキン工業株式会社 | 1,1,1,2,3,3,3−ヘプタフルオロプロパンの製造方法 |
US6376727B1 (en) | 1997-06-16 | 2002-04-23 | E. I. Du Pont De Nemours And Company | Processes for the manufacture of 1,1,1,3,3-pentafluoropropene, 2-chloro-pentafluoropropene and compositions comprising saturated derivatives thereof |
US6224781B1 (en) | 1997-08-25 | 2001-05-01 | E. I. Du Pont De Nemours And Company | Compositions comprising hydrofluorocarbons and their manufacture |
US6107267A (en) * | 1997-08-25 | 2000-08-22 | E. I. Du Pont De Nemours And Company | Compositions comprising CF3 CF2 CHF2 and their manufacture |
US6407297B1 (en) | 1997-11-25 | 2002-06-18 | Ineos Fluor Holdings Limited | Preparation of fluorine-containing organic compounds |
US6018083A (en) * | 1998-04-03 | 2000-01-25 | E. I. Du Pont De Nemours And Company | Process for the production of fluorocarbons |
US6281395B1 (en) | 1998-04-03 | 2001-08-28 | E. I. Du Pont De Nemours And Company | 1,1,1,2,3,3,3-heptafluoropropane manufacturing process |
AU2001280179A1 (en) * | 2000-08-30 | 2002-03-13 | Showa Denko K K | Production and use of octafluoropropane |
JP4539793B2 (ja) * | 2000-08-30 | 2010-09-08 | 昭和電工株式会社 | オクタフルオロプロパンの製造方法及びその用途 |
EP1351908B1 (fr) | 2001-01-15 | 2005-07-20 | Showa Denko K.K. | Procede de preparation d'octafluoropropane |
US7064240B2 (en) * | 2001-02-23 | 2006-06-20 | Showa Denko K.K. | Process for producing perfluorocarbons and use thereof |
JP4703865B2 (ja) * | 2001-02-23 | 2011-06-15 | 昭和電工株式会社 | パーフルオロカーボン類の製造方法およびその用途 |
KR100447804B1 (ko) * | 2001-07-09 | 2004-09-08 | 울산화학주식회사 | 고순도 퍼플루오로프로판의 제조방법 |
EP1291337A1 (fr) * | 2001-09-07 | 2003-03-12 | SOLVAY (Société Anonyme) | Procédé pour l'obtention d'heptafluoropropane purifié |
US7329786B2 (en) * | 2001-09-28 | 2008-02-12 | Great Lakes Chemical Corporation | Processes for producing CF3CFHCF3 |
US7223351B2 (en) * | 2003-04-17 | 2007-05-29 | Great Lakes Chemical Corporation | Fire extinguishing mixtures, methods and systems |
US20050038302A1 (en) * | 2003-08-13 | 2005-02-17 | Hedrick Vicki E. | Systems and methods for producing fluorocarbons |
JP2007176842A (ja) * | 2005-12-27 | 2007-07-12 | Showa Denko Kk | オクタフルオロプロパンの製造方法 |
US11034636B2 (en) | 2018-01-17 | 2021-06-15 | Showa Denko K.K. | Method for producing tetrafluoromethane |
KR102487702B1 (ko) * | 2018-01-19 | 2023-01-12 | 쇼와 덴코 가부시키가이샤 | 테트라플루오로메탄의 제조 방법 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB630606A (en) * | 1944-06-23 | 1949-10-18 | Walter Norman Haworth | Production of fluorocarbons and fluorohydrocarbons |
GB785641A (en) * | 1943-03-09 | 1957-10-30 | Atomic Energy Authority Uk | Process for the preparation of fluorocarbons |
FR1287036A (fr) * | 1960-03-22 | 1962-03-09 | Allied Chem | Production d'heptafluoropropane par réaction catalytique en phase gazeuse d'hexafluoropropène et d'acide fluorhydrique |
GB902590A (en) * | 1960-03-22 | 1962-08-01 | Allied Chem | Production of heptafluoropropane |
FR2403321A1 (fr) * | 1977-09-20 | 1979-04-13 | Ici Ltd | Procede de production du 1,1,1,2-tetrafluoroethane |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2981763A (en) * | 1960-03-22 | 1961-04-25 | Allied Chem | Manufacture of fluorocarbons |
US3047640A (en) * | 1960-03-22 | 1962-07-31 | Allied Chem | Production of fluoropropene |
DE1900241C3 (de) * | 1969-01-03 | 1978-09-21 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von fluorierten aliphatischen Kohlenwasserstoffen mit zwei und mehr C-Atomen oder von fluorierten cycloaliphatischen Kohlenwasserstoffen |
NL7408139A (fr) * | 1973-06-23 | 1974-12-30 |
-
1977
- 1977-03-23 DE DE2712732A patent/DE2712732C2/de not_active Expired
-
1978
- 1978-03-21 IT IT21441/78A patent/IT1093902B/it active
- 1978-03-21 GB GB11144/78A patent/GB1568020A/en not_active Expired
- 1978-03-21 US US05/888,731 patent/US4158023A/en not_active Expired - Lifetime
- 1978-03-22 NL NLAANVRAGE7803103,A patent/NL189085C/xx not_active IP Right Cessation
- 1978-03-22 CA CA299,523A patent/CA1107766A/fr not_active Expired
- 1978-03-22 JP JP3281978A patent/JPS53119802A/ja active Granted
- 1978-03-23 FR FR7808493A patent/FR2384734A1/fr active Pending
- 1978-03-23 BE BE186232A patent/BE865260A/fr unknown
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB785641A (en) * | 1943-03-09 | 1957-10-30 | Atomic Energy Authority Uk | Process for the preparation of fluorocarbons |
GB630606A (en) * | 1944-06-23 | 1949-10-18 | Walter Norman Haworth | Production of fluorocarbons and fluorohydrocarbons |
FR1287036A (fr) * | 1960-03-22 | 1962-03-09 | Allied Chem | Production d'heptafluoropropane par réaction catalytique en phase gazeuse d'hexafluoropropène et d'acide fluorhydrique |
GB902590A (en) * | 1960-03-22 | 1962-08-01 | Allied Chem | Production of heptafluoropropane |
FR2403321A1 (fr) * | 1977-09-20 | 1979-04-13 | Ici Ltd | Procede de production du 1,1,1,2-tetrafluoroethane |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1995032935A1 (fr) * | 1994-05-26 | 1995-12-07 | E.I. Du Pont De Nemours And Company | Production de 1,2-dihydro et 2,2-dihydro hexafluoropropanes et d'azeotropes de ces derniers a l'aide de fluorure d'hydrogene |
US5563304A (en) * | 1994-05-26 | 1996-10-08 | E. I. Du Pont De Nemours And Company | Production of 1,2-dihydro and 2,2-dihydro hexafluoropropanes and azeotropes thereof with HF |
US6388147B1 (en) | 1994-05-26 | 2002-05-14 | E. I. Du Pont De Nemours And Company | Production of 1,2-dihydro and 2,2-dihydro hexafluoropropanes and azeotropes thereof with HF |
WO1998028247A1 (fr) * | 1996-12-23 | 1998-07-02 | Alliedsignal Inc. | Procede de production de 1,1,1,2,3,3,3-heptafluoropropane |
WO1999006342A1 (fr) * | 1997-07-31 | 1999-02-11 | Imperial Chemical Industries Plc | Preparation de 1,1,1,2,3,3,3-heptafluoropropane en phase vapeur |
US6472574B2 (en) | 1999-12-10 | 2002-10-29 | E. I. Du Pont Nemours And Company | Production of 1,2-dihydro and 2,2-dihydro hexafluoropropanes and azeotropes thereof with HF |
Also Published As
Publication number | Publication date |
---|---|
US4158023A (en) | 1979-06-12 |
GB1568020A (en) | 1980-05-21 |
DE2712732A1 (de) | 1978-09-28 |
JPS6220170B2 (fr) | 1987-05-06 |
BE865260A (fr) | 1978-09-25 |
IT7821441A0 (it) | 1978-03-21 |
NL189085C (nl) | 1993-01-04 |
NL7803103A (nl) | 1978-09-26 |
CA1107766A (fr) | 1981-08-25 |
DE2712732C2 (de) | 1986-03-13 |
JPS53119802A (en) | 1978-10-19 |
NL189085B (nl) | 1992-08-03 |
IT1093902B (it) | 1985-07-26 |
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