EA201270641A1 - Катализатор и способ получения амина - Google Patents
Катализатор и способ получения аминаInfo
- Publication number
- EA201270641A1 EA201270641A1 EA201270641A EA201270641A EA201270641A1 EA 201270641 A1 EA201270641 A1 EA 201270641A1 EA 201270641 A EA201270641 A EA 201270641A EA 201270641 A EA201270641 A EA 201270641A EA 201270641 A1 EA201270641 A1 EA 201270641A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- catalyst
- cobalt
- nickel
- primary
- containing compounds
- Prior art date
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/835—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with germanium, tin or lead
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/03—Precipitation; Co-precipitation
- B01J37/031—Precipitation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/03—Precipitation; Co-precipitation
- B01J37/031—Precipitation
- B01J37/035—Precipitation on carriers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
- C07D295/027—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements containing only one hetero ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
- C07D295/027—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements containing only one hetero ring
- C07D295/03—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements containing only one hetero ring with the ring nitrogen atoms directly attached to acyclic carbon atoms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/16—Reducing
- B01J37/18—Reducing with gases containing free hydrogen
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
Изобретение кается способа получения амина посредством реакции обмена первичного или вторичного спирта, альдегида и/или кетона с водородом и соединением азота, выбранным из группы аммиака, первичных и вторичных аминов, в присутствии содержащего медь, никель и кобальт катализатора на инертном носителе, причем каталитически активная масса катализатора перед восстановлением водородом содержит кислородсодержащие соединения алюминия, меди, никеля и кобальта и 0,2-5,0 мас.% кислородсодержащих соединений олова, рассчитанных как SnO, а также катализаторов, как определено выше.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09177914 | 2009-12-03 | ||
PCT/EP2010/068375 WO2011067199A1 (de) | 2009-12-03 | 2010-11-29 | Katalysator und verfahren zur herstellung eines amins |
Publications (2)
Publication Number | Publication Date |
---|---|
EA201270641A1 true EA201270641A1 (ru) | 2013-01-30 |
EA021623B1 EA021623B1 (ru) | 2015-07-30 |
Family
ID=43971025
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EA201270641A EA021623B1 (ru) | 2009-12-03 | 2010-11-29 | Катализатор на носителе и способ получения амина |
Country Status (8)
Country | Link |
---|---|
US (1) | US8487135B2 (ru) |
EP (1) | EP2506966B1 (ru) |
JP (1) | JP5755236B2 (ru) |
CN (1) | CN102639231B (ru) |
EA (1) | EA021623B1 (ru) |
SA (1) | SA110310894B1 (ru) |
SG (1) | SG181100A1 (ru) |
WO (1) | WO2011067199A1 (ru) |
Families Citing this family (87)
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JP5755237B2 (ja) | 2009-12-03 | 2015-07-29 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 触媒及びアミンの製造方法 |
CN102639231B (zh) | 2009-12-03 | 2014-12-10 | 巴斯夫欧洲公司 | 制备胺的催化剂和方法 |
US8445726B2 (en) | 2010-04-07 | 2013-05-21 | Basf Se | Process for preparing unsymmetric secondary tert-butylamines in the liquid phase |
US8450530B2 (en) | 2010-04-07 | 2013-05-28 | Basf Se | Process for preparing unsymmetric secondary tert-butylamines in the gas phase |
US8455693B2 (en) | 2010-05-21 | 2013-06-04 | Basf Se | Process for preparing 2-(2-tert-butylaminoethoxy)ethanol (tert-butylaminodiglycol, TBADG) |
US8637668B2 (en) | 2010-06-15 | 2014-01-28 | Basf Se | Process for preparing a cyclic tertiary methylamine |
US8710269B2 (en) | 2010-07-29 | 2014-04-29 | Basf Se | DMAPN having a low DGN content and a process for preparing DMAPA having a low DGN content |
US8933223B2 (en) | 2010-10-14 | 2015-01-13 | Basf Se | Process for preparing a cyclic tertiary amine |
US9193666B2 (en) | 2011-03-08 | 2015-11-24 | Basf Se | Process for preparing alkanolamines by homogeneously catalyzed alcohol amination |
US8912361B2 (en) | 2011-03-08 | 2014-12-16 | Basf Se | Process for preparing di-, tri- and polyamines by homogeneously catalyzed alcohol amination |
US8637709B2 (en) | 2011-03-08 | 2014-01-28 | Basf Se | Process for the preparation of primary amines by homogeneously catalyzed alcohol amination |
US8785693B2 (en) | 2011-03-08 | 2014-07-22 | Basf Se | Process for the preparation of primary amines by homogeneously catalyzed alcohol amination |
KR101403698B1 (ko) | 2011-07-29 | 2014-06-27 | 한국에너지기술연구원 | 금속 구조체 촉매 및 이의 제조방법 |
US8946459B2 (en) | 2011-08-31 | 2015-02-03 | Basf Se | Process for preparing EDDN and/or EDMN by reacting EDFA and/or EDMFA with HCN |
US8952156B2 (en) | 2011-08-31 | 2015-02-10 | Basf Se | Process for working up reaction outputs from the hydrogenation of EDDN or EDMN |
US9096497B2 (en) | 2011-08-31 | 2015-08-04 | Basf Se | Process for preparing EDDN and EDMN |
US9012638B2 (en) | 2011-08-31 | 2015-04-21 | Basf Se | Process for preparing EDDN and/or EDMN by conversion of FACH and EDA |
IN2014DN03136A (ru) | 2011-11-17 | 2015-05-22 | Basf Se | |
US9040451B2 (en) | 2011-11-17 | 2015-05-26 | Basf Se | Process for producing Sn-comprising catalysts |
HUE029629T2 (en) * | 2012-06-01 | 2017-03-28 | Basf Se | A method for preparing a mono-N-alkylpiperazine |
US8884015B2 (en) | 2012-06-01 | 2014-11-11 | Basf Se | Process for the preparation of a mono-N-alkypiperazine |
HUE027611T2 (en) | 2012-06-01 | 2016-10-28 | Basf Se | Process for the preparation of monoalkyl piperazines |
IN2014DN09263A (ru) | 2012-06-06 | 2015-07-10 | Basf Se | |
US8981093B2 (en) | 2012-06-06 | 2015-03-17 | Basf Se | Process for preparing piperazine |
WO2013182465A1 (de) | 2012-06-06 | 2013-12-12 | Basf Se | Verfahren zur herstellung von piperazin |
US9315479B2 (en) | 2012-07-13 | 2016-04-19 | Basf Se | Process for preparing pyrrolidine |
JP6261576B2 (ja) * | 2012-07-13 | 2018-01-17 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | ピロリジンの製造法 |
JP6159327B2 (ja) * | 2012-07-20 | 2017-07-05 | 広栄化学工業株式会社 | 2−(イソプロピルアミノ)エタノールの製造方法 |
DE102012016433A1 (de) | 2012-08-17 | 2014-05-15 | Oxea Gmbh | Kontinuierliches Verfahren zur Herstellung primärer aliphatischer Amine aus Aldehyden |
CN102895978B (zh) * | 2012-10-19 | 2014-11-12 | 南京信息工程大学 | 一种用于合成多氨基化合物的催化剂及其制备方法与应用 |
US9126866B2 (en) | 2013-03-06 | 2015-09-08 | Construction Research & Technology Gmbh | Polycarboxylate ethers with branched side chains |
EP2774899A1 (de) | 2013-03-06 | 2014-09-10 | Construction Research & Technology GmbH | Polycarboxylatether mit verzweigten Seitenketten |
BR112015024601A2 (pt) | 2013-03-28 | 2017-07-18 | Basf Se | mistura de éter amina, processo para fabricação de uma mistura de éter amina, e, uso de uma mistura de éter amina |
HUE043499T2 (hu) | 2013-03-28 | 2019-09-30 | Procter & Gamble | Poliéteramin-tartalmú tiszítószerek |
WO2014184048A1 (de) * | 2013-05-16 | 2014-11-20 | Basf Se | Verfahren zur herstellung von n-alkyl-piperazinen |
WO2014184039A1 (de) | 2013-05-16 | 2014-11-20 | Basf Se | Verfahren zur herstellung von n-alkyl-piperazinen |
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WO2015140023A2 (de) * | 2014-03-19 | 2015-09-24 | Basf Se | Verfahren zur herstellung tertiärer amine |
JP6275864B2 (ja) | 2014-03-27 | 2018-02-07 | ザ プロクター アンド ギャンブル カンパニー | ポリエーテルアミンを含有する洗浄組成物 |
CN106132918A (zh) * | 2014-03-27 | 2016-11-16 | 巴斯夫欧洲公司 | 基于1,2‑二醇的醚胺 |
JP2017517560A (ja) | 2014-03-27 | 2017-06-29 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | ジアルコールをベースとするエーテルアミン |
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US9974985B2 (en) | 2014-05-15 | 2018-05-22 | Basf Se | Etheramines based on 1,2-dialcohols |
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US9388368B2 (en) | 2014-09-26 | 2016-07-12 | The Procter & Gamble Company | Cleaning compositions containing a polyetheramine |
CN107001612B (zh) | 2014-12-12 | 2019-12-10 | 巴斯夫欧洲公司 | 制备聚醚胺的方法 |
EP3061743A1 (de) | 2015-02-25 | 2016-08-31 | Basf Se | Verfahren zur Herstellung von primären Aminen unter Verwendung eines Nickel-Festbettkatalysators |
EP3162880A1 (en) | 2015-10-29 | 2017-05-03 | The Procter and Gamble Company | Liquid detergent composition |
ES2689048T3 (es) | 2015-10-29 | 2018-11-08 | The Procter & Gamble Company | Composición detergente líquida |
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EP3257924A1 (en) | 2016-06-17 | 2017-12-20 | The Procter and Gamble Company | Liquid detergent composition |
EP3279301A1 (en) | 2016-08-04 | 2018-02-07 | The Procter & Gamble Company | Water-soluble unit dose article comprising a cleaning amine |
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EP3634934B1 (de) | 2017-06-09 | 2022-04-06 | Basf Se | Verfahren zur herstellung von ethylenaminen |
JP7105811B2 (ja) * | 2017-06-09 | 2022-07-25 | ビーエーエスエフ ソシエタス・ヨーロピア | エチレンアミンの製造方法 |
CN111093803B (zh) | 2017-09-04 | 2022-06-24 | 巴斯夫欧洲公司 | 用于选择性去除硫化氢的吸收剂和方法 |
WO2019105782A1 (de) | 2017-11-30 | 2019-06-06 | Basf Se | Verfahren zur kontinuierlichen herstellung von 1,2-propylendiamin (1,2-pda) und dimethyldiet-hylentriamin (dmdeta) |
HUE058944T2 (hu) | 2018-02-22 | 2022-09-28 | Basf Se | Eljárás 2-metoxietanol (MOE) szegényítésére |
EP3755691B1 (de) | 2018-02-22 | 2022-04-06 | Basf Se | Verfahren zur kontinuierlichen destillativen auftrennung von gemischen enthaltend morpholin (mo), monoaminodiglykol (adg), ammoniak, wasser und methoxyethanol (moe) |
WO2019174221A1 (en) * | 2018-03-15 | 2019-09-19 | Rhodia Operations | Process for producing an amine in a solvent system containing water |
US11390578B2 (en) * | 2018-04-06 | 2022-07-19 | Basf Se | Method for synthesizing amines |
CN109678734B (zh) * | 2018-12-27 | 2021-12-21 | 浙江工业大学 | 一种由乙二醇单甲醚直接催化胺化制备2-甲氧基乙胺的方法 |
CN113453784A (zh) | 2019-02-18 | 2021-09-28 | 巴斯夫欧洲公司 | 从流体料流中脱除酸性气体的方法 |
CA3153809A1 (en) | 2019-09-10 | 2021-03-18 | Basf Se | Process for removal of acid gases from a fluid stream |
CN112691677B (zh) * | 2019-10-23 | 2024-02-13 | 中国石油化工股份有限公司 | 一种乙醇临氢氨化制备乙胺的催化剂及其制法和应用 |
CA3163479A1 (en) | 2019-12-03 | 2021-06-10 | Basf Se | Process for preparing amines over a copper catalyst |
CN114425347B (zh) * | 2020-10-29 | 2023-08-08 | 中国石油化工股份有限公司 | 环己亚胺的合成方法 |
CN114433113B (zh) * | 2020-10-30 | 2023-07-21 | 中国石油化工股份有限公司 | 具有催化醇氨化功能的催化剂和载体及其制备方法和应用 |
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WO2022179864A1 (en) | 2021-02-25 | 2022-09-01 | Basf Se | Process for the production of polyalkylene-polyamines by condensation of alkylene-diamines |
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CN113856726B (zh) * | 2021-10-28 | 2023-05-23 | 中南大学 | 一种适用于β-硝基醇制备的高效低成本非均相催化剂 |
WO2023135035A1 (en) | 2022-01-14 | 2023-07-20 | Basf Se | Method for the manufacture or conversion of alkanolamines |
CN114478353A (zh) * | 2022-02-21 | 2022-05-13 | 八叶草健康产业研究院(厦门)有限公司 | 一种褪黑素的合成方法 |
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DE10153410A1 (de) | 2001-10-30 | 2003-05-15 | Basf Ag | Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese |
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CN101489979B (zh) * | 2006-07-14 | 2015-04-08 | 巴斯夫欧洲公司 | 生产胺的方法 |
CN101903092B (zh) | 2007-12-21 | 2013-03-20 | 巴斯夫欧洲公司 | 生产胺的方法 |
WO2009080515A1 (de) | 2007-12-21 | 2009-07-02 | Basf Se | Verfahren zur herstellung eines amins |
US20100274008A1 (en) | 2007-12-21 | 2010-10-28 | Basf Se | Method for the production of an amine |
WO2009080509A1 (de) | 2007-12-21 | 2009-07-02 | Basf Se | Verfahren zur herstellung eines amins |
CN101903096B (zh) | 2007-12-21 | 2013-04-03 | 巴斯夫欧洲公司 | 生产胺的方法 |
JP2011506530A (ja) | 2007-12-21 | 2011-03-03 | ビーエーエスエフ ソシエタス・ヨーロピア | アミンの製造方法 |
EP2225029B1 (de) | 2007-12-21 | 2016-08-03 | Basf Se | Verfahren und katalysator zur herstellung eines amins |
JP2011513489A (ja) | 2008-03-10 | 2011-04-28 | ハンツマン ペトロケミカル エルエルシー | シクロヘキサンジメタノールの直接アミン化によるシクロヘキサンジメタンアミンの製造 |
CN102159311B (zh) | 2008-09-19 | 2013-07-10 | 巴斯夫欧洲公司 | 使用铝-铜催化剂连续制备胺的方法 |
CN102639231B (zh) | 2009-12-03 | 2014-12-10 | 巴斯夫欧洲公司 | 制备胺的催化剂和方法 |
JP5755237B2 (ja) | 2009-12-03 | 2015-07-29 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 触媒及びアミンの製造方法 |
-
2010
- 2010-11-29 CN CN201080054878.3A patent/CN102639231B/zh active Active
- 2010-11-29 JP JP2012541434A patent/JP5755236B2/ja active Active
- 2010-11-29 WO PCT/EP2010/068375 patent/WO2011067199A1/de active Application Filing
- 2010-11-29 EP EP10784512.5A patent/EP2506966B1/de active Active
- 2010-11-29 EA EA201270641A patent/EA021623B1/ru not_active IP Right Cessation
- 2010-11-29 SG SG2012039202A patent/SG181100A1/en unknown
- 2010-12-02 US US12/958,545 patent/US8487135B2/en active Active
- 2010-12-04 SA SA110310894A patent/SA110310894B1/ar unknown
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US8487135B2 (en) | 2013-07-16 |
SA110310894B1 (ar) | 2014-10-15 |
SG181100A1 (en) | 2012-07-30 |
JP2013512871A (ja) | 2013-04-18 |
CN102639231B (zh) | 2014-12-10 |
CN102639231A (zh) | 2012-08-15 |
EA021623B1 (ru) | 2015-07-30 |
WO2011067199A1 (de) | 2011-06-09 |
JP5755236B2 (ja) | 2015-07-29 |
US20110137030A1 (en) | 2011-06-09 |
EP2506966A1 (de) | 2012-10-10 |
EP2506966B1 (de) | 2017-08-16 |
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