DE68918524D1 - Pyrazol-Derivate und diese enthaltende Herbizide. - Google Patents

Pyrazol-Derivate und diese enthaltende Herbizide.

Info

Publication number
DE68918524D1
DE68918524D1 DE68918524T DE68918524T DE68918524D1 DE 68918524 D1 DE68918524 D1 DE 68918524D1 DE 68918524 T DE68918524 T DE 68918524T DE 68918524 T DE68918524 T DE 68918524T DE 68918524 D1 DE68918524 D1 DE 68918524D1
Authority
DE
Germany
Prior art keywords
alkyl
hydrogen
alkoxy
halogen
substituted
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE68918524T
Other languages
English (en)
Other versions
DE68918524T2 (de
Inventor
Eiichi C O Nissan Chemical Oya
Junichi C O Nissan Ch Watanabe
Yasuo C O Nissan Chemica Kondo
Takuya C O Nissan Chemi Kakuta
Koichi C O Nissan Chemi Suzuki
Tsutomu C O Nissan Ch Nawamaki
Shigeomi C O Nissan C Watanabe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nissan Chemical Corp
Original Assignee
Nissan Chemical Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nissan Chemical Corp filed Critical Nissan Chemical Corp
Publication of DE68918524D1 publication Critical patent/DE68918524D1/de
Application granted granted Critical
Publication of DE68918524T2 publication Critical patent/DE68918524T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D405/00—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom
    • C07D405/02—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom containing two hetero rings
    • C07D405/12—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom containing two hetero rings linked by a chain containing hetero atoms as chain links
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/27—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups
    • C07C205/35—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups having nitro groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C205/36—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups having nitro groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton to carbon atoms of the same non-condensed six-membered aromatic ring or to carbon atoms of six-membered aromatic rings being part of the same condensed ring system
    • C07C205/37—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups having nitro groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton to carbon atoms of the same non-condensed six-membered aromatic ring or to carbon atoms of six-membered aromatic rings being part of the same condensed ring system the oxygen atom of at least one of the etherified hydroxy groups being further bound to an acyclic carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C317/00—Sulfones; Sulfoxides
    • C07C317/44—Sulfones; Sulfoxides having sulfone or sulfoxide groups and carboxyl groups bound to the same carbon skeleton
    • C07C317/46—Sulfones; Sulfoxides having sulfone or sulfoxide groups and carboxyl groups bound to the same carbon skeleton the carbon skeleton being further substituted by singly-bound oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C07D231/22—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C07D231/22—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
    • C07D231/24—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms having sulfone or sulfonic acid radicals in the molecule
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D409/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having sulfur atoms as the only ring hetero atoms
    • C07D409/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having sulfur atoms as the only ring hetero atoms containing two hetero rings
    • C07D409/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having sulfur atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/08—Esters of oxyacids of phosphorus
    • C07F9/09—Esters of phosphoric acids
    • C07F9/12—Esters of phosphoric acids with hydroxyaryl compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/645—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having two nitrogen atoms as the only ring hetero atoms
    • C07F9/6503—Five-membered rings
    • C07F9/65031—Five-membered rings having the nitrogen atoms in the positions 1 and 2

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • Dentistry (AREA)
  • Engineering & Computer Science (AREA)
  • Plant Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Hydrogenated Pyridines (AREA)
DE68918524T 1988-07-15 1989-07-11 Pyrazol-Derivate und diese enthaltende Herbizide. Expired - Fee Related DE68918524T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP17675888 1988-07-15
JP2603089 1989-02-03

Publications (2)

Publication Number Publication Date
DE68918524D1 true DE68918524D1 (de) 1994-11-03
DE68918524T2 DE68918524T2 (de) 1995-05-04

Family

ID=26363753

Family Applications (1)

Application Number Title Priority Date Filing Date
DE68918524T Expired - Fee Related DE68918524T2 (de) 1988-07-15 1989-07-11 Pyrazol-Derivate und diese enthaltende Herbizide.

Country Status (13)

Country Link
US (2) US4986845A (de)
EP (1) EP0352543B1 (de)
KR (1) KR0128286B1 (de)
CN (1) CN1017240B (de)
AT (1) ATE112271T1 (de)
BR (1) BR8903486A (de)
CA (1) CA1338788C (de)
DE (1) DE68918524T2 (de)
DK (1) DK170439B1 (de)
ES (1) ES2064388T3 (de)
HU (1) HU205912B (de)
IL (1) IL90819A (de)
RU (2) RU1792280C (de)

Families Citing this family (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4008403A1 (de) * 1990-03-16 1991-09-19 Merck Patent Gmbh Glykolsaeurederivate
ATE180257T1 (de) * 1992-03-03 1999-06-15 Idemitsu Kosan Co Pyrazolderivate
DE4311722C1 (de) * 1993-04-08 1994-04-07 Basf Ag Verfahren zur Herstellung von Halogenmethyl-benzoylcyaniden und neue Halogenmethyl-benzoylcyanide
KR960705817A (ko) * 1993-11-09 1996-11-08 이데미쓰 유우치 피라졸유도체 및 그것을 이용한 제초제
JP3478412B2 (ja) * 1994-01-27 2003-12-15 富士写真フイルム株式会社 ピラゾール化合物
PL180802B1 (pl) * 1994-11-24 2001-04-30 Basf Ag Sposób wytwarzania cyjanków chlorowcometylo-benzoilu
EA001810B1 (ru) * 1995-02-13 2001-08-27 Идемицу Козан Ко., Лтд. Производные тиохроманпиразолов и гербицидная композиция на их основе
CZ293254B6 (cs) 1995-02-24 2004-03-17 Basf Aktiengesellschaft Pyrazolylbenzoylový derivát, způsob jeho přípravy, herbicidní prostředek s jeho obsahem a způsob potírání nežádoucích rostlin
DE19532312A1 (de) * 1995-09-01 1997-03-06 Basf Ag Pyrazol-4-yl-benzoylderivate
EE05455B1 (et) * 1997-01-17 2011-08-15 Basf Aktiengesellschaft 3-heterotskll-asendatud bensolderivaadid ja neid sisaldavad vahendid, nende saamise meetodid ning nende kasutamine herbitsiididena
AR012141A1 (es) * 1997-03-24 2000-09-27 Dow Agrosciences Llc PROCESO PARA PREPARAR 1-ALQUILO-4-(2-CLORO-3-ALCOXIBENCENO), COMPUESTOS INTERMEDIARIOS DE APLICACIoN EN DICHO PROCESO Y PROCEDIMIENTO PARA PREPARAR DICHOS COMPUESTOS INTERMEDIARIOS
US6211403B1 (en) 1997-03-24 2001-04-03 Dow Agrosciences Llc Process for preparing 2-chloro-3-alkoxy-4-alkylsulfonyl-benzoic acids and esters
AR012142A1 (es) * 1997-03-24 2000-09-27 Dow Agrosciences Llc Compuestos de 1-alquil-4-benzoil-5-hiroxipirazol, composiciones herbicidas que los contienen; metodo para controlar vegetacion no deseada y compuestosintermediarios utiles para preparar dichos compuestos
CA2289003A1 (en) * 1997-05-07 1998-11-12 Basf Aktiengesellschaft Substituted 4-benzoyl-pyrazoles
EP0914317A2 (de) 1997-05-23 1999-05-12 Dow AgroSciences LLC 1-alkyl-4-benzoyl-5-hydroxypyrazol-verbindungen und ihre verwendung als herbizide
US6140271A (en) * 1998-05-22 2000-10-31 Dow Agrosciences Llc 1-alkyl-4-benzoyl-5-hydroxypyrazole compounds and their use as herbicides
DE69933222T2 (de) * 1998-07-14 2007-01-04 Nippon Soda Co. Ltd. Benzoesäurederivate und verfahren zu ihrer herstellung
JP2002531562A (ja) 1998-12-04 2002-09-24 ビーエーエスエフ アクチェンゲゼルシャフト ３−（ヘテロシクリル）−置換ベンゾイルピラゾール類
DE19914140A1 (de) * 1999-03-27 2000-09-28 Bayer Ag Substituierte Benzoylpyrazole
DE19946853A1 (de) 1999-09-30 2001-04-05 Bayer Ag Substituierte Arylketone
US6864219B2 (en) 2000-01-17 2005-03-08 Bayer Aktiengesellschaft Substituted aryl ketones
DE10037149A1 (de) * 2000-07-29 2002-02-07 Bayer Ag Substituierte Arylketone
DE10043074A1 (de) * 2000-09-01 2002-03-14 Aventis Cropscience Gmbh Herbizid wirksame Benzoylcyclohexandione
EP1387831A1 (de) * 2001-05-09 2004-02-11 Bayer CropScience AG Substituierte arylketone
DE10136449A1 (de) * 2001-05-09 2002-11-14 Bayer Ag Substituierte Arylketone
DE10138577A1 (de) * 2001-05-21 2002-11-28 Bayer Ag Substituierte Benzoylpyrazole
DE10206792A1 (de) * 2002-02-19 2003-08-28 Bayer Cropscience Ag Substituierte Arylketone
DE10209645A1 (de) * 2002-03-05 2003-09-18 Bayer Cropscience Ag Substituierte Arylketone
DE10235945A1 (de) 2002-08-06 2004-02-19 Bayer Cropscience Gmbh 3-Aminocarbonyl substituierte Benzoylpyrazolone
WO2005058037A1 (en) * 2003-12-12 2005-06-30 Syngenta Participations Ag Picolinylpyrazoles as herbicides
KR100643510B1 (ko) * 2005-01-20 2006-11-10 박현문 반도체 장비용 대형 오링의 제조장치 및 그 성형장치에의해 제조된 대형 오링
AR056889A1 (es) * 2005-12-15 2007-10-31 Ishihara Sangyo Kaisha Compuestos benzoilpirazol y herbicidas que los contienen
UA94003C2 (uk) * 2006-11-28 2011-03-25 Ишихара Санджай Кайша, Лтд. Сполуки бензоїлпіразолу, гербіцид на їх основі та спосіб боротьби з небажаними рослинами
JP5420169B2 (ja) * 2006-12-27 2014-02-19 石原産業株式会社 ベンゾイルピラゾール系化合物を含有する除草剤
JP5416354B2 (ja) * 2007-02-02 2014-02-12 石原産業株式会社 ベンゾイルピラゾール系化合物を含有する除草性組成物
EP1980556A1 (de) 2007-04-12 2008-10-15 Bayer CropScience AG 4-(4-Trifluormethyl-3-thiobenzoyl)pyrazole und ihre Verwendung als Herbizide
DE102007026875A1 (de) 2007-06-11 2008-12-24 Bayer Cropscience Ag 3-Cyclopropyl-4-(3-thiobenzoyl)pyrazole und ihre Verwendung als Herbizide
JP5449855B2 (ja) * 2008-05-20 2014-03-19 石原産業株式会社 ピラゾール系化合物、それらの製造方法及びそれらを含有する除草剤
EP2127521A1 (de) 2008-05-29 2009-12-02 Bayer CropScience Aktiengesellschaft Herbizid wirksame 4-(3-Alkylsulfinylbenzoyl)pyrazole
JP5584452B2 (ja) * 2008-12-11 2014-09-03 石原産業株式会社 ベンゾイルピラゾール系化合物を含有する除草性組成物
EA201270088A1 (ru) * 2009-07-29 2012-09-28 Байер Кропсайенс Аг 4-(3-алкилтиобензоил)пиразолы и их применение в качестве гербицидов
CN102906096A (zh) 2010-03-23 2013-01-30 巴斯夫欧洲公司 具有除草作用的吡啶类
AU2011231819A1 (en) 2010-03-23 2012-10-18 Basf Se Pyridothiazines having herbicidal action
EP2550277A1 (de) 2010-03-23 2013-01-30 Basf Se Substituierte pyridazine mit herbizider wirkung
US20130065760A1 (en) 2010-03-23 2013-03-14 Basf Se Substituted Pyridines Having Herbicidal Action
US8575068B2 (en) 2010-03-23 2013-11-05 Basf Se Pyrazinothiazines having herbicidal action
AR081526A1 (es) 2010-03-23 2012-10-03 Basf Se Piridazinas sustituidas que tienen accion herbicida
MX2013000589A (es) 2010-07-21 2013-03-05 Bayer Ip Gmbh 4-(4-halogenoalquil-3-tiobenzoil) pirazoles y uso de los mismos como herbicidas.
UA108681C2 (uk) 2010-12-23 2015-05-25 Басф Се Заміщені піридини, що мають гербіцидну активність
CN103596959A (zh) 2011-06-09 2014-02-19 巴斯夫欧洲公司 具有除草活性的取代吡啶类
WO2012168241A1 (en) 2011-06-09 2012-12-13 Basf Se Substituted pyrazines having herbicidal activity
IN2014MN02343A (de) 2012-06-01 2015-08-14 Basf Se
US20160102103A1 (en) 2013-05-24 2016-04-14 Basf Se Substituted pyridine compounds having herbicidal activity
CN108264484A (zh) * 2016-12-30 2018-07-10 浙江省化工研究院有限公司 一种带醚结构的取代的苯基酮类化合物、其制备方法及应用

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JPS5436648B2 (de) * 1974-03-28 1979-11-10
FR2277826A2 (fr) * 1974-07-09 1976-02-06 Sandoz Sa Stabilisation de matieres organiques au moyen de derives de pyrazole
US4083925A (en) * 1976-03-22 1978-04-11 Martin Marietta Aluminum, Inc. Method for removing ferrous iron from alkali metal aluminate liquor
US4230481A (en) * 1977-08-12 1980-10-28 Ishihara Sangyo Kaisha Limited Pyrazole derivatives useful as a herbicidal component
JPS58185568A (ja) * 1982-04-24 1983-10-29 Nissan Chem Ind Ltd ピラゾ−ル誘導体，その製造方法および該誘導体を含有する選択性除草剤
US4744815A (en) * 1985-05-11 1988-05-17 Nissan Chemical Industries, Ltd. 4-benzoyl-1-alkyl (alkenyl) - pyrazoles, composition containing them, herbicidal method of using them, and intermediate in their preparation
US4643757A (en) * 1985-05-20 1987-02-17 Nissan Chemical Industries, Ltd. Herbicidal 4-benzoyl-1-methyl-5-hydroxypyrazoles
IL85659A (en) * 1987-03-17 1992-03-29 Nissan Chemical Ind Ltd 4-benzoylpyrazole derivatives,method for their preparation and herbicidal compositions containing them

Also Published As

Publication number Publication date
CA1338788C (en) 1996-12-10
HUT51256A (en) 1990-04-28
HU205912B (en) 1992-07-28
DK349289D0 (da) 1989-07-14
IL90819A (en) 1994-06-24
CN1039586A (zh) 1990-02-14
DE68918524T2 (de) 1995-05-04
KR0128286B1 (ko) 1998-04-02
US4986845A (en) 1991-01-22
AU618609B2 (en) 1992-01-02
CN1017240B (zh) 1992-07-01
RU2042667C1 (ru) 1995-08-27
ES2064388T3 (es) 1995-02-01
RU1792280C (ru) 1993-01-30
AU3800589A (en) 1990-01-25
DK170439B1 (da) 1995-09-04
EP0352543A1 (de) 1990-01-31
IL90819A0 (en) 1990-01-18
EP0352543B1 (de) 1994-09-28
USRE34779E (en) 1994-11-08
KR900001657A (ko) 1990-02-27
BR8903486A (pt) 1990-03-13
ATE112271T1 (de) 1994-10-15
DK349289A (da) 1990-01-16

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