CN1382034A - 含水粉末组合物及其制造方法和含该粉末组合物的化妆料 - Google Patents
含水粉末组合物及其制造方法和含该粉末组合物的化妆料 Download PDFInfo
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- CN1382034A CN1382034A CN00814777A CN00814777A CN1382034A CN 1382034 A CN1382034 A CN 1382034A CN 00814777 A CN00814777 A CN 00814777A CN 00814777 A CN00814777 A CN 00814777A CN 1382034 A CN1382034 A CN 1382034A
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- water
- containing powder
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- powder
- aqueous gel
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Abstract
把用疏水性粉体被覆水性凝胶的芯物质而构成的含水粉末组合物及水相成分通过水溶性凝胶化剂进行凝胶化后,制成粉末状的水性凝胶芯物质,然后,用疏水性粉体被覆该水性凝胶芯物质的上述含水粉末组合物的制造方法。本申请发明的组合物的特征是制造稳定性及保存稳定性优良、使用时用手指等施加压力时破裂放出水,是广泛用于化妆品、食品、香料、农药、医药等方面的含水粉末组合物。
Description
技术领域
本发明涉及将水粉末化的组合物。更详细地讲是涉及制造稳定性和保存稳定性优良，使用时通过用手指等施加压力而破裂、放出水的含水粉末组合物。该含水粉末组合物可广泛用于化妆品、食品、香料、农药、医药等方面。
背景技术
本发明人首先开发了作为制品的形态是粉末、使用时通过用手指等施加压力而破裂、放出水的含水粉末化妆料，并申请了专利(特开平5-65212号公报)。该含水粉末组合物是使用疏水二氧化硅和氟化合物处理粉末、根据将水及油粉末化的技术制得的。该疏水二氧化硅的疏水性存在离散，在稳定的制造及保存的稳定性方面有时存在问题。
因此，本发明者通过微胶囊化技术的应用，对是否可以稳定地制得具有上述性质的含水粉末化妆料进行了研究。
于是，已公开了用疏水性粉体包容水、进行微胶囊化的技术(特公平3-67737号等)、该方法是把水冷却固化后，粉碎使之冻结粉末化、然后用疏水性粉体对其被覆的技术。
然而，上述的微胶囊化技术存在以下问题：①将冻结的水粉碎时，粒径很难变细，②将冻结的水粉碎后到被覆表面之间，水(冰)粒子容易产生凝聚、合一，③被覆粉末化的水(冰)粒子的表面时，容易引起粒子的凝聚和合一等，很难获得具有实用性的微胶囊。
因此，谋求改进以往的微胶囊化技术、开发出在生产时没有上述之类的问题、使用时通过用手指施加压力而破裂、放出水的含水粉末组合物的技术。
发明内容
本发明人反复进行了可解决上述课题的研究的结果，发现用水溶性凝胶化剂把水相成分凝胶化后，再通过将其高速剪断和冻结粉碎等制成粉末状的水性凝胶芯物质，然后用疏水性粉体被覆该芯物质的表面，可得到细粒径的含水粉末，而且也不产生粒子的凝聚及合一的问题。另外，发现所得的含水粉末制造稳定性及保存稳定性优良、保持了在使用时用手指等施加压力时破裂而放出水的性质，从而完成了本发明。
即本发明是提供用疏由水性粉体被覆水性凝胶组成的芯物质所得到的含水粉末组合物。
另外，本发明提供含水粉末组合物的制造方法，其特征在于：用水溶性凝胶化剂把水相成分凝胶化后，通过高速剪断和冻结粉碎等制成粉末状的水性凝胶芯物质，然后用疏水性粉体被覆该水性凝胶芯物质。
又，本发明还提供含上述任一项记载的含水粉末组合物的化妆料又及使用它的皮肤的化妆方法。
实施发明的最佳方案
本发明的含水粉末组合物是具有用疏水性粉体被覆水性凝胶芯物质的外侧的结构的物质。该含水粉末组合物是用水溶性凝胶化剂把水相成分凝胶化后，通过高速剪断和冻结粉碎等制成粉末状的水性凝胶芯物质，然后用疏水性粉体被覆该粉体而制得的。
在本发明的含水粉末组合物中，其水的含有量在水性凝胶中优选约30～99.7质量％(以下仅简略为“％”)，更优选40～98％，在该范围内时，可更良好地感觉到水的清凉感。
所谓构成由该水性凝胶组成的芯物质的水相成分意味着具有水或亲水性的有效成分等。作为该有效成分可列举对羟基苯甲酸酯、苯氧基乙醇等防腐剂，1，3-丁二醇、二丙二醇、乙二醇、甘油、双甘油等保湿剂，乙醇、薄荷醇等清凉剂，表面活性剂，维生素C衍生物等药剂等。另外，作为水相成分，也可以用使油分在水中乳化分散的水中油型乳化物，或使粉体分散在水中或水中油型乳化物中的悬浊液。
另一方面，作为水溶性凝胶化剂，是通过在水中溶解或膨润而使水凝胶化的物质。例如，可列举琼脂、古柯豆胶、槐豆胶、温柏种子胶、フア-センラン(furcellaran)、角叉藻胶、海藻酸钠、ジエラン胶(gellan gum)、淀粉、果胶、魔芋等植物类天然高分子，明胶等动物类天然高分子，甲基纤维素，羟甲基纤维素、羟乙基纤维素、羟丙基纤维素、羧基甲基纤维素等纤维素衍生物等半合成高分子，聚乙烯醇、羧基乙烯基聚合物、烷基改性羧基乙烯基聚合物、聚丙烯酸钠、聚甲基丙烯酸钠、聚乙烯基吡咯烷酮等合成高分子，硅酸钠镁、含水硅酸铝、蒙脱石、皂石、锂蒙脱石、四氟硅云母等的水膨润性粘土矿物等，它们可用一种或不小于二种。它们的水溶性凝胶化剂，从高速剪断和冻结粉碎时容易粉碎和提高保存稳定性的观点考虑，优选如琼脂、明胶、角叉藻胶、ジエラン胶、硅酸钠镁那样与水形成硬凝胶的物质。
本发明所用的水溶性凝胶化剂的含量，为了使水相成分凝胶化，要有足够的量，它随水溶性凝胶化剂的种类而异，优选在水性凝胶中约为0.1～10％。
本发明所用的水溶性凝胶化剂，如羧基乙烯基聚合物、烷基改性羧基乙烯基聚合物等那样，为了使水凝胶化，需要耐碱时，例如可以用氢氧化钠、氢氧化钾、三乙醇胺、二乙醇胺等。此时，水溶性凝胶化剂与碱的比随水溶性高分子的种类而异，按质量比，优选使水溶性凝胶化剂与碱的比大体为1∶0.001～1∶1。
本发明中，作为使由水相成分与水溶性凝胶剂构成的水性凝胶成为粉末状的水性凝胶芯物质的方法，可列举进行高速剪断和冻结粉碎的方法等。作为高速剪断的方法可列举用高速针磨机及剪切混合机等的方法。而作为冻结粉碎的方法，可列举用液氮等冷媒冻结水性凝胶，粉碎该水性凝胶的方法。冻结粉碎水性凝胶的温度影响到水性凝胶的凝胶硬度和凝固点等，优选大约-20℃～190℃的范围，冻结粉碎后的粒径优选大约为1～30μm。
被覆这样制得的水性凝胶的粉末状粒子的疏水性粉体，通过粘附或吸附在水性凝胶的粉末状粒子的表面，从而具有防止凝聚和提高保存稳定性的作用。作为这种疏水性粉体，可以用粉体本身是疏水性的粉体，或用通常公知的疏水剂对亲水性粉体进行表面处理的粉体，或为了进一步提高疏水性而用疏水剂对疏水性粉体再处理的粉体等。该疏水性粉体的粒径必须小于水性凝胶的粉末状粒子的粒径，而从对表面的被覆效率的观点考虑，更优选为不大于水性凝胶粉末状粒子的粒径的1/10。
本发明所用的疏水性粉体中，粉体自身作为疏水性的粉体，例如，可举出聚苯乙烯粉末、聚乙烯粉末、聚有机硅氧烷弹性体粉末、聚甲基倍半硅氧烷粉末、N-酰基赖氨酸、聚四氟乙烯树脂粉末、丙烯酸树脂粉末、环氧树脂粉末、尼龙粉末、硬脂酸铝、月桂酸锌、硬脂酸镁等，可使用它们的一种或不小于二种。
另外，也可以使用用疏水剂对亲水性粉体进行了表面处理的疏水性粉末，作为此情况所用的疏水剂，可列举三甲基硅烷基化剂、甲基氢二烯聚硅氧烷等有机硅化合物，全氟聚醚烷基磷酸、全氟烷基硅烷等氟化合物、金属皂、油剂等，可以使用它们的一种或不小于二种，其中如果是有机硅化合物或氟化合物，则由于进一步提高了疏水性，所以是理想的。此外，作为亲水性粉体，例如可列举氧化钛、氧化锌、二氧化硅、氧化铝、氧化镁、氧化锆、碳酸镁、碳酸钙、硅酸铝、硅酸镁、硅酸铝镁、云母、合成云母、合成绢云母、绢云母、滑石、碳化硅、硫酸钡、氮化硼、氯酸铋，云母钛等无机粉体类，蚕丝粉、淀粉、结晶纤维素等有机粉体类，细粒子氧化钛被覆云母钛、细粒子氧化锌被覆云母钛、硫酸钡被覆云母钛等复合粉体等。这些用疏水剂进行表面处理的亲水性粉体，也可以使用一种或将不小于二种组合使用。
上面所示的疏水性粉体中，保存稳定性效果更高的是把平均粒径0.001～0.1μm的烟雾状二氧化硅进行疏水化处理的粉体，使用这种粉体特别理想。这样的疏水性粉体是作为AEROSILR 974、R972、RX200、RX 300(均是日本アエロジル公司制)、キャボジル TS-530(キャボツト公司制)等市售的产品。另外，本发明的含水粉末组合物中，水性凝胶的粉末状物与疏水性粉体的比例会影响到疏水性粉体的粒径和水性凝胶的粉末状物的粒径等，按质量比大约为100∶0.5～100∶25是更优选的。
本发明中，在水性凝胶的粉末状物表面被覆疏水性粉体的方法没有特殊限制，例如，可列举在搅拌机中加入疏水性粉末，在随温度的上升而不引起熔解、凝聚的低温下，一边搅拌一边添加水性凝胶的粉末状物，从而混合搅拌进行被覆的方法。另外，进行混合的搅拌机器最好是安装具有冷却机构的水套，在水套内的壁面和底面安装撞击·接触少的形状的搅拌叶的搅拌机。
在本发明的化妆料中，前述含水粉末组合物的含有量优选为10～100％，更优选30～90％。在该范围内使用时，可得到水灵程度和，清凉感等在化妆料中配合水的效果特别优良的化妆料。
在含有本发明含水粉末组合物的化妆料中，除了上述含水粉末组合物外，在不损害本发明效果的范围，还可配合通常化妆料中广泛使用的粉末、油剂、表面活性剂、部分交联型聚有机硅氧烷和糊精脂肪酸酯等油凝胶化剂，紫外线吸收剂、丙烯酸改性聚硅氧烷和三甲基甲硅烷氧基硅酸等油溶性被膜形成剂，乙醇等溶剂，对羟基苯甲酸衍生物、苯氧基乙醇等防腐剂，维生素类、消炎剂、抗氧化剂、螯合剂、维生素C衍生物等药剂，二醇类等保湿剂，水、水溶性高分子、多元醇、清凉剂、香料等成分。
其中，可配合到本发明的化妆料中的粉体，是通常化妆料中以着色效果、化妆效果、紫外线遮蔽效果、触感调整效果等为目的而配合的粉体，对粒子的形状、大小、结构等没有特殊限制，可列举无机粉体类、光亮性粉体类、有机粉体类、染料粉体类、复合粉体类等，可以使用它们的一种或不小于二种。具体地说，可列举氧化钛、普鲁士蓝、群青、红色氧化铁、黄色氧化铁、黑色氧化铁、氧化锌、氧化铝、二氧化硅、氧化镁、氧化锆、碳酸镁、碳酸钙、氧化铬、氢氧化铬、碳黑、硅酸铝、硅酸镁、硅酸铝镁、云母、合成云母、合成绢云母、绢云母、滑石、高岭土、碳化硅、硫酸钡、膨润土、蒙脱石、氮化硼等无机粉体类，氯酸铋、云母钛、氧化铁被覆云母、氧化铁云母钛、有机颜料处理云母钛、铝粉等的光亮性粉体类，尼龙粉，聚甲基丙烯酸甲酯、丙烯腈-甲基丙烯酸共聚物粉、偏氯乙烯-甲基丙烯酸共聚物粉、聚乙烯粉、聚苯乙烯粉、聚有机硅氧烷弹性体粉、聚甲基倍半硅氧烷粉、聚四氟乙烯粉、羊毛粉、蚕丝粉、结晶纤维素、硬脂酸镁、硬脂酸锌、N-酰基赖氨酸等有机粉体类，有机焦油系颜料、有机染料的色淀颜料等染料粉体类，微粒氧化钛被覆云母钛、微粒氧化锌被覆云母钛、硫酸钡被覆云母钛、含氧化钛的二氧化硅、含氧化锌的二氧化硅等的复合粉体等，可以使用它们的一种或二种。
作为上述粉体，也可以使用将其一种或不小于二种进行复合化的粉体，还可以是使用氟化合物、有机硅系油剂、金属皂、蜡、表面活性剂、油脂、烃等，通过公知的方法进行表面处理的粉体。这些粉体在本发明化妆料中的配合量会影响到粉体的配合目的、化妆料的剂型等，优选为大约1～90％。
另外，可配合到本发明的化妆料中的油剂，是在通常的化妆料中作为提高对皮肤的粘附性、赋予润滑感、提高化妆持久性等目的而配合的油剂，不论动物油、植物油、合成油等的起源及固体油、半固体油、液体油、挥发性油等的性状，可列举烃类、油脂类、蜡类、固化油类、酯油类、脂肪酸类、高级醇类、有机硅油类、氟系油类、含水羊毛脂衍生物类等油剂。具体地说，可列举石蜡、丝胶蛋白蜡、天然地蜡、微晶蜡、木蜡、褐煤蜡、鱼雷蜡、聚乙烯蜡、液体石蜡、凡士林、三十碳烷等烃类、巴西棕榈蜡、蜂蜡、含水羊毛脂蜡、小烛树蜡等天然物质，山嵛酸甘油酯、玫瑰酸季戊四醇酯、肉豆蔻酸异丙酯、碳酸二烷酯、三辛酸甘油酯、三异硬脂酸双甘油酯等酯类，硬脂酰硅氧烷等烷基改性聚硅氧烷类，硬脂酸，1，2-羟基硬脂酸、山嵛酸、油酸等脂肪酸类、鲸蜡醇、硬脂醇、山嵛醇等高级醇类，橄榄油、蓖麻油、霍霍巴油、水貂油等油脂类，含水羊毛脂脂肪酸异丙酯、含水羊毛脂醇等含水羊毛脂衍生物，二甲基聚硅氧烷、甲基苯基聚硅氧烷等的有机硅油，十甲基环戊硅氧烷、八甲基环四硅氧烷等环状聚硅氧烷类，聚烯化氧改性或烷基改性有机硅油，全氟癸烯、全氟辛烯等氟系油类等，可以使用它们的一种或二种。
本发明的化妆料中，配合这些油剂时的配合量会影响到油剂的配合目的、化妆料的剂型等，优选大约为0.1～50％。
含有本发明的含水粉末组合物的化妆料没有特殊限制，可列举眼脂、粉底霜、胭脂、白粉等美容化妆料、爽身粉、抗汗粉、美白粉、乳液、霜、美容液等的护肤化妆料、防晒化妆料。
以上说明的本发明化妆料，在使用时通过用手指或手掌，或用海绵或球棒等小工具涂擦，使化妆料中所含的含水粉末组合物破裂，放出水性成分，可得到具有清凉感和成膜性等特征的使用感。
本发明的含水粉末组合物是制造稳定性、长期保存稳定性优良，通过用手指或手掌、或用海绵或球棒等小工具涂擦，容易破裂、放出水性成分的物质。配合有本发明的含水粉末组合物的化妆料，其外观是粉末及固体状，如上所述，因为使用时容易破裂、放出水性成分，所以具有以往技术不能得到的清凉感、成膜性等特征。另外，本发明的含水粉末组合物除化妆品外，在食品、香料、农药、医药等广泛领域可有效地被利用。
实施例
以下，列举实施例更详细地说明本发明，当然，本发明并不受这些实施例限制。
实施例1
含水粉末组合物：
按表1所示的组成，用下述制造方法调制含水粉末组合物。对所得的含水粉末组合物，用以下所示的评价方法，评价“制造稳定性”、“保存稳定性”、“用手指施加压力时(使用时)的易破性”。结果示于表2。
(配合组成)：见表1
表1 (质量％)
| 本发明品 | 比较品 | |
| 1 2 3 4 5 6 7 | 1 | |
| 1.精制水2.琼脂3.明胶4.角叉藻胶5.淀粉6.羧基乙烯基聚合物7.硅酸钠镁[注1]8.烷基改性羧基乙烯基聚合物[注2]9.甘油10.1，3-丁二醇11.防腐剂12.三乙醇胺13.液体石蜡14.滑石15.大豆磷脂质16.香料 17.疏水处理二氧化硅[注3]18.疏水处理二氧化硅[注4] | 余量 余量 余量 余量 余量 余量 余量0.2 2 2 - - - 1- - - 3 - - -- - - - 0.05 0.05 -- - - 0.2 - - -- - - - 0.7 - -- - - - - - 10- - - - - 0.5 -2 2 2 2 2 2 210 10 10 10 10 10 10适量 适量 适量 适量 适量 适量 适量- - - - 0.7 0.5 -- - - - - 5 -- - - - 3 - -- - - - 0.3 - -适量 适量 适量 适量 适量 适量 适量3 3 25 - - - -- - - 3 3 3 3 | 余量-------210适量----适量-3 |
注1：ラポナイトXLG(ラポナイト公司制)
注2：カ-ボポ-ル1342(グッド リツチ化学公司制)
注3：AEROSIL R972(二甲基二氯硅烷处理的二氧化硅/日本アエロジル公司制)
注4：AEROSIL RX300(六甲基二硅氨烷处理的二氧化硅/日本アエロジル公司制)(制造方法)A.把成分1～12混合溶解(或膨润)。B.在A中添加成分13～16，进行混合分散。C.用液氮把B冷却到-80℃，进行冻结粉碎后，得到粒径约80μm的水性凝胶的粉末状物。D.在混合搅拌机中一边搅拌成分17或成分18，一边添加C，混合得到含水粉末组合物。(评价方法)制造稳定性：
用以下标准评价在同一条件下生产5次含水粉末组合物时的粒径的离散。
评价：内容
◎ 完全均匀没有离散
○ 略有离散、大致均匀
△ 有离散
× 有很大离散保存稳定性：
用以下标准评价将各含水粉末组合物在40℃保存6个月的状态。
评价：内容
◎ 保存后的外观没有变化
○ 可稍微看到保存后的粉末的合一
△ 可看到保存后的粒子的合一
× 可看到保存后的水的分离用手指施加压力时(使用时)的易破性
用下述标准评价用手指压破各含水粉末组合物时的水的放出状态。
评价：内容
◎ 用手指压立即破裂、放出水。
○ 略难破裂、放出水
△ 用手指压难破裂、放出水
× 用手指压难破裂、难放出水
(结果)：见表2
表2
| 本发明品 | 比较品 | |||||||
| 1 | 2 | 3 | 4 | 5 | 6 | 7 | 1 | |
| 制造稳定性 | ○ | ◎ | ○ | ◎ | ○ | ○ | ○ | △ |
| 保存稳定性 | ○ | ◎ | ◎ | ◎ | ○ | ○ | ○ | × |
| 使用时的易破性 | ○ | ◎ | ○ | ◎ | ○ | ○ | ○ | ○ |
由表2的结果表明，本发明品1～7的含水粉末组合物与比较例相比，是“制造稳定性”、“保存稳定性”、“用手指压时(使用时)的易破性”均优良的含水粉末组合物。
实施例2
含水粉末组合物：
按照下述的组成及制法，调制含水粉末组合物。同实施例1一样，对所制得的含水粉末组合物，评价“制造稳定性”、“保存稳定性”、“用手指压时(使用时)的易破性”的结果，任一项评价均是◎。
(配合组成) 质量％
1.精制水 余量
2.琼脂 1
3.硅酸钠镁[注1] 5
4.甘油 2
5.1，3-丁二醇 10
6.防腐剂 适量
7.三乙醇胺 1
8.硬脂酸 2
9.单硬脂酸甘油酯 1
10.鲸蜡醇 1
11.二甲基聚硅氧烷 1
12.液体石蜡 5
13.对甲氧基肉桂酸2-乙基己酯 1
14.倍半油酸山梨糖醇酐 0.5
15.单油酸聚氧乙烯梨糖醇酐 0.5
16.尼龙粉末 1
17.香料 适量
18.疏水处理的二氧化硅2[注4] 3(制造方法)A.把成分1～7混合溶解(或膨润)。B.加热溶解成分8～15，添加到A中进行乳化。C.添加成分16～17，进行混合分散。D.用液氮把C冷却到-120℃，进行冻结粉碎得到粒径约80μm的水性凝胶的粉末状物。E.在混合搅拌机中一边搅拌成分18，一边添加D，混合后得含水粉末组合物。
实施例3
除臭粉：
(配合组成) 质量％
1.羟基氯化铝 20
2.精制水 余量
3.琼脂 3
4.丙二醇 5
5.聚氧乙烯(20mol)油醚 0.5
6.乙醇 5
7.氯化亚苄基毒芹 0.2
8.香料 0.3
9.疏水处理的二氧化硅2注4) 5
(制造方法)A.把1～4混合溶解。B.把5～8混合溶解。C.在A中添加B，进行可溶化。D.用高速亨舍尔混合机(三井三池化工机械公司制)将C粉末化。E.一边混合9，一边在其中添加D，制得除臭粉。
实施例4
果酒粉
(配合组成) 质量％
1.精制水 10
2.琼脂 1
3.果酒 86
4.硬脂酸镁处理的二氧化硅 3
(制造方法)A.把1～2加热溶解、添加3进行混合。B.把A冷却到-80～100°后，进行冻结粉碎。C.一边混合4一边向其中添加B得到果酒粉。制剂例1
含水粉末状化妆料(粉底霜)
(配合组成) 质量％
1.氟化合物处理的氧化钛注5) 5
2.氟化合物处理的红色氧化铁注5) 0.1
3.氟化合物处理的黄色氧化铁注5) 1
4.氟化合物处理的黑色氧化铁注5) 0.05
5.有机硅处理的绢云母注6) 余量
6.有机硅处理的滑石注6) 10
7.实施例1的含水粉末组合物 70
注5：5％全氟烷基磷酸盐处理的粉体
注6：3％甲基氢二烯聚硅氧烷处理的粉体。制剂例2
含水粉末化妆料(睑黛)
(配合成分) 质量％
1.实施例1的含水粉末组合物 余量
2.部分交联型聚有机硅氧烷膨润物注8) 2
3.二甲基聚硅氧烷 1
4.有机硅处理的二氧化硅注6) 5
5.有机硅处理的红色202号注6) 0.3
6.黄色氧化铁 1
7.氟化合物处理的云母钛注5) 5
8.金属皂处理的滑石注9) 10
9.氧化钛 1
10.防腐剂 适量
注8：硅KSG-18(信越化学工业公司制)
注9：3％月桂酸锌处理的粉体制剂例3
含水粉末化妆料(美容液)：
(配合成分) 质量％
1.实施例2的含水粉末组合物 余量
2.蔗糖脂肪酸酯 1
3.二丙二醇 1
4.聚苯乙烯粉 3
5.防腐剂 适量制剂例4
含水粉末化妆料(美白粉)：
(配合成分) 质量％
1.实施例1的含水组合物 余量
2.抗坏血酸磷酸酯镁 1
3.抗坏血酸磷酸酯钠 1
4.双甘油 0.5
5.加氢大豆磷脂 1
6.三十碳烷 2
7.糊精脂肪酸酯 0.3
8.氟化合物处理的尼龙粉注5) 3
9.香料 适量
10.防腐剂 适量
注5：5％全氟烷基磷酸盐处理的粉体制剂例5
含水粉末化妆料(防晒化妆料)：
(配合成分) 质量％
1.实施例2的含水粉末化妆料 余量
2.氟化合物处理的细粒子氧化钛注5) 2
3.有机硅处理的细粒子氧化锌注6) 1
4.2-乙基己酸三甘油酯 1
5.4-叔丁基-4’-甲氧基二苯甲酰甲烷 0.05
6.聚丙烯酸烷基酯粉 5
7.香料 适量
8.防腐剂 适量
注5.5％全氟烷基磷酸盐处理的粉体
注6：3％甲基氢二烯聚硅氧烷处理的粉体制剂例6
含水粉末化妆料(爽身粉)
(配合成分) 质量％
1.实施例3的含水粉末化妆料 余量
2.1-薄荷醇 0.05
3.莰烷 0.05
4.乙醇 2
5.二氧化硅 10
6.防腐剂 适量
Claims (9)
1.一种含水粉末组合物，其特征是：用疏水性粉体被覆由水性凝胶组成的芯物质而成的。
2.权利要求1记载的含水粉末组合物，其特征是：由水性凝胶组成的芯物质是采用水溶性凝胶化剂把水相成分凝胶化后进行冻结粉碎而制得的。
3.权利要求1或2记载的含水粉末组合物，其特征是：疏水性粉体的粒径不大于由水性凝胶组成的芯物质的粒径的1/10。
4.权利要求1～3的任一项记载的含水粉末组合物，其特征是：水溶性凝胶化剂是从琼脂、明胶、角叉藻胶、ジエラン胶或硅酸钠镁中选出的一种或不少于二种。
5.权利要求1～4的任一项记载的含水粉末组合物，其特征是：采用水溶性凝胶化剂把水相成分凝胶化后，进行冻结粉碎制成粉末状的水性凝胶芯物质，然后用疏水性粉体被覆该水性凝胶芯物质。
6.一种含水粉末组合物的制造方法，其特征是：采用水溶性凝胶化剂把水相成分凝胶化后，制成粉末状的水性凝胶芯物质，然后用疏水性粉体被覆该水性凝胶芯物质。
7.权利要求6记载的含水粉末组合物的制造方法，其特征是：通过把采用水溶性凝胶化剂凝胶化的水相成分冻结粉碎而制成粉末状的水性凝胶芯物质。
8.一种化妆料，其特征是：含上述权利要求1～5的任一项记载的含水粉末组合物。
9.一种皮肤的化妆方法，其特征是：把上述权利要求8记载的化妆料涂在要化妆的皮肤上，对其施加压力，使水分从该组合物中放出。
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP237149/99 | 1999-08-24 | ||
| JP23714999 | 1999-08-24 | ||
| JP237149/1999 | 1999-08-24 | ||
| JP172172/2000 | 2000-06-08 | ||
| JP2000172172A JP4514902B2 (ja) | 1999-08-24 | 2000-06-08 | 含水粉末組成物及びその製造法並びに当該粉末組成物を含有する化粧料 |
| JP172172/00 | 2000-06-08 |
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| Publication Number | Publication Date |
|---|---|
| CN1382034A true CN1382034A (zh) | 2002-11-27 |
| CN1170517C CN1170517C (zh) | 2004-10-13 |
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| Country | Link |
|---|---|
| EP (1) | EP1206928B1 (zh) |
| JP (1) | JP4514902B2 (zh) |
| KR (1) | KR100718604B1 (zh) |
| CN (1) | CN1170517C (zh) |
| AT (1) | ATE526059T1 (zh) |
| HK (1) | HK1049963B (zh) |
| TW (1) | TW592712B (zh) |
| WO (1) | WO2001013864A1 (zh) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100335023C (zh) * | 2003-04-28 | 2007-09-05 | 莱雅公司 | 含有皮脂吸收粉剂和低临界表面能粉剂的化妆品组合物 |
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| CN101500699B (zh) * | 2006-08-08 | 2013-08-21 | 宝洁公司 | 制备可崩解含水胶囊的方法 |
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| JP3854522B2 (ja) * | 2002-03-25 | 2006-12-06 | 株式会社コーセー | メーキャップ化粧料 |
| FR2844448B1 (fr) | 2002-09-17 | 2006-06-23 | Lcw Les Colorants Wackherr | Methode de preparation extemporanee de compositions cosmetiques ayant la texture d'une creme, et compositions pour la mise en oeuvre de cette methode |
| FR2848419B1 (fr) * | 2002-12-13 | 2006-08-04 | Oreal | Composition cosmetique comprenant une matiere pigmentaire dispersee dans un gel aqueux, cette matiere pigmentaire etant constituee d'une charge liee physiquement ou chimiquement a un pigment |
| KR100863233B1 (ko) * | 2003-09-13 | 2008-10-15 | 이경록 | 기능성 워터인 파우더 화장료 조성물 |
| FR2860435B1 (fr) * | 2003-10-07 | 2008-08-01 | Cosmetic Lab Concepts C L C | Poudre d'eau a base de silice hydrophobe |
| WO2005058256A1 (de) * | 2003-12-01 | 2005-06-30 | Degussa Ag | Verstreichbare kosmetische zubereitung mit hohem wassergehalt |
| JP4808456B2 (ja) * | 2004-09-27 | 2011-11-02 | 株式会社コーセー | 粉末状化粧料 |
| US7341743B2 (en) | 2004-10-28 | 2008-03-11 | Revlon Consumer Products Corporation | Color cosmetic compositions |
| DE102004056862A1 (de) * | 2004-11-25 | 2006-06-14 | Degussa Ag | Pulverförmige, kosmetische Zubereitung mit hohem Wassergehalt |
| DE102005055226A1 (de) * | 2004-12-24 | 2006-07-13 | Degussa Ag | Lagerung pulverförmiger Stoffe mit hohem Wassergehalt |
| JP5128937B2 (ja) * | 2005-03-25 | 2013-01-23 | 株式会社コーセー | 含水粉末化粧料 |
| FR2890557B1 (fr) * | 2005-09-14 | 2012-07-13 | Oreal | Composition cosmetique comprenant un actif et des particules contenant au moins un pigment inorganique colore dans une matrice, et utilisation en soin de peau. |
| US20080038301A1 (en) * | 2006-08-08 | 2008-02-14 | The Procter & Gamble Company | Personal care product comprising collapsible water-containing capsules |
| JP5663778B2 (ja) * | 2007-07-06 | 2015-02-04 | 中村 憲司 | 結晶性複合粉末及びその製造方法 |
| KR100904552B1 (ko) * | 2007-12-27 | 2009-06-25 | 주식회사보광화학 | 피부처짐 개선용 화장료 조성물 |
| JP5519706B2 (ja) | 2009-02-06 | 2014-06-11 | ザ プロクター アンド ギャンブル カンパニー | 崩壊性水含有カプセル |
| CA2750411C (en) | 2009-02-06 | 2014-01-14 | The Procter & Gamble Company | Collapsible water-containing capsules |
| DE102009002267A1 (de) * | 2009-04-07 | 2010-10-14 | Henkel Ag & Co. Kgaa | Pulverförmige Zusammensetzung zur Form- und Glanzgebung keratinischer Fasern |
| US8933134B2 (en) | 2010-06-09 | 2015-01-13 | L'oreal | Compositions containing agar and a softening agent |
| DE102011077298A1 (de) | 2011-06-09 | 2012-12-13 | Evonik Degussa Gmbh | Kern-Hülle-Partikel mit einem hohen Gehalt an Glycerin, ihre Herstellung und Verwendung |
| WO2014099946A1 (en) * | 2012-12-19 | 2014-06-26 | Johnson & Johnson Consumer Companies, Inc. | Anhydrous powder-to-liquid particles |
| WO2015055494A1 (en) * | 2013-10-15 | 2015-04-23 | Unilever N.V. | Cosmetic composition with increased opacity |
| WO2015055416A1 (en) * | 2013-10-15 | 2015-04-23 | Unilever N.V. | Cosmetic composition with increased opacity |
| BR112016029317A2 (pt) | 2014-06-16 | 2017-08-22 | Johnson & Johnson Consumer Inc | composições e métodos para melhorar a aplicação tópica de um cosmético colorido |
| JP2020158457A (ja) * | 2019-03-27 | 2020-10-01 | 株式会社ナリス化粧品 | 粉末化粧料 |
| JP7267159B2 (ja) * | 2019-09-12 | 2023-05-01 | 三井金属鉱業株式会社 | 表面処理酸化亜鉛粒子及び塗布用組成物 |
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| US3242051A (en) * | 1958-12-22 | 1966-03-22 | Ncr Co | Coating by phase separation |
| FR1334917A (fr) * | 1958-12-22 | 1963-08-16 | Upjohn Co | Procédé d'enduction de matières hydrophiles liquides et solides |
| US3405071A (en) | 1963-12-30 | 1968-10-08 | Ibm | Process of making microcapsules |
| JPS5855813B2 (ja) * | 1978-02-04 | 1983-12-12 | ぺんてる株式会社 | マイクロカプセルとその製造方法 |
| JPS5946124A (ja) * | 1982-09-07 | 1984-03-15 | Nippon Sanso Kk | マイクロカプセルの製造法 |
| JPS5946125A (ja) * | 1982-09-07 | 1984-03-15 | Nippon Sanso Kk | マイクロカプセルの製造法 |
| JP2891262B2 (ja) * | 1990-01-10 | 1999-05-17 | 松本油脂製薬株式会社 | 化粧料 |
-
2000
- 2000-06-08 JP JP2000172172A patent/JP4514902B2/ja not_active Expired - Lifetime
- 2000-08-17 EP EP00953468A patent/EP1206928B1/en not_active Expired - Lifetime
- 2000-08-17 WO PCT/JP2000/005510 patent/WO2001013864A1/ja active Application Filing
- 2000-08-17 KR KR1020027002327A patent/KR100718604B1/ko active IP Right Grant
- 2000-08-17 CN CNB008147779A patent/CN1170517C/zh not_active Expired - Lifetime
- 2000-08-17 AT AT00953468T patent/ATE526059T1/de not_active IP Right Cessation
- 2000-08-24 TW TW089117123A patent/TW592712B/zh not_active IP Right Cessation
-
2003
- 2003-03-24 HK HK03102125.1A patent/HK1049963B/zh not_active IP Right Cessation
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100335023C (zh) * | 2003-04-28 | 2007-09-05 | 莱雅公司 | 含有皮脂吸收粉剂和低临界表面能粉剂的化妆品组合物 |
| CN101500699B (zh) * | 2006-08-08 | 2013-08-21 | 宝洁公司 | 制备可崩解含水胶囊的方法 |
| CN102686207A (zh) * | 2009-12-26 | 2012-09-19 | 赢创德固赛有限公司 | 含水的粉状组合物 |
| US8647653B2 (en) | 2009-12-26 | 2014-02-11 | Evonik Degussa Gmbh | Water containing powder composition |
| CN102686207B (zh) * | 2009-12-26 | 2014-05-28 | 赢创德固赛有限公司 | 含水的粉状组合物 |
| CN101953765A (zh) * | 2010-09-10 | 2011-01-26 | 浙江省农业科学院 | 一种蚕丝爽身粉及其制备工艺 |
| CN101953765B (zh) * | 2010-09-10 | 2011-09-07 | 浙江省农业科学院 | 一种蚕丝爽身粉及其制备工艺 |
Also Published As
| Publication number | Publication date |
|---|---|
| ATE526059T1 (de) | 2011-10-15 |
| JP4514902B2 (ja) | 2010-07-28 |
| CN1170517C (zh) | 2004-10-13 |
| EP1206928A4 (en) | 2004-06-02 |
| KR100718604B1 (ko) | 2007-05-16 |
| TW592712B (en) | 2004-06-21 |
| HK1049963B (zh) | 2005-05-20 |
| KR20020060164A (ko) | 2002-07-16 |
| EP1206928A1 (en) | 2002-05-22 |
| WO2001013864A1 (fr) | 2001-03-01 |
| JP2001131528A (ja) | 2001-05-15 |
| EP1206928B1 (en) | 2011-09-28 |
| HK1049963A1 (en) | 2003-06-06 |
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