CN1257950A - Polypropylene spinning oil and preparation method thereof - Google Patents
Polypropylene spinning oil and preparation method thereof Download PDFInfo
- Publication number
- CN1257950A CN1257950A CN 99124278 CN99124278A CN1257950A CN 1257950 A CN1257950 A CN 1257950A CN 99124278 CN99124278 CN 99124278 CN 99124278 A CN99124278 A CN 99124278A CN 1257950 A CN1257950 A CN 1257950A
- Authority
- CN
- China
- Prior art keywords
- oil
- polypropylene fiber
- polyoxyethylene ether
- fiber spinning
- agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- -1 Polypropylene Polymers 0.000 title claims abstract description 43
- 238000009987 spinning Methods 0.000 title claims abstract description 23
- 239000004743 Polypropylene Substances 0.000 title claims abstract description 21
- 229920001155 polypropylene Polymers 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title 1
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 29
- 239000000654 additive Substances 0.000 claims abstract description 14
- 230000000996 additive effect Effects 0.000 claims abstract description 14
- 239000002270 dispersing agent Substances 0.000 claims abstract description 14
- 238000004519 manufacturing process Methods 0.000 claims abstract description 11
- 239000000835 fiber Substances 0.000 claims description 28
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 18
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 18
- 239000003921 oil Substances 0.000 claims description 15
- 239000002202 Polyethylene glycol Substances 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 229920001223 polyethylene glycol Polymers 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 10
- 239000004359 castor oil Substances 0.000 claims description 9
- 235000019438 castor oil Nutrition 0.000 claims description 9
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 9
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 150000002148 esters Chemical class 0.000 claims description 8
- 229910019142 PO4 Inorganic materials 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 7
- 239000010452 phosphate Substances 0.000 claims description 7
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 claims description 6
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 5
- 239000001103 potassium chloride Substances 0.000 claims description 5
- 235000011164 potassium chloride Nutrition 0.000 claims description 5
- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 150000004665 fatty acids Chemical class 0.000 claims description 4
- 229940070765 laurate Drugs 0.000 claims description 4
- 239000002480 mineral oil Substances 0.000 claims description 4
- 235000010446 mineral oil Nutrition 0.000 claims description 4
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 3
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 3
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 3
- 239000005642 Oleic acid Substances 0.000 claims description 3
- ZRIUUUJAJJNDSS-UHFFFAOYSA-N ammonium phosphates Chemical compound [NH4+].[NH4+].[NH4+].[O-]P([O-])([O-])=O ZRIUUUJAJJNDSS-UHFFFAOYSA-N 0.000 claims description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 3
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims description 3
- 229920000570 polyether Polymers 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 229920002545 silicone oil Polymers 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 238000005259 measurement Methods 0.000 claims description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N n-octadecyl alcohol Natural products CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 2
- 238000009499 grossing Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 4
- 239000012209 synthetic fiber Substances 0.000 description 4
- 229920002994 synthetic fiber Polymers 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 241000676840 Elater Species 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000007380 fibre production Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
A polypropylene spinning oil agent and a manufacturing method thereof are disclosed, wherein the weight percentage of each component is 65-75% of a smoothing agent, 2-8% of a dispersing agent, 15-25% of a bundling agent and 2-8% of an additive.
Description
The present invention relates to a kind of polypropylene fiber spinning oil and manufacture method thereof, belong to the auxiliary agent manufacturing technology field in the synthetic fiber process technology.
As everyone knows; the special protective layer of processing because synthetic fiber do not have surface of natural fibers to have like that to be suitable for to weave; therefore; in order to guarantee that synthetic fiber carry out spinning under certain condition smoothly; improve the quality of fibre property and silk; and the value of raising fibre, in spinning process, must use finish.Existing synthetic fiber finish because it constitutes the difference of component, is prone to lousiness, broken end phenomenon in the spinning application process, cause coiling and molding poor, and the high-class product rate is low, and corrosion phenomenon is serious, is difficult to adapt to the user demand of polypropylene spinning technology.
The purpose of this invention is to provide a kind of stable performance, good spinnability can satisfy the requirement of polypropylene fiber spinning technique, effectively improves the polypropylene fiber spinning oil and the manufacture method thereof of polypropylene spinning quality.
The present invention is a polypropylene fiber spinning oil, mainly by smooth agent, and dispersant, collecting agent, compositions such as additive is characterized in that the percentage by weight of each component is: smooth agent 65～75%, dispersant 2～8%, collecting agent 15～25%, additive 2～8%.
Described smooth agent can be mineral oil, double base alcohol ester, triol ester, quaternary alcohol ester, the mixture of one or more in the fatty acid polyethylene glycol ester.The effect of smooth agent can keep between fiber and the fiber, the suitable coefficient of friction between fiber and other contact components, improves level and smooth performance, helps carrying out smoothly of spin-drawing.
Described dispersant can be castor oil polyoxyethylene ether, lauryl alcohol polyoxyethylene ether, the mixture of one or more in the polyoxyethylene nonylphenol ether.The effect of dispersant is the various components in the finish are uniformly dispersed, and makes finish become even, transparent, stable oily solution in use.
Described collecting agent can be the polyethylene glycol Glycol Oleic Acid Ester, polyethylene glycol laurate dibasic acid esters, castor oil polyoxyethylene ether, the mixture of one or more in the octanol high-molecular weight atactic polyethers.The adding of collecting agent can improve the convergence and the flatness of finish, makes fiber not fluffy, at random in process, and fiber is played the obvolvent effect.
Described additive can be silicone oil, modified organic silicon, higher alcohol, higher acid, lauryl alcohol phosphate polyoxyethylene ether sylvite, hexadecanol phosphate kalium salt, the octadecanol phosphate kalium salt, lauryl alcohol polyoxyethylene ether phosphate sylvite, the mixture of one or more in the amphoteric phosphate ammonium salt.The adding of additive can guarantee the use and the bin stability of finish, reduces the finish surface tension, improves stability of emulsion.
The manufacture method of polypropylene fiber spinning oil of the present invention can be: the percentage by weight of pressing each component, elder generation is with collecting agent, the dispersant suction reactor of accurate measurement, being heated to 40-80 ℃ stirs, again with in the smooth agent suction reactor, after stirring 30-50min, add additive, the back cooling stirs, filter packing.
The present invention compared with prior art has following distinguishing feature and good effect:
1, this product oils uniform and stablely, can guarantee that fiber has convergence preferably;
2, film strength height makes fiber antistatic behaviour, flatness, flexibility after oiling all good, to guarantee carrying out smoothly of fiber production;
3, strong, the polypropylene spinning equipment that can adapt to different model of tack;
4, convergence is better, is specially adapted to add the processing of elater;
Oil for polypropylene fibre of the present invention is applicable to 68D-900D polypropylene fibre multifilament, and the production of textured filament and shaped filaments is used through the Duo Jia chemical fibre factory, and spinning, the production that stretches run well, and the fiber quality index reaches customer requirements.
Below in conjunction with embodiment the present invention is further described:
By weight percentage, determine the ratio of each component:
Embodiment 1:
Dispersant 5%, wherein castor oil polyoxyethylene ether (EL class) 1%, polyoxyethylene nonylphenol ether (TX class) 4%;
Collecting agent 20%, octanol high-molecular weight atactic polyethers 8% wherein, castor oil polyoxyethylene ether 12%;
Smooth agent 70%, its mineral oil in fluid 20%, quaternary alcohol ester 40%, fatty acid polyethylene glycol ester 10%;
Additive 5%, wherein silicone oil 3%, hexadecanol phosphate kalium salt 2%.
Embodiment 2:
Dispersant 7%, lauryl alcohol polyoxyethylene ether (MOA class) 3% wherein, castor oil polyoxyethylene ether (TX class) 4%;
Collecting agent 24%, wherein the polyethylene glycol Glycol Oleic Acid Ester 5%, castor oil polyoxyethylene ether (EL class) 7%, polyethylene glycol laurate dibasic acid esters 12%;
Smooth agent 66%, wherein triol ester 20%, quaternary alcohol ester 30%, mineral oil 16%;
Additive 3%, wherein the amphoteric phosphate ammonium salt 2%, higher acid 1%.
Embodiment 3:
Dispersant 3%, polyoxyethylene nonylphenol ether (TX class) 2% wherein, lauryl alcohol polyoxyethylene ether (EL class) 1%;
Collecting agent 17%, polyethylene glycol laurate dibasic acid esters 5% wherein, castor oil polyoxyethylene ether 12%;
Smooth agent 73%, wherein binary alcohol esters 30%, triol ester 15%, fatty acid polyethylene glycol ester 28%;
Additive 7%, wherein higher alcohol 1%, modified organic silicon 2%, lauryl alcohol polyoxyethylene ether phosphate sylvite 4%.
After the described ratio batching of above-mentioned three embodiment, the manufacture method of its polypropylene fiber spinning oil is:
With collecting agent, dispersant suction reactor is opened and is stirred, and is warming up to about 50 ℃, stirs, with smooth agent suction reactor, keep about 50 ℃ of temperature again, stir 30min, add additive at last, stir 15min, stir and finish, be cooled to about 30 ℃, blowing, filtration, packing are promptly.
The polypropylene fiber spinning oil of producing according to proportioning of the present invention and manufacture method can reach following quality index:
1, outward appearance (25 ℃) is yellow to brown yellow transparent liquid
2, pH value (1% aqueous solution, 20 ℃) 7.0-8.0
3, effective component content (%, 〉=) 95.0
4, kinematic viscosity (40 ± 0.1 ℃, m
2/ s) (6.5～8.0) * 10
-5
5, stable one week of 18% aqueous solution is not stratified
Claims (6)
1, a kind of polypropylene fiber spinning oil, by smooth agent, dispersant, collecting agent, additive is formed, and it is characterized in that the percentage by weight of each component is: smooth agent 65～75%, dispersant 2～8%, collecting agent 15～25%, additive 2～8%.
2, by the described polypropylene fiber spinning oil of claim 1, it is characterized in that described smooth agent can be mineral oil, double base alcohol ester, triol ester, quaternary alcohol ester, the mixture of one or more in the fatty acid polyethylene glycol ester.
3, by the described polypropylene fiber spinning oil of claim 1, it is characterized in that described dispersant can be castor oil polyoxyethylene ether, lauryl alcohol polyoxyethylene ether, the mixture of one or more in the polyoxyethylene nonylphenol ether.
4, by the described polypropylene fiber spinning oil of claim 1, it is characterized in that described collecting agent can be the polyethylene glycol Glycol Oleic Acid Ester, polyethylene glycol laurate dibasic acid esters, castor oil polyoxyethylene ether, the mixture of one or more in the octanol high-molecular weight atactic polyethers.
5, by the described polypropylene fiber spinning oil of claim 1, it is characterized in that described additive can be silicone oil, modified organic silicon, higher alcohol, higher acid, lauryl alcohol phosphate polyoxyethylene ether sylvite, the hexadecanol phosphate kalium salt, the octadecanol phosphate kalium salt, lauryl alcohol polyoxyethylene ether phosphate sylvite, the mixture of one or more in the amphoteric phosphate ammonium salt.
6, by claim 1 or 2,3, the manufacture method of 4,5 described polypropylene fiber spinning oils is characterized in that the percentage by weight by each component, elder generation is with collecting agent, the dispersant suction reactor of accurate measurement, be heated to 40～80 ℃ and stir, again with in the smooth agent suction reactor, behind stirring 30～50min, add additive, back cooling, filtration, packing stir.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 99124278 CN1257950A (en) | 1999-12-21 | 1999-12-21 | Polypropylene spinning oil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 99124278 CN1257950A (en) | 1999-12-21 | 1999-12-21 | Polypropylene spinning oil and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1257950A true CN1257950A (en) | 2000-06-28 |
Family
ID=5283362
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 99124278 Pending CN1257950A (en) | 1999-12-21 | 1999-12-21 | Polypropylene spinning oil and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1257950A (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101476177B (en) * | 2009-01-03 | 2010-12-08 | 郭清海 | Polypropylene spinning fixation oil solution and production method thereof |
| CN101906714A (en) * | 2010-08-01 | 2010-12-08 | 张中法 | Environment-friendly polypropylene filament yarn oil agent and production method thereof |
| CN102121140A (en) * | 2011-01-13 | 2011-07-13 | 中国石油化工股份有限公司 | Method for producing polyester staple fibers |
| CN101886334B (en) * | 2009-05-15 | 2012-03-07 | 中国石油天然气股份有限公司 | Oiling agent for polypropylene spinning |
| CN103225155A (en) * | 2013-04-16 | 2013-07-31 | 南通纺织职业技术学院 | Mineral filtering canvas made from polypropylene short fibers |
| CN105133311A (en) * | 2015-08-18 | 2015-12-09 | 苏州晟德竹科技发展有限公司 | Polypropylene fiber filament finish, and applications thereof |
| CN105220498A (en) * | 2015-11-03 | 2016-01-06 | 杭州电子科技大学 | A kind of new chemical fibre spinning lubricating oils |
| CN105821665A (en) * | 2015-12-28 | 2016-08-03 | 福建恒安集团有限公司 | Multifunctional ES fiber spinning oil |
| CN105876884A (en) * | 2016-05-16 | 2016-08-24 | 宏杰内衣股份有限公司 | Intelligent ventilated massaging bra and preparation method thereof |
| CN105962446A (en) * | 2016-05-16 | 2016-09-28 | 宏杰内衣股份有限公司 | Washable, antibacterial and breathable bra underwear and preparation method thereof |
| CN106758187A (en) * | 2016-12-10 | 2017-05-31 | 天长市天龙泵阀成套设备厂 | Flame-retardant polypropylene spinning oil and its processing method |
| CN106978726A (en) * | 2017-04-25 | 2017-07-25 | 上海新浦特种助剂有限公司 | A kind of polypropylene fiber spinning oil |
-
1999
- 1999-12-21 CN CN 99124278 patent/CN1257950A/en active Pending
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101476177B (en) * | 2009-01-03 | 2010-12-08 | 郭清海 | Polypropylene spinning fixation oil solution and production method thereof |
| CN101886334B (en) * | 2009-05-15 | 2012-03-07 | 中国石油天然气股份有限公司 | Oiling agent for polypropylene spinning |
| CN101906714A (en) * | 2010-08-01 | 2010-12-08 | 张中法 | Environment-friendly polypropylene filament yarn oil agent and production method thereof |
| CN102121140A (en) * | 2011-01-13 | 2011-07-13 | 中国石油化工股份有限公司 | Method for producing polyester staple fibers |
| CN102121140B (en) * | 2011-01-13 | 2016-04-13 | 中国石油化工股份有限公司 | A kind of manufacture method of polyester staple fiber |
| CN103225155A (en) * | 2013-04-16 | 2013-07-31 | 南通纺织职业技术学院 | Mineral filtering canvas made from polypropylene short fibers |
| CN105133311B (en) * | 2015-08-18 | 2017-10-24 | 苏州晟德竹科技发展有限公司 | A kind of polypropylene filament yarn oil agent and its application method |
| CN105133311A (en) * | 2015-08-18 | 2015-12-09 | 苏州晟德竹科技发展有限公司 | Polypropylene fiber filament finish, and applications thereof |
| CN105220498A (en) * | 2015-11-03 | 2016-01-06 | 杭州电子科技大学 | A kind of new chemical fibre spinning lubricating oils |
| CN105821665A (en) * | 2015-12-28 | 2016-08-03 | 福建恒安集团有限公司 | Multifunctional ES fiber spinning oil |
| CN105876884A (en) * | 2016-05-16 | 2016-08-24 | 宏杰内衣股份有限公司 | Intelligent ventilated massaging bra and preparation method thereof |
| CN105962446A (en) * | 2016-05-16 | 2016-09-28 | 宏杰内衣股份有限公司 | Washable, antibacterial and breathable bra underwear and preparation method thereof |
| CN106758187A (en) * | 2016-12-10 | 2017-05-31 | 天长市天龙泵阀成套设备厂 | Flame-retardant polypropylene spinning oil and its processing method |
| CN106978726A (en) * | 2017-04-25 | 2017-07-25 | 上海新浦特种助剂有限公司 | A kind of polypropylene fiber spinning oil |
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