CN109293600B - 一种去除环氧氯丙烷油层中残留过氧化氢的方法 - Google Patents
一种去除环氧氯丙烷油层中残留过氧化氢的方法 Download PDFInfo
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- CN109293600B CN109293600B CN201811340527.3A CN201811340527A CN109293600B CN 109293600 B CN109293600 B CN 109293600B CN 201811340527 A CN201811340527 A CN 201811340527A CN 109293600 B CN109293600 B CN 109293600B
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/08—Compounds containing oxirane rings with hydrocarbon radicals, substituted by halogen atoms, nitro radicals or nitroso radicals
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- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Epoxy Compounds (AREA)
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Description
实施例 | 油层质量/g | 处理前双氧水含量/% | 接收料液双氧水含量/% | 去除率/% |
11 | 600 | 0.1 | 0.0042 | 95.8 |
12 | 500 | 0.3 | 0.0108 | 96.4 |
13 | 400 | 0.4 | 0.0100 | 97.5 |
14 | 300 | 0.6 | 0.0102 | 98.3 |
15 | 200 | 0.8 | 0.0120 | 98.5 |
16 | 100 | 1.0 | 0.0170 | 98.3 |
实施例 | 温度/℃ | 流速/g·min<sup>-1</sup> | 接收料液过氧化氢含量/% | 去除率/% |
17 | 10 | 3 | 0.0225 | 95.5 |
18 | 20 | 4 | 0.0160 | 96.8 |
19 | 25 | 5 | 0.0140 | 97.2 |
20 | 30 | 7 | 0.0115 | 97.7 |
21 | 30 | 6 | 0.0085 | 98.3 |
22 | 35 | 8 | 0.0060 | 98.8 |
23 | 40 | 5 | 0.0090 | 98.2 |
24 | 40 | 10 | 0.0120 | 97.6 |
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CN111774064B (zh) * | 2019-04-04 | 2023-04-11 | 中国石油化工股份有限公司 | 一种用于分解3-氯丙烯与过氧化氢环氧化反应产物中过氧化氢的催化剂 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2005113452A1 (fr) * | 2004-04-22 | 2005-12-01 | Sidel Participations | Procede de production d'eau de qualite a partir d'un effluent contenant un melange de reactifs oxydants peroxygenes et application a une installation de decontamination d'objets |
JP2015130844A (ja) * | 2014-01-15 | 2015-07-23 | 株式会社片山化学工業研究所 | 過酸化水素の分解処理方法 |
CN105481644A (zh) * | 2015-12-02 | 2016-04-13 | 中国天辰工程有限公司 | 一种去除有机溶剂水溶液中过氧化氢的方法 |
CN106140178A (zh) * | 2015-04-18 | 2016-11-23 | 中国石油化工股份有限公司 | 分解过氧化氢的催化剂及其用于分解环氧化反应产物中过氧化氢的方法 |
CN106140139A (zh) * | 2015-04-18 | 2016-11-23 | 中国石油化工股份有限公司 | 一种用于过氧化氢分解的催化剂以及应用方法 |
CN106140186A (zh) * | 2015-04-18 | 2016-11-23 | 中国石油化工股份有限公司 | 一种分解催化剂及其环氧化反应产物中分解过氧化氢的方法 |
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- 2018-11-12 CN CN201811340527.3A patent/CN109293600B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2005113452A1 (fr) * | 2004-04-22 | 2005-12-01 | Sidel Participations | Procede de production d'eau de qualite a partir d'un effluent contenant un melange de reactifs oxydants peroxygenes et application a une installation de decontamination d'objets |
JP2015130844A (ja) * | 2014-01-15 | 2015-07-23 | 株式会社片山化学工業研究所 | 過酸化水素の分解処理方法 |
CN106140178A (zh) * | 2015-04-18 | 2016-11-23 | 中国石油化工股份有限公司 | 分解过氧化氢的催化剂及其用于分解环氧化反应产物中过氧化氢的方法 |
CN106140139A (zh) * | 2015-04-18 | 2016-11-23 | 中国石油化工股份有限公司 | 一种用于过氧化氢分解的催化剂以及应用方法 |
CN106140186A (zh) * | 2015-04-18 | 2016-11-23 | 中国石油化工股份有限公司 | 一种分解催化剂及其环氧化反应产物中分解过氧化氢的方法 |
CN105481644A (zh) * | 2015-12-02 | 2016-04-13 | 中国天辰工程有限公司 | 一种去除有机溶剂水溶液中过氧化氢的方法 |
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