CN108524778A - A kind of stem of noble dendrobium freeze-dried powder and preparation method thereof - Google Patents
A kind of stem of noble dendrobium freeze-dried powder and preparation method thereof Download PDFInfo
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Abstract
This method discloses a kind of stem of noble dendrobium freeze-dried powder, is prepared by the raw material of following parts by weight：15 40 parts of Dendrobidium huoshanness freeze-dried powder, 5 20 parts of olive berry extract, 10 15 parts of vitamin C, 10 20 parts of broken wall spiral shell pollen pini, 58 parts of ginkgo leaf, 20 30 parts of Sheng Mali Jis extracting solution, 5 10 parts of Cranberry, 5 10 parts of dandelion powder, 35 parts of fennel powder, 36 parts of marigold, 59 parts of lycium ruthenicum extract, 10 15 parts of green plum yeast powder, 5 10 parts of ginseng, 5 10 parts of Radix Astragali, 1 15 parts of isomalt, 1 20 parts of cornstarch, 5 25 parts of magnesium stearate.The present invention dries fresh dendrobium candidum using boulton process, obtains fresh dendrobium candidum freeze-dried powder, can effectively ensure the quality of dendrobium candidum.
Description
Technical field
This method is related to a kind of freeze-dried powder, specifically a kind of stem of noble dendrobium freeze-dried powder and preparation method thereof.
Background technology
Dendrobium candidum (scientific name：DendrobiumofficinaleKimuraetMigo), also known as：Ribbed hedyotis herb, Yunnan iron sheet,
Iron sheet bucket maple.Belong to micro- specific item, the perennial herbaceous plant that grows nonparasitically upon another plant of orchid family.Stem is upright, cylindrical, 9-35 centimetres long, 2-4 millimeters thick,
Sepal and petal yellow green, close similar, long round shape lanceolar is about 1.8cm, wide 4~5mm, 3~June of florescence.It is distributed mainly on
The ground such as Chinese Anhui, Zhejiang, Fujian.Its stem is used as medicine, and belongs to the yin tonics in tonic.
Dendrobium candidum is herbaceos perennial, is distributed widely in the ground such as Guangxi, Yunnan, Zhejiang, Fujian, is typically distributed about
On the dark and damp rock in mountainous region half.
The morphological feature of dendrobium candidum：Stem is upright, cylindrical, 9-35 centimetres long, 2-4 millimeters thick, not branch, has more piece,
1-3-1.7 centimetres of internode length, often in middle part 3-5 pieces of leaf of the above alternate；Ye Erlie, papery, long round shape lanceolar, long 3-4 (- 7)
Centimetre, wide 9-11 (- 15) millimeter, apex is blunt and how many hook turn, and base portion is downward to embrace the sheath of stem, and edge and middle rib are often with pale purple
Color；Leaf sheath often with purple plague purpura, when old its upper limb and stem pine from and opens, and leave 1 ashen gap of ring-type with saving.
Raceme is often sent out from the old stem top for having fallen leaf, has 2-3 flower；Common peduncle is 5-10 millimeters long, and base portion has 2-3
Piece short sheath；Rachis inflection sigmoid, it is 2-4 centimetres long；Petal piece dry film matter, shallow white is oval, 5-7 millimeters long, and apex is slightly
It is blunt；Bennet and ovary are 2-2.5 centimetres long；Sepal and petal yellow green, nearly similar, long round shape lanceolar is about 1.8 centimetres, wide
4-5 millimeters, the sharp point of apex has 5 arteries and veins；Side sepal base portion is broader, about 1 centimetre wide；Calyx capsule cone, is about 5 millimeters, end
It is round；Lip white, base portion have the corpus callosum of 1 green or yellow, and ovum shape lanceolar is more slightly shorter than sepal, middle part reflexed, apex
Anxious point, does not split or unobvious 3 is split, and both sides below middle part have aubergine striped, and how much wavy edge is；Lip disk gathers thin papillary
Hair, and have 1 aubergine patch more than middle part；Stamen column yellow green is about 3 millimeters, and apex both sides respectively have 1 purple point；Stamen
Column foot yellow green band aubergine striped, thinly covered hair；Anther cap white, long ovate triangle are about 2.3 millimeters, and the nearly sharp point in top is simultaneously
And 2 split.The month at florescence 3-6.
In terms of habit, dendrobium candidum is suitable in nice and cool, moistening, the ambient growth of clear air.Usually it is born in sea
It pulls out up on the dark and damp rock in 1600 meters of mountainous region half, the environment of happiness warm and moist weather and half cloudy half light can not resist cold.
In terms of geographical distribution, dendrobium candidum is distributed widely in the Anhui west and south (Dabie Mountain), Eastern Part of Zhejiang Province, China (Yinxian County, day
Platform, fairy house), In Western Fujian Province (Ninghua), the Guangxi northwestward (Tiane), Sichuan, southeastern Yunnan (stone screen, mountain of papers, Malipo, west
Farmland).
In terms of propagation method, fast numerous method and plant division cutting propagation etc. in a organized way.
Tissue rapid propagation method：14~21 days hardenings should be first carried out before tissue-cultured seedling cultivation, concrete measure is to move to tissue-cultured seedling
Hardening room makes its gradual reform of nature environment in the environment of open variation, can bottle outlet plantation when tissue-cultured seedling leaf color is dark green.
First bottle cap is opened before bottle outlet, bottle seedling is allowed to be placed in outdoor air 2~3 days, allows its reform of nature humiture.So
After carry out washing seedling, the seedling with culture medium is gently taken out when washing seedling, is placed in basin and cleans, pollutes seedling and bare-root seeding or few root
Seedling is answered separated.Tissue-cultured seedling is first cleaned with tap water, should mainly wash off agar, in case agar is mouldy to cause rotten, then
It is rinsed with clear water again.When washing seedling preferably based on the size of seedling and quality synchronize be classified, to cultivate, to manage, improve
The survival rate of tissue-cultured seedling simultaneously keeps growth neat.
Plant division cutting propagation method：Selected when plant division life in 1 year or life in 2 years, color and luster it is light green, it is healthy and strong, sprout more, well developed root system and
The plant of no disease and pests harm makees kind of a strain, cuts off deadwood, disconnected branch, old branch and long fibrous root, strain clump is cut, and is divided into little Cong, every clump
Stem strain with leaf 5~7, you can plantation.
In terms of cultivation technique, the planting time of dendrobium candidum is usually annual spring and autumn, and spring is better than autumn.
In Zhejiang area, the Best Times of officinal dendrobium stem plantation are annual mid-April to late June, and this period, temperature was 12~25
DEG C, and air humidity is larger, the test tube seedling transplanting survival rate after bottle outlet is higher and growth time is longer；Followed by mid-September is extremely
Late October, the transplanting of this period are important to carry out the antifreeze work of cold-resistant.The cultivation matrix of dendrobium candidum is High efficiency and high quality cultivation
The biological nature of key, dendrobium candidum requires the existing good water-retaining property of cultivation matrix to have ventilating air permeability, large-scale production again
It is required that cultivation matrix raw material is easy to get, is easy to operate.Report mesostroma has sphagna, rubble, peanut shell, moss, coconut skin, pine tree
Skin, sawdust, charcoal, wooden unit etc., application in production is mainly bark, sawdust or bark, sawdust, rubble, organic fertilizer mixing
Object, wherein bark are ground into 2~3cm or less particles.Officinal dendrobium stem plantation requires to carry out in greenhouse, and the construction of greenhouse requires to do
It keeps off the rain to ventilation, shade, have fly net, and according to the habit of dendrobium candidum, consider the illumination in place, temperature, humidity, lead to
The natural causes such as wind.The preference temperature of Growth of Dendrobium candidum is 15~30 DEG C, and in Zhejiang area, summer is more hot, general to use
80% sunshade net covering, is raised plastic film, is cooled down with profit；Winter is colder, with double under 30%~50% sunshade degree
Layer plastic membrane sealing heat preservation.Dendrobium candidum requires that matrix moistening, air humidity is kept to keep 80% or more preferably, but cannot
Ponding, it is best using sprinkling irrigation or trickle irrigation when watering, it must not irrigation.Different seasons it is different regional irrigation amount it is also different.
Version in 2010《Chinese Pharmacopoeia》The dendrobium candidums of page 265.Dendrobium candidum is as orchid dendrobium candidum
The drying stem of DendrobiumofficinaleKimuraetMigo, plant dendrobium candidum are harvested March in November to next year, are removed
Impurity cuts off part fibrous root, is twisted into spiral shape or spring-like in heating, dries, here it is " Tiepi Fengdous " of people's common name
(earrings dendrobium)；Or cut into chunks, dry or low temperature drying is exactly " dendrobium candidum " of people's common name.As it can be seen that there are three among these
Appellation, one is fresh plant dendrobium candidum, i.e. orchid dendrobium candidum DendrobiumofficinaleKimuraetMigo；Its
Two be the fresh plant through dry and be twisted into the drying stem of spiral shape or spring-like, is known as " Tiepi Fengdou " medicinal material；The third is should
Fresh plant is through cutting into chunks and drying, " dendrobium candidum " medicinal material.Above-mentioned pharmacopeia records the big gun for specifying orchid dendrobium candidum
Method processed, and usually final products form of the people from commercially available orchid dendrobium candidum.As it can be seen that classical
Dendrobium candidum processing, application method are to need to dry fresh orchid dendrobium candidum.It is well known that large batch of iron
The problem of drying of the skin stem of noble dendrobium needs stringent control to go mouldy, and need in this drying process to use smoking process, it is therefore, existing
Process so that various forms of dendrobium candidums is generated secondary pollutions, such as the sulfur content in medicine materical crude slice can be caused seriously to surpass
Mark, so as to cause serious injury to health.
Therefore, with fresh dendrobium candidum convection drying and powdered dendrobium candidum medicine materical crude slice is made, there will be great value
's.For example, the present inventor attempts fresh dendrobium candidum being directly dried in vacuo, removed in a manner of distillation under extremely low temperature
Moisture in dendrobium candidum, then by dried frozen aquatic products through being ground into fine powder, obtained fresh dendrobium candidum freeze-dried powder can make effective ingredient
It is fully retained, the absorptivity of active constituent greatly improves.
It is this fresh however, ensureing that effective ingredient is fully retained, and under the premise of active ingredient draws rate greatly improves
The physical behavior of dendrobium candidum freeze-dried powder is to be improved, such as since powder is loose, in the case where not adding any additive,
Powder flowbility is poor, will cause apparent technical problem when the accurate subpackage of fresh dendrobium candidum freeze-dried powder fills.
Therefore, those skilled in the art are still expected for people and provide a kind of not adding any additive, effective ingredient
The fresh dendrobium candidum freeze-dried powder that be fully retained, active ingredient draws rate greatly improves, and this kind of fresh dendrobium candidum freeze-dried powder
Physical behavior is excellent, to be suitble to be produced in clear production equipment.
Method content
This method is designed to provide a kind of stem of noble dendrobium freeze-dried powder and preparation method thereof, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, this method provides the following technical solutions：
A kind of stem of noble dendrobium freeze-dried powder, is prepared by the raw material of following parts by weight：15-40 parts of Dendrobidium huoshanness freeze-dried powder, olive
5-20 parts of berry extract, 10-15 parts of vitamin C, 10-20 parts of broken wall spiral shell pollen pini, 5-8 parts of ginkgo leaf, Sheng Mali Ji extracting solutions
20-30 parts, 5-10 parts of Cranberry, 5-10 parts of dandelion powder, 3-5 parts of fennel powder, 3-6 parts of marigold, lycium ruthenicum extract 5-9
Part, 10-15 parts of green plum yeast powder, 5-10 parts of ginseng, 5-10 parts of Radix Astragali, 1-15 parts of isomalt, 1-20 parts of cornstarch,
5-25 parts of magnesium stearate.
As this method further embodiment：It is prepared by the raw material of following parts by weight：15 parts of Dendrobidium huoshanness freeze-dried powder,
It is 5 parts of olive berry extract, 10 parts of vitamin C, 10 parts of broken wall spiral shell pollen pini, 5 parts of ginkgo leaf, 20 parts of Sheng Mali Jis extracting solution, climing
More 5 parts of the certain kind of berries, 5 parts of dandelion powder, 3 parts of fennel powder, 3 parts of marigold, 5 parts of lycium ruthenicum extract, 10 parts of green plum yeast powder, ginseng
5 parts, 5 parts of Radix Astragali, 1 part of isomalt, 1 part of cornstarch, 5 parts of magnesium stearate.
As this method further embodiment：It is prepared by the raw material of following parts by weight：40 parts of Dendrobidium huoshanness freeze-dried powder,
It is 20 parts of olive berry extract, 15 parts of vitamin, 20 parts of broken wall spiral shell pollen pini, 8 parts of ginkgo leaf, 30 parts of Sheng Mali Jis extracting solution, climing
More 10 parts of the certain kind of berries, 10 parts of dandelion powder, 5 parts of fennel powder, 6 parts of marigold, 9 parts of lycium ruthenicum extract, 15 parts of green plum yeast powder, people
10 parts of ginseng, 10 parts of Radix Astragali, 15 parts of isomalt, 20 parts of cornstarch, 25 parts of magnesium stearate.
As this method further embodiment：It is prepared by the raw material of following parts by weight：20 parts of Dendrobidium huoshanness freeze-dried powder,
It is 10 parts of olive berry extract, 12 parts of vitamin C, 12 parts of broken wall spiral shell pollen pini, 6 parts of ginkgo leaf, 25 parts of Sheng Mali Jis extracting solution, climing
More 6 parts of the certain kind of berries, 6 parts of dandelion powder, 4 parts of fennel powder, 4 parts of marigold, 6 parts of lycium ruthenicum extract, 11 parts of green plum yeast powder, ginseng
6 parts, 6 parts of Radix Astragali, 5 parts of isomalt, 5 parts of cornstarch, 6 parts of magnesium stearate.
As this method further embodiment：It is prepared by the raw material of following parts by weight：25 parts of Dendrobidium huoshanness freeze-dried powder,
It is 15 parts of olive berry extract, 15 parts of vitamin C, 20 parts of broken wall spiral shell pollen pini, 8 parts of ginkgo leaf, 30 parts of Sheng Mali Jis extracting solution, climing
More 10 parts of the certain kind of berries, 10 parts of dandelion powder, 5 parts of fennel powder, 6 parts of marigold, 9 parts of lycium ruthenicum extract, 15 parts of green plum yeast powder, people
10 parts of ginseng, 10 parts of Radix Astragali, 15 parts of isomalt, 20 parts of cornstarch, 5-25 parts of magnesium stearate.
As this method further scheme：A kind of preparation method of stem of noble dendrobium freeze-dried powder, includes the following steps：1) it chooses
It picks：It washes using fresh dendrobium candidum former material as raw material, remove impurity removing, rinsed with pure water；2) stripping and slicing：By step 1) treated iron
Skin stem of noble dendrobium machinery segment, is cut into the section of 5cm long；3) by step 2), treated that dendrobium candidum is placed in steam-explosion jar, is first passed through nitrogen
Gas to steam explosion pressure inside the tank is 1.2-2.4MPa, explosion treatment 5-35min；Then being passed through steam to steam explosion pressure inside the tank rapidly is
After 1.0-1.8MPa, Steam explosion treatment 2-5min, room temperature is concentrated into relative density 1.10-1.20, is spray-dried concentrate, obtains
Powder；S2,3-8 times of water is added into powder, neutral proteinase is added for the ratio of 2-3% by mass percentage, by quality hundred
Divide than being that flavor protease is added in 1-2%, digests 1-2h at 30-50 DEG C, filter, obtain enzymolysis liquid；4) enzymolysis liquid receives：Enzymolysis liquid
Pass through 28-32 mesh filter screens；5) it is dried in vacuo：Vacuum drying is divided into three phases：Precooling treatment, freezing processing, heating treatment；Institute
The temperature for stating precooling is -18 DEG C~-20 DEG C, overnight；Condenser temperature is -26 DEG C during the freezing processing, and cooling time is
16~22h, the sublimation temperature during heating treatment are 40~45 DEG C, and sublimation time is 12~18h；Entire process of vacuum drying
In vacuum degree be -1.1~-0.1Mpa；Obtain freeze-dried powder；6) it crushes：Freeze-dried powder is crushed neatly through pulverizer, particle passes through
70-90 mesh screens；7) it collects：The particle by 70-90 mesh screens is collected, is packed, sealing.
Compared with prior art, the advantageous effect of this method is：The present invention prepares the present invention using vacuum drying technique
Fresh dendrobium candidum freeze-dried powder, vacuum drying technique be sample freezing after in the case where keeping freezing state, sloughed using vacuum condition
The process of excessive moisture in sample.And drying process carries out under low-temperature condition, relatively conventional dries, dries, spraying
The original color of sample can be effectively ensured for mist drying etc. and active ingredient retains to the maximum extent.Boulton process will not
The physical arrangement for changing article, the shape for keeping article drying front and back are basically unchanged with size, compare and use other methods drying sample
Closer to fresh products after rehydration, and fresh sample is freeze-dried rear convenient for preservation and transport.So the present invention is dry using vacuum
Dry method dries fresh dendrobium candidum, obtains fresh dendrobium candidum freeze-dried powder, can effectively ensure the quality of dendrobium candidum.
Specific implementation mode
The technical solution in this method embodiment is clearly and completely described below, it is clear that described embodiment
Only this method a part of the embodiment, instead of all the embodiments.Based on the embodiment in this method, the common skill in this field
The every other embodiment that art personnel are obtained without making creative work belongs to the model of this method protection
It encloses.
A kind of embodiment 1, stem of noble dendrobium freeze-dried powder, is prepared by the raw material of following parts by weight：Dendrobidium huoshanness freeze-dried powder 15-40
Part, 5-20 parts of olive berry extract, 10-15 parts of vitamin C, 10-20 parts of broken wall spiral shell pollen pini, 5-8 parts of ginkgo leaf, Sheng Mali Jis
20-30 parts of extracting solution, 5-10 parts of Cranberry, 5-10 parts of dandelion powder, 3-5 parts of fennel powder, 3-6 parts of marigold, lycium ruthenicum carry
Take 5-9 parts of object, 10-15 parts of green plum yeast powder, 5-10 parts of ginseng, 5-10 parts of Radix Astragali, 1-15 parts of isomalt, cornstarch
1-20 parts, 5-25 parts of magnesium stearate.
A kind of embodiment 2, stem of noble dendrobium freeze-dried powder, is prepared by the raw material of following parts by weight：15 parts of Dendrobidium huoshanness freeze-dried powder,
It is 5 parts of olive berry extract, 10 parts of vitamin C, 10 parts of broken wall spiral shell pollen pini, 5 parts of ginkgo leaf, 20 parts of Sheng Mali Jis extracting solution, climing
More 5 parts of the certain kind of berries, 5 parts of dandelion powder, 3 parts of fennel powder, 3 parts of marigold, 5 parts of lycium ruthenicum extract, 10 parts of green plum yeast powder, ginseng
5 parts, 5 parts of Radix Astragali, 1 part of isomalt, 1 part of cornstarch, 5 parts of magnesium stearate.
A kind of embodiment 3, stem of noble dendrobium freeze-dried powder, is prepared by the raw material of following parts by weight：40 parts of Dendrobidium huoshanness freeze-dried powder,
It is 20 parts of olive berry extract, 15 parts of vitamin, 20 parts of broken wall spiral shell pollen pini, 8 parts of ginkgo leaf, 30 parts of Sheng Mali Jis extracting solution, climing
More 10 parts of the certain kind of berries, 10 parts of dandelion powder, 5 parts of fennel powder, 6 parts of marigold, 9 parts of lycium ruthenicum extract, 15 parts of green plum yeast powder, people
10 parts of ginseng, 10 parts of Radix Astragali, 15 parts of isomalt, 20 parts of cornstarch, 25 parts of magnesium stearate.
A kind of embodiment 4, stem of noble dendrobium freeze-dried powder, is prepared by the raw material of following parts by weight：20 parts of Dendrobidium huoshanness freeze-dried powder,
It is 10 parts of olive berry extract, 12 parts of vitamin C, 12 parts of broken wall spiral shell pollen pini, 6 parts of ginkgo leaf, 25 parts of Sheng Mali Jis extracting solution, climing
More 6 parts of the certain kind of berries, 6 parts of dandelion powder, 4 parts of fennel powder, 4 parts of marigold, 6 parts of lycium ruthenicum extract, 11 parts of green plum yeast powder, ginseng
6 parts, 6 parts of Radix Astragali, 5 parts of isomalt, 5 parts of cornstarch, 6 parts of magnesium stearate.
A kind of embodiment 5, stem of noble dendrobium freeze-dried powder, is prepared by the raw material of following parts by weight：25 parts of Dendrobidium huoshanness freeze-dried powder,
It is 15 parts of olive berry extract, 15 parts of vitamin C, 20 parts of broken wall spiral shell pollen pini, 8 parts of ginkgo leaf, 30 parts of Sheng Mali Jis extracting solution, climing
More 10 parts of the certain kind of berries, 10 parts of dandelion powder, 5 parts of fennel powder, 6 parts of marigold, 9 parts of lycium ruthenicum extract, 15 parts of green plum yeast powder, people
10 parts of ginseng, 10 parts of Radix Astragali, 15 parts of isomalt, 20 parts of cornstarch, 5-25 parts of magnesium stearate.
A kind of preparation method of stem of noble dendrobium freeze-dried powder, includes the following steps：1) it picks：Using fresh dendrobium candidum former material as raw material
It washes, remove impurity removing, rinsed with pure water；2) stripping and slicing：By step 1) treated dendrobium candidum machinery segment, it is cut into 5cm's long
Section；3) by step 2), treated that dendrobium candidum is placed in steam-explosion jar, and it is 1.2- to be first passed through nitrogen to steam explosion pressure inside the tank
2.4MPa, explosion treatment 5-35min；Then it is 1.0-1.8MPa to be passed through steam to steam explosion pressure inside the tank rapidly, at steam blasting
After managing 2-5min, room temperature is concentrated into relative density 1.10-1.20, is spray-dried concentrate, obtains powder；S2, it is added into powder
Neutral proteinase is added for the ratio of 2-3% by mass percentage in 3-8 times of water, and flavor egg is added for 1-2% by mass percentage
White enzyme digests 1-2h at 30-50 DEG C, filters, obtains enzymolysis liquid；4) enzymolysis liquid receives：Enzymolysis liquid passes through 28-32 mesh filter screens；5) true
Sky is dry：Vacuum drying is divided into three phases：Precooling treatment, freezing processing, heating treatment；The temperature of the precooling is -18 DEG C
~-20 DEG C, overnight；Condenser temperature is -26 DEG C during the freezing processing, and cooling time is 16~22h, heating treatment process
In sublimation temperature be 40~45 DEG C, sublimation time be 12~18h；Vacuum degree in entire process of vacuum drying is -1.1~-
0.1Mpa；Obtain freeze-dried powder；6) it crushes：Freeze-dried powder is crushed neatly through pulverizer, particle passes through 70-90 mesh screens；7) it collects：
The particle by 70-90 mesh screens is collected, is packed, sealing.
The present invention prepares the fresh dendrobium candidum freeze-dried powder of the present invention using vacuum drying technique, and vacuum drying technique is sample
After product freezing in the case where keeping freezing state, the process of the excessive moisture in sample is sloughed using vacuum condition.And drying process is
Carried out under low-temperature condition, it is relatively conventional dry, dry, being spray-dried etc. can be effectively ensured the original color of sample, perfume (or spice),
Taste and active ingredient retain to the maximum extent.Boulton process will not change the physical arrangement of article, before and after so that article is dried
Shape is basically unchanged with size, is compared closer to fresh products after using other methods drying sample rehydration, and fresh sample passes through
It is convenient for preservation and transport after freeze-drying.So the present invention dries fresh dendrobium candidum using boulton process, fresh dendrobium candidum is obtained
Freeze-dried powder can effectively ensure the quality of dendrobium candidum.
It is obvious to a person skilled in the art that this method is not limited to the details of above-mentioned exemplary embodiment, Er Qie
Without departing substantially from this method spirit or essential attributes in the case of, can realize this method in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the range of this method is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included in this method.In addition, it should be understood that although this specification is described in terms of embodiments, but it is not each
Embodiment only contains an independent technical solution, and this description of the specification is merely for the sake of clarity, this field
Technical staff should consider the specification as a whole, and the technical solutions in the various embodiments may also be suitably combined, form this
The other embodiment that field technology personnel are appreciated that.
Claims (6)
1. a kind of stem of noble dendrobium freeze-dried powder, which is characterized in that be prepared by the raw material of following parts by weight：Dendrobidium huoshanness freeze-dried powder 15-
40 parts, 5-20 parts of olive berry extract, 10-15 parts of vitamin C, 10-20 parts of broken wall spiral shell pollen pini, 5-8 parts of ginkgo leaf, Sheng Mali
20-30 parts of Ji extracting solution, 5-10 parts of Cranberry, 5-10 parts of dandelion powder, 3-5 parts of fennel powder, 3-6 parts of marigold, lycium ruthenicum
5-9 parts of extract, 10-15 parts of green plum yeast powder, 5-10 parts of ginseng, 5-10 parts of Radix Astragali, 1-15 parts of isomalt, corn form sediment
1-20 parts of powder, 5-25 parts of magnesium stearate.
2. stem of noble dendrobium freeze-dried powder according to claim 1, which is characterized in that be prepared by the raw material of following parts by weight：Suddenly
15 parts of mountain stem of noble dendrobium freeze-dried powder, 5 parts of olive berry extract, 10 parts of vitamin C, 10 parts of broken wall spiral shell pollen pini, 5 parts of ginkgo leaf, Sheng Ma
20 parts of sharp Ji extracting solution, 5 parts of Cranberry, 5 parts of dandelion powder, 3 parts of fennel powder, 3 parts of marigold, 5 parts of lycium ruthenicum extract, blueness
10 parts of plum yeast powder, 5 parts of ginseng, 5 parts of Radix Astragali, 1 part of isomalt, 1 part of cornstarch, 5 parts of magnesium stearate.
3. stem of noble dendrobium freeze-dried powder according to claim 1, which is characterized in that be prepared by the raw material of following parts by weight：Suddenly
40 parts of mountain stem of noble dendrobium freeze-dried powder, 20 parts of olive berry extract, 15 parts of vitamin, 20 parts of broken wall spiral shell pollen pini, 8 parts of ginkgo leaf, Sheng Ma
30 parts of sharp Ji extracting solution, 10 parts of Cranberry, 10 parts of dandelion powder, 5 parts of fennel powder, 6 parts of marigold, 9 parts of lycium ruthenicum extract,
15 parts of green plum yeast powder, 10 parts of ginseng, 10 parts of Radix Astragali, 15 parts of isomalt, 20 parts of cornstarch, 25 parts of magnesium stearate.
4. stem of noble dendrobium freeze-dried powder according to claim 1, which is characterized in that be prepared by the raw material of following parts by weight：Suddenly
20 parts of mountain stem of noble dendrobium freeze-dried powder, 10 parts of olive berry extract, 12 parts of vitamin C, 12 parts of broken wall spiral shell pollen pini, 6 parts of ginkgo leaf, Sheng Ma
25 parts of sharp Ji extracting solution, 6 parts of Cranberry, 6 parts of dandelion powder, 4 parts of fennel powder, 4 parts of marigold, 6 parts of lycium ruthenicum extract, blueness
11 parts of plum yeast powder, 6 parts of ginseng, 6 parts of Radix Astragali, 5 parts of isomalt, 5 parts of cornstarch, 6 parts of magnesium stearate.
5. stem of noble dendrobium freeze-dried powder according to claim 1, which is characterized in that be prepared by the raw material of following parts by weight：Suddenly
25 parts of mountain stem of noble dendrobium freeze-dried powder, 15 parts of olive berry extract, 15 parts of vitamin C, 20 parts of broken wall spiral shell pollen pini, 8 parts of ginkgo leaf, Sheng Ma
30 parts of sharp Ji extracting solution, 10 parts of Cranberry, 10 parts of dandelion powder, 5 parts of fennel powder, 6 parts of marigold, 9 parts of lycium ruthenicum extract,
15 parts of green plum yeast powder, 10 parts of ginseng, 10 parts of Radix Astragali, 15 parts of isomalt, 20 parts of cornstarch, magnesium stearate 5-25
Part.
6. a kind of preparation method of stem of noble dendrobium freeze-dried powder as described in claim 1, which is characterized in that include the following steps：1) it chooses
It picks：It washes using fresh dendrobium candidum former material as raw material, remove impurity removing, rinsed with pure water；2) stripping and slicing：By step 1) treated iron
Skin stem of noble dendrobium machinery segment, is cut into the section of 5cm long；3) by step 2), treated that dendrobium candidum is placed in steam-explosion jar, is first passed through nitrogen
Gas to steam explosion pressure inside the tank is 1.2-2.4MPa, explosion treatment 5-35min；Then being passed through steam to steam explosion pressure inside the tank rapidly is
After 1.0-1.8MPa, Steam explosion treatment 2-5min, room temperature is concentrated into relative density 1.10-1.20, is spray-dried concentrate, obtains
Powder；S2,3-8 times of water is added into powder, neutral proteinase is added for the ratio of 2-3% by mass percentage, by quality hundred
Divide than being that flavor protease is added in 1-2%, digests 1-2h at 30-50 DEG C, filter, obtain enzymolysis liquid；4) enzymolysis liquid receives：Enzymolysis liquid
Pass through 28-32 mesh filter screens；5) it is dried in vacuo：Vacuum drying is divided into three phases：Precooling treatment, freezing processing, heating treatment；Institute
The temperature for stating precooling is -18 DEG C~-20 DEG C, overnight；Condenser temperature is -26 DEG C during the freezing processing, and cooling time is
16~22h, the sublimation temperature during heating treatment are 40~45 DEG C, and sublimation time is 12~18h；Entire process of vacuum drying
In vacuum degree be -1.1~-0.1Mpa；Obtain freeze-dried powder；6) it crushes：Freeze-dried powder is crushed neatly through pulverizer, particle passes through
70-90 mesh screens；7) it collects：The particle by 70-90 mesh screens is collected, is packed, sealing.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106473143A (en) * | 2016-10-19 | 2017-03-08 | 南京希元生物医药科技有限公司 | A kind of Herba Dendrobii lyophilized powder buccal tablet |
| CN106722981A (en) * | 2016-11-26 | 2017-05-31 | 上海兰葹生物科技有限公司 | A kind of health food of Dendrobidium huoshanness |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106473143A (en) * | 2016-10-19 | 2017-03-08 | 南京希元生物医药科技有限公司 | A kind of Herba Dendrobii lyophilized powder buccal tablet |
| CN106722981A (en) * | 2016-11-26 | 2017-05-31 | 上海兰葹生物科技有限公司 | A kind of health food of Dendrobidium huoshanness |
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Application publication date: 20180914 |