CN108166076A - Mulberry silk fiber soaking technology - Google Patents
Mulberry silk fiber soaking technology Download PDFInfo
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- CN108166076A CN108166076A CN201810131487.5A CN201810131487A CN108166076A CN 108166076 A CN108166076 A CN 108166076A CN 201810131487 A CN201810131487 A CN 201810131487A CN 108166076 A CN108166076 A CN 108166076A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
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Abstract
The present invention proposes a kind of mulberry silk fiber soaking technology, and including water quality allotment → immersion → discharging, flushing, dehydration → boiling-off → bundle wash, rinse, be dehydrated, soft, drying process.Increase the surface-active of silk fiber by impregnating wet processes, there is more flexible absorbent, antistatic, sterilization and easy dyeing etc. by the silk fiber material after surface treatment, and remain the bioactivity of silk fiber material, the performance of silk fiber material is improved, the fiber quality produced is good.The soaking technology of the present invention can be such that product residue glue is controlled well 1.5% -2.5%, and for residual oil content within 3%, which not only reduces the damage to fiber, while also mitigates labor intensity.
Description
Technical field
The present invention relates to mulberry silk fiber manufacture crafts, and in particular to a kind of mulberry silk fiber soaking technology.
Background technology
Mulberry silk is secretion silk liquid concretionary continuous fiber when matured silkworm cocoons, is the animal that the mankind utilize earliest
One of fiber, the strand being pumped from single silk cocoon are known as silk, it borrows silk gum bonding to coat by two single fibers.Silkworm
Silk, is natural animal protein fiber, is that silk weaves most important raw material.Its smooth pliable rich in gloss, has the winter to warm up the summer
Cool feeling, there is when friction that unique " " phenomenon has good extensibility, preferable heat resistance to scroop.
China is the cradle of Sericulture, is global maximum Silk quality producing country and supply country, in international Silk quality
Occupy leading status and absolute monopoly position in the market, major contribution is made that for national economy and foreign exchange earning.Due to
China's silkworm production new districtdevelopment is rapid, and at present, production technology lag, production environment rather harsh, working condition is poor, adds
The fluctuation of Cocoon Price, there is also the declines of different amplitudes for silk cocoon cocoon quality.Silk cocoon classification on, silk cocoon be broadly divided into get on the bus cocoon and
Spoiled cocoon, spoiled cocoon mainly includes dupion, yellow spotted cocoon, cocoon pressed by cocooning frame, malformed cocoon, thin shelled cocoon, dead worm cocoon, maggot-pierced cocoon etc., with cocoon quality
Decline, the ratio of spoiled cocoon is continuously increased, and the thing followed is that knabs material is also continuously increased.According to incompletely statistics, it is national
The silkworm spoiled cocoon produced every year is in ten thousand tons of 5-6, and mulberry shoot is spat, 50,000 tons of basinetto silk agreement that contracts a film or TV play to an actor or actress.These large quantities of spoiled cocoons and mulberry shoot are spat, basinetto silk
Piece can only carry out deep processing and become silk spinning raw material, be processed into Sang Mianqiu and silk quilt etc..
On silk spinning raw material product, the quality of entire silk spinning raw material is played very in immersion of the mulberry silk fiber in soak
Crucial effect.Existing immersion process immersion effect is bad, so as to cause the fiber quality that postorder is produced undesirable, influences
Silk spinning product.
Invention content
The technical problems to be solved by the invention are to provide a kind of mulberry silk fiber soaking technology, in the mistake of processing silk fiber
The technique can be such that mulberry silk fiber is preferably impregnated in journey, and the fiber quality produced is good, make the functional characteristic of silk fiber
It is not fully exerted.
In order to solve the above technical problems, the technical solution used in the present invention is：A kind of mulberry silk fiber soaking technology, packet
Include following process：
Water quality allotment → immersion → discharging, flushing, dehydration → boiling-off → bundle are washed, are rinsed, being dehydrated, soft, drying, wherein：
Water quality is allocated, and implantation temperature is 90 DEG C~98 DEG C of 2 tons of water in soaking pit, and lightweight sodium bicarbonate 3000 is added in into soaking pit
Gram, sodium silicate（Waterglass）2500 grams~3500 grams, silk spinning refining 1000 grams~1500 grams of brightening agent, 3000 grams of 209 detergent
~5000 grams, 20000 grams~25000 grams of hydrogen peroxide, bath raio 1：20, pH value 9~10；
Impregnate, in soaking pit add in item spit, basinetto silk, spoiled cocoon raw material at least one 100kg, impregnate 12h~16h；
Discharging is rinsed, dehydration, and the raw material after immersion is pulled out, then is fully rinsed well de- dry；
Boiling-off, added in cocoon cooking machine rinse, dewatered raw material, add 150 grams~300 grams of lightweight sodium bicarbonate, 209 wash
Wash 300 grams~500 grams of agent, 250 grams of thiourea dioxide drug auxiliary agent, bath raio 1：60,90 DEG C~100 DEG C of boiling-off temperature, boiling-off
The min of 18 min of time~24；
Bundle is washed, is rinsed, being dehydrated, soft, drying, and the raw material after boiling-off is carried out pricking washing, rinsing successively again, is taken off again after wash clean
Water finally softens, dries.
The present invention is increased using the mulberry silk fiber soaking technology designed by above-mentioned technical proposal by impregnating wet processes
The surface-active of silk fiber, by the silk fiber material after surface treatment have more flexible absorbent, it is antistatic, sterilization and
The functions such as easy dyeing, and the bioactivity of silk fiber material is remained, the performance of silk fiber material is improved, is produced
Fiber quality it is good, expanded application range and the field of silk fiber material, the needs of different application can be met.The present invention's
Soaking technology can be such that product residue glue is controlled well 1.5% -2.5%, and within 3%, which not only reduces residual oil content
Damage to fiber, while also mitigate labor intensity.
Description of the drawings
Fig. 1 shows the process flow diagrams of mulberry silk fiber soaking technology of the present invention.
Specific embodiment
It elaborates below in conjunction with the accompanying drawings to mulberry silk fiber soaking technology of the present invention.
Embodiment 1
Mulberry silk fiber soaking technology of the present invention, including following process：
Water quality allotment → immersion → discharging, flushing, dehydration → boiling-off → bundle are washed, are rinsed, being dehydrated, soft, drying.Wherein：
Water quality is allocated, and implantation temperature is 90 DEG C of 2 tons of water in soaking pit, and 3000 grams of lightweight sodium bicarbonate, bubble are added in into soaking pit
Choline（Waterglass）2500 grams, silk spinning refining 1000 grams of brightening agent, 3000 grams of 209 detergent, 20000 grams of hydrogen peroxide, bath raio 1：
20（That is 100 kilograms of raw material is put in 2 tons of water）, pH value 9；
Impregnate, in soaking pit add in item spit, basinetto silk, spoiled cocoon raw material at least one 100kg, impregnate 12h.Immersion mainly first makes
Silk gum Peng Run in boiling-off convenient for degumming, reduces the damage to silk fiber；
Discharging is rinsed, dehydration, and the raw material after immersion is pulled out, then is fully rinsed well de- dry；
Boiling-off adds in flushing, dewatered raw material in cocoon cooking machine, adds 150 grams of lightweight sodium bicarbonate, 209 detergent 300
Gram, the drug auxiliary agent of 250 grams of thiourea dioxide, bath raio 1：60,90 DEG C of boiling-off temperature, 18 min of boiling-off time；
Bundle is washed, is rinsed, being dehydrated, soft, drying, and the raw material after boiling-off is carried out pricking washing, rinsing successively again, is passed through again after wash clean
Dewaterer is dehydrated, and is softened finally by soft machine and is dried by dryer.
Embodiment 2
Mulberry silk fiber soaking technology of the present invention, including following process：
Water quality allotment → immersion → discharging, flushing, dehydration → boiling-off → bundle are washed, are rinsed, being dehydrated, soft, drying.Wherein：
Water quality is allocated, and implantation temperature is 94 DEG C of 2 tons of water in soaking pit, and 3000 grams of lightweight sodium bicarbonate, bubble are added in into soaking pit
Choline（Waterglass）3000 grams, silk spinning refining 1300 grams of brightening agent, 4000 grams of 209 detergent, 23000 grams of hydrogen peroxide, bath raio 1：
20（That is 100 kilograms of raw material is put in 2 tons of water）, pH value 9.5；
Impregnate, in soaking pit add in item spit, basinetto silk, spoiled cocoon raw material at least one 100kg, impregnate 14h.Immersion mainly first makes
Silk gum Peng Run in boiling-off convenient for degumming, reduces the damage to silk fiber；
Discharging is rinsed, dehydration, and the raw material after immersion is pulled out, then is fully rinsed well de- dry；
Boiling-off adds in flushing, dewatered raw material in cocoon cooking machine, adds 230 grams of lightweight sodium bicarbonate, 209 detergent 400
Gram, the drug auxiliary agent of 250 grams of thiourea dioxide, bath raio 1：60,95 DEG C of boiling-off temperature, boiling-off time 21min；
Bundle is washed, is rinsed, being dehydrated, soft, drying, and the raw material after boiling-off is carried out pricking washing, rinsing successively again, is passed through again after wash clean
Dewaterer is dehydrated, and is softened finally by soft machine and is dried by dryer.
Embodiment 3
Mulberry silk fiber soaking technology of the present invention, including following process：
Water quality allotment → immersion → discharging, flushing, dehydration → boiling-off → bundle are washed, are rinsed, being dehydrated, soft, drying.Wherein：
Water quality is allocated, and implantation temperature is 98 DEG C of 2 tons of water in soaking pit, and 3000 grams of lightweight sodium bicarbonate, bubble are added in into soaking pit
Choline（Waterglass）3500 grams, silk spinning refining 1500 grams of brightening agent, 5000 grams of 209 detergent, 25000 grams of hydrogen peroxide, bath raio 1：
20（That is 100 kilograms of raw material is put in 2 tons of water）, pH value 10；
Impregnate, in soaking pit add in item spit, basinetto silk, spoiled cocoon raw material at least one 100kg, impregnate 16h.Immersion mainly first makes
Silk gum Peng Run in boiling-off convenient for degumming, reduces the damage to silk fiber；
Discharging is rinsed, dehydration, and the raw material after immersion is pulled out, then is fully rinsed well de- dry；
Boiling-off adds in flushing, dewatered raw material in cocoon cooking machine, adds 300 grams of lightweight sodium bicarbonate, 209 detergent 500
Gram, the drug auxiliary agent of 250 grams of thiourea dioxide, bath raio 1：60,100 DEG C of boiling-off temperature, 24 min of boiling-off time；
Bundle is washed, is rinsed, being dehydrated, soft, drying, and the raw material after boiling-off is carried out pricking washing, rinsing successively again, is passed through again after wash clean
Dewaterer is dehydrated, and is softened finally by soft machine and is dried by dryer.
According to national standard, the quality of silkworm cotton balls, according to by the comprehensive of the qualitative techniques index and presentation quality for examining cotton balls
Achievement is synthesized, is divided into I -1 grade of A, I -2 grade of A, I -3 grade of A, II -1 grade of B, II -2 grade of B, III -1 grade of C, III -2 grade of C and grade outer product.Silkworm
The qualitative techniques index of cotton balls provides as follows.
Mulberry silk fiber soaking technology of the present invention, the testing result after being impregnated at random to more batches of mulberry silk fibers are as follows.
Mulberry silk fiber impregnate after by randomly select detection, average fiber length, short fiber index, cotton knot, cleanliness factor and
The indices such as oil content are above national standard, further demonstrate that mulberry silk fiber soaking technology of the present invention impregnates significant effect.
Claims (1)
1. a kind of mulberry silk fiber soaking technology, it is characterized in that including following process：
Water quality allotment → immersion → discharging, flushing, dehydration → boiling-off → bundle are washed, are rinsed, being dehydrated, soft, drying, wherein：
Water quality is allocated, and implantation temperature is 90 DEG C~98 DEG C of 2 tons of water in soaking pit, and lightweight sodium bicarbonate 3000 is added in into soaking pit
Gram, sodium silicate（Waterglass）2500 grams~3500 grams, silk spinning refining 1000 grams~1500 grams of brightening agent, 3000 grams of 209 detergent
~5000 grams, 20000 grams~25000 grams of hydrogen peroxide, bath raio 1：20, pH value 9~10；
Impregnate, in soaking pit add in item spit, basinetto silk, spoiled cocoon raw material at least one 100kg, impregnate 12h~16h；
Discharging is rinsed, dehydration, and the raw material after immersion is pulled out, then is fully rinsed well de- dry；
Boiling-off, added in cocoon cooking machine rinse, dewatered raw material, add 150 grams~300 grams of lightweight sodium bicarbonate, 209 wash
Wash 300 grams~500 grams of agent, 250 grams of thiourea dioxide drug auxiliary agent, bath raio 1：60,90 DEG C~100 DEG C of boiling-off temperature, boiling-off
The min of 18 min of time~24；
Bundle is washed, is rinsed, being dehydrated, soft, drying, and the raw material after boiling-off is carried out pricking washing, rinsing successively again, is taken off again after wash clean
Water finally softens, dries.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810131487.5A CN108166076A (en) | 2018-02-09 | 2018-02-09 | Mulberry silk fiber soaking technology |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810131487.5A CN108166076A (en) | 2018-02-09 | 2018-02-09 | Mulberry silk fiber soaking technology |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108166076A true CN108166076A (en) | 2018-06-15 |
Family
ID=62513912
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810131487.5A Pending CN108166076A (en) | 2018-02-09 | 2018-02-09 | Mulberry silk fiber soaking technology |
Country Status (1)
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| CN (1) | CN108166076A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109576802A (en) * | 2018-12-08 | 2019-04-05 | 河南民兴生物科技股份有限公司 | A kind of silk deep processing device and method |
| CN113798212A (en) * | 2021-08-26 | 2021-12-17 | 深圳同益新中控实业有限公司 | Silkworm cocoon pretreatment equipment and pretreatment process thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02264009A (en) * | 1989-04-05 | 1990-10-26 | Terusuke Sakai | Sericin scouring control of raw silk |
| CN102206875A (en) * | 2011-05-18 | 2011-10-05 | 南充银海丝绸有限公司 | Method for separating and refining silk reeling leftovers |
| CN102560696A (en) * | 2011-11-29 | 2012-07-11 | 湖州市农业科学研究院 | Production method of natural colorful mulberry silk floss |
| CN104195649A (en) * | 2014-08-26 | 2014-12-10 | 宜州市壮歌茧丝绸有限公司 | Method and device for processing silk floss winter clothes raw materials by silkworm light defective cocoon |
| CN106894099A (en) * | 2017-01-22 | 2017-06-27 | 江苏苏丝丝绸股份有限公司 | The preparation method of silk refined silk |
-
2018
- 2018-02-09 CN CN201810131487.5A patent/CN108166076A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02264009A (en) * | 1989-04-05 | 1990-10-26 | Terusuke Sakai | Sericin scouring control of raw silk |
| CN102206875A (en) * | 2011-05-18 | 2011-10-05 | 南充银海丝绸有限公司 | Method for separating and refining silk reeling leftovers |
| CN102560696A (en) * | 2011-11-29 | 2012-07-11 | 湖州市农业科学研究院 | Production method of natural colorful mulberry silk floss |
| CN104195649A (en) * | 2014-08-26 | 2014-12-10 | 宜州市壮歌茧丝绸有限公司 | Method and device for processing silk floss winter clothes raw materials by silkworm light defective cocoon |
| CN106894099A (en) * | 2017-01-22 | 2017-06-27 | 江苏苏丝丝绸股份有限公司 | The preparation method of silk refined silk |
Non-Patent Citations (3)
| Title |
|---|
| S.R.SHUKLA等: "《蚕丝的还原漂白》", 《国外纺织技术》 * |
| 王菊生等，: "《染整工艺原理 第二册》", 30 June 1990, 纺织工业出版社 * |
| 邓一民: "《天然纺织纤维加工化学》", 30 September 2010, 西南师范大学出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109576802A (en) * | 2018-12-08 | 2019-04-05 | 河南民兴生物科技股份有限公司 | A kind of silk deep processing device and method |
| CN113798212A (en) * | 2021-08-26 | 2021-12-17 | 深圳同益新中控实业有限公司 | Silkworm cocoon pretreatment equipment and pretreatment process thereof |
| CN113798212B (en) * | 2021-08-26 | 2023-04-07 | 那坡同益新丝绸科技实业有限公司 | Silkworm cocoon pretreatment equipment and pretreatment process thereof |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180615 |
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| RJ01 | Rejection of invention patent application after publication |