CN106894099A - The preparation method of silk refined silk - Google Patents
The preparation method of silk refined silk Download PDFInfo
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- CN106894099A CN106894099A CN201710045005.XA CN201710045005A CN106894099A CN 106894099 A CN106894099 A CN 106894099A CN 201710045005 A CN201710045005 A CN 201710045005A CN 106894099 A CN106894099 A CN 106894099A
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- silk
- continuous piece
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- refined
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01B—MECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING
- D01B7/00—Obtaining silk fibres or filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
- D01C3/02—De-gumming silk
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Animal Husbandry (AREA)
- Mechanical Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses the preparation method of silk refined silk, include successively：Initial Soak, be dehydrated for the first time, open continuous, secondary immersion, two, triple dewatering, bleaching, four dehydrations, reduction, trough washery and five dehydrations, tie it is wet, be dehydrated, shake up, drying for six times, Hui Xing, the quality of raising whole product relatively low by the refined silk percentage of impurity of multiple rinsing.
Description
Technical field
The present invention relates to silk process field, and in particular to a kind of preparation method of silk refined silk.
Background technology
Silk is to integrate light, soft, thin natural fiber in nature, have the good reputation of " human body Second Skin ", quilt
Industry is referred to as " fiber queen ".Using silk as the silk quilt of the inner tube of a tyre there is warming, fluffy soft, Breathable healthcare next to the skin etc. to obtain day
Only thick quality and advantage, existing silk are washed with water the easy cake knot of rear silk fetus, and reason is oil-containing in silk, warp many containing glue
Washing stirring is crossed, factice forms block with silk mixed plate, and these problems are mainly caused by defect present on technique, especially
In the preparation of refined silk, refined silk oil removing removal of impurities not thoroughly oil-containing in follow-up silk fetus, containing it is miscellaneous will be many, the silk being made
By easily it is hardened, it is second-rate.
The content of the invention
The present invention overcomes existing defect to disclose a kind of preparation method of silk refined silk, oil removing good impurity removing effect, greatly
Degree improves the quality of silk quilt.
The present invention is achieved through the following technical solutions：
The preparation method of silk refined silk, comprises the following steps successively：
1）Initial Soak：Silk cocoon is put into succinct machine and is soaked, add the soda ash of the 5-9% of silk cocoon weight, silk cocoon weight 1-1.3%
Detergent and keep soak PH be 8.5-10.5, control 80-100 DEG C of water temperature, soak time 12-18h；Immersion can be by
The oil being attached on silk cocoon is separated, and reaches oil removing purpose.
2）First dehydration：Silk cocoon after immersion is pulled out to be put into dewaterer from succinct machine and is dehydrated for the first time；Dehydration
Operation makes oil removing more thorough.
3）Open silk floss：Silk cocoon after first dehydration opens the continuous piece of continuous formation by opener；
4）Secondary immersion：Continuous piece is put into secondary immersion in tank, soda ash, the control water temperature 80-100 of continuous sheet weight 3% is added
DEG C, soak time 60-72h；Open the silk quality after silk floss loose, can be separated off for the oil of residual by now secondary immersion, remove
Oil is more thorough.
5）2nd, triple dewatering：Continuous piece after immersion carries out second dehydration, then rinses well, then carries out triple dewatering；
Repeatedly dehydration ensures that oil removing is totally thorough.
6）Bleaching：Continuous piece after triple dewatering is bleached in being put into tank, and the 20-40%'s of the continuous sheet weight of addition is double in tank
Oxygen water, bleaching time 14-16h；By the treatment of upstream multiple operation, there is inevitable aberration in silk, bleaching can be protected
Demonstrate,prove the uniformity of product appearance.
7）Four dehydrations：Being pulled out from tank during the continuous piece after bleaching is put into dewaterer carries out four dehydrations：Improve follow-up
The quality of reduction.
8）Reduction：Continuous piece after four times are dehydrated is reduced in being put into succinct machine, adds the 1% of continuous sheet weight soda ash and silk floss
The detergent of the 2% of sheet weight, steam is passed through while 100 DEG C of water temperature of control, and reduction process takes 15min；Remove step upstream
The chemical agent of residual.
9）Trough washery and five dehydrations：Continuous piece after reduction is put into tank carries out five dehydrations after rinsing repeatedly；Wash repeatedly
Wash and be dehydrated, it is ensured that no chemical residues.
10）Knot is wet：Continuous piece after five dehydrations ties wet 15min in being put into 28-32 DEG C of water, and softening agent is added in water；Disappear
Except continuous piece internal electrostatic, soften continuous piece, shorten follow-up time and wake up the time.
11）Six dehydrations：Continuous piece after wet to knot carries out six dehydrations；Ensure that each step impurity does not bring downstream process into.
12）Shake up：Continuous piece after six dehydrations is placed on the machine of shaking up shakes up；Increase fluffy degree degree, play certain removal of impurities effect
Really.
13）Drying：Continuous piece after shaking up is put into drying in steam drying machine and is made refined silk；
14）Hui Xing：Refined silk after drying be placed on normal temperature next time wake up just be available within 5-7 days subsequent technique to use.Silk Hui Xing is one
Individual natural process, returns awake quality and is softened at normal temperatures, prevents subsequent mechanical from processing the fracture of wire phenomenon for occurring.
Further improvement project of the invention is that silk cocoon immersion rotates the roller one of succinct machine when starting every half an hour
It is secondary, add up corotation dynamic 4 times.
Improvement project of the invention further is, it is described it is secondary, three times, four times, five times, six dehydrations take off in drum-type
Dehydration in water dispenser.Repeatedly dehydration and clean, it is ensured that raw material it is pure.
The present invention has advantages below compared with prior art：
What the first, first, secondary immersion of the invention was used is soda ash, and the suitable water temperature of low alkalinity soak cooperation can make attachment
Oil, glue on silk depart from, the effect by reaching oil removing removing glue after cleaning and dewatering, the low refined silk being made of the content of factice
Molding is difficult after washing, fluffy degree is good, in addition, the soak of low alkalinity will not produce destruction by this body structure to silk, it is ensured that former
The quality of material.
2nd, the chemical agent that reduction step of the present invention can remain process upstream, the hydrogen peroxide cleaning especially bleached
Totally, prevent chemical residual, it is ensured that refined silk it is pure, it is ensured that product quality.
3rd, the continuous piece quality by bleaching, reduction is crisp, and tying wet step can soften continuous piece, eliminates the electrostatic between continuous piece,
Greatly shorten the time of follow-up Hui Xing.
4th, step of shaking up of the invention can make silk continuous more fluffy, moreover it is possible to shake off the impurity being entrained in continuous piece, carry
High yield quality.
Brief description of the drawings
Fig. 1 shakes up machine schematic top plan view for the present invention.
Fig. 2 for the present invention shake up machine transmission schematic diagram.
Specific embodiment
Embodiment 1
The preparation method of silk refined silk, comprises the following steps successively：Silk cocoon is put into succinct machine and is soaked, add silk cocoon weight
5% soda ash, silk cocoon weight 1% detergent and keep soak PH be 8.5-10.5, control 80 DEG C of water temperature, during immersion
Between 12h；Silk cocoon after immersion is pulled out to be put into dewaterer from succinct machine and is dehydrated for the first time；Silk cocoon after first dehydration leads to
Cross opener and open the continuous piece of continuous formation；Continuous piece is put into secondary immersion in tank, the 3% of continuous sheet weight soda ash, control water temperature is added
80 DEG C, soak time 60h；Continuous piece after secondary immersion carries out second dehydration, then rinses well, then carries out triple dewatering；
Continuous piece after triple dewatering is bleached in being put into tank, and the 20% of continuous sheet weight hydrogen peroxide, bleaching time 14h are added in tank；From
Being pulled out in tank during the continuous piece after bleaching is put into dewaterer carries out four dehydrations：Continuous piece after four times are dehydrated is put into succinct machine
Reduction, add the 1% of continuous sheet weight soda ash and continuous sheet weight 2% detergent, be passed through steaming while 100 DEG C of control water temperature
Vapour, the process takes 15min；Continuous piece after reduction is put into tank carries out five dehydrations after rinsing repeatedly；After five dehydrations
Continuous piece ties wet 15min in being put into 28 DEG C of water, and softening agent is added in water；Continuous piece after wet to knot carries out six dehydrations；Take off for six times
Continuous piece after water is placed on the machine of shaking up shakes up；Continuous piece after shaking up is put into drying in steam drying machine and is made refined silk, after drying
Refined silk be placed on normal temperature next time wake up just be available within 5-7 days subsequent technique to use.
Once, it is dynamic 4 times to add up corotation for the roller for rotating succinct machine every half an hour when silk cocoon immersion starts, it is secondary, three times,
Four times, five times, six dehydrations dehydration in drum-type dewaterer.Softening agent uses the silk softening agent, detergent to be
Silk detergent.The succinct machine that succinct machine is voluntarily developed using Sijuan Group Co., Ltd., Jiangsu.
Shake up machine such as Fig. 1,2, including frame 1, balance staff 2 is horizontally arranged in frame 1 by bearing block 3, the both sides of balance staff 2
Multiple support bars 4 for carrying material are horizontally fixed with, the support bar 4 is uniformly arranged along the axial direction of balance staff 2, the frame 1
One end be provided with transmission case 5, is provided with motor 6 in the transmission case 5, the motor 6 is rotated by belt drive belt wheel 7, belt wheel 7
Wheel shaft be provided with concentric eccentric wheel 8, eccentric wheel 8 drives the reciprocally swinging of centering block 10 by connecting rod 9, the centering block 10 with
The balance staff 2 is connected.Particularly motor is rotated, and band movable belt pulley is rotated so as to the eccentric rotation of band is dynamic, and one end of connecting rod follows partially
Heart wheel side face is moved, and the other end is upward, push down on centering block realizes that centering block swings, and then realizes that swing rod swings.
Embodiment 2
In embodiment 2：Initial Soak add 9% soda ash, silk cocoon weight 1.3% detergent, control 100 DEG C of water temperature, immersion
Time 18h；100 DEG C of water temperature, soak time 72h are controlled during secondary immersion；The 40% of the continuous sheet weight of the interior addition of tank is double during bleaching
Oxygen water, bleaching time 16h；Continuous piece is put into 32 DEG C of water when tying wet ties wet；Other steps and parameter are same as Example 1.
Embodiment 3
In embodiment 3：Initial Soak add 7% soda ash, silk cocoon weight 1.1% detergent, control 90 DEG C of water temperature, during immersion
Between 15h；90 DEG C of water temperature, soak time 70h are controlled during secondary immersion；The 40% of continuous sheet weight dioxygen is added during bleaching in tank
Water, bleaching time 15h；Continuous piece is put into 30 DEG C of water when tying wet ties wet；Other steps and parameter are same as Example 1.
The silk refined silk being made of embodiment 1,2,3, by national textile product quality testing inspection center（Jiangyin）Inspection
The data of survey such as following table：
From embodiment 1,2,3, the refined silk oil content being made up of the method for the present invention is well below professional standard, oil-containing
It is difficult hardened after the washing of finished product that the low refined silk of rate is made, the refined silk percentage of impurity by multiple rinsing is relatively low, improves whole
The quality of product.
Claims (3)
1. the preparation method of silk refined silk, its feature is comprised the following steps successively：
1）Initial Soak：Silk cocoon is put into succinct machine and is soaked, add the soda ash of the 5-9% of silk cocoon weight, the 1- of silk cocoon weight
The 1.3% detergent and PH for keeping soak is 8.5-10.5, controls 80-100 DEG C of water temperature, soak time 12-18h；
2）First dehydration：Silk cocoon after immersion is pulled out to be put into dewaterer from succinct machine and is dehydrated for the first time；
3）Open silk floss：Silk cocoon after first dehydration opens the continuous piece of continuous formation by opener；
4）Secondary immersion：Continuous piece is put into secondary immersion in tank, the 3% of continuous sheet weight soda ash, control water temperature 80-100 is added
DEG C, soak time 60-72h；
5）2nd, triple dewatering：Continuous piece after immersion carries out second dehydration, then rinses well, then carries out triple dewatering；
6）Bleaching：Continuous piece after triple dewatering is bleached in being put into tank, and the hydrogen peroxide of the 20-40% of continuous sheet weight is added in tank,
Bleaching time 14-16h；
7）Four dehydrations：Being pulled out from tank during the continuous piece after bleaching is put into dewaterer carries out four dehydrations：
8）Reduction：Continuous piece after four times are dehydrated is reduced in being put into succinct machine, adds the 1% of continuous sheet weight soda ash and continuous piece weight
The detergent of the 2% of amount, steam is passed through while 100 DEG C of water temperature of control, and reduction process takes 15min；
9）Trough washery and five dehydrations：Continuous piece after reduction is put into tank carries out five dehydrations after rinsing repeatedly；
10）Knot is wet：Continuous piece after five dehydrations ties wet 15min in being put into 28-32 DEG C of water, and softening agent is added in water；
11）Six dehydrations：Continuous piece after wet to knot carries out six dehydrations；
12）Shake up：Continuous piece after six dehydrations is placed on the machine of shaking up shakes up；
13）Drying：Continuous piece after shaking up is put into drying in steam drying machine and is made refined silk；
14）Hui Xing：Refined silk after drying be placed on normal temperature next time wake up just be available within 5-7 days subsequent technique to use.
2. the preparation method of silk refined silk as claimed in claim 1, it is characterised in that：Silk cocoon immersion is small every half when starting
When rotate the roller of succinct machine once, add up corotation dynamic 4 times.
3. the preparation method of silk refined silk as claimed in claim 1, it is characterised in that：It is described it is secondary, three times, four times, five
Secondary, six dehydrations are dehydrated in drum-type dewaterer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710045005.XA CN106894099A (en) | 2017-01-22 | 2017-01-22 | The preparation method of silk refined silk |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710045005.XA CN106894099A (en) | 2017-01-22 | 2017-01-22 | The preparation method of silk refined silk |
Publications (1)
| Publication Number | Publication Date |
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| CN106894099A true CN106894099A (en) | 2017-06-27 |
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ID=59199098
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710045005.XA Pending CN106894099A (en) | 2017-01-22 | 2017-01-22 | The preparation method of silk refined silk |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108166076A (en) * | 2018-02-09 | 2018-06-15 | 河南民兴生物科技股份有限公司 | Mulberry silk fiber soaking technology |
| CN109811560A (en) * | 2019-01-26 | 2019-05-28 | 桐乡市钜汪家纺有限公司 | A kind of production technology of seven color silk cottons |
| CN111304756A (en) * | 2020-03-06 | 2020-06-19 | 邹仁员 | A eiderdown belt cleaning device for down coat production |
| CN113106622A (en) * | 2021-03-30 | 2021-07-13 | 江苏苏丝丝绸股份有限公司 | Production method of high-purity short-staple cotton combed velvet quilt |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1084908A (en) * | 1992-09-29 | 1994-04-06 | 东台绢纺厂 | Improve the process of basinetto silk and refined silk quality |
| CN102965871A (en) * | 2012-12-19 | 2013-03-13 | 安徽源牌实业（集团）有限责任公司 | Production technique for colorful cocoon silk cotton |
| CN103757713A (en) * | 2013-12-19 | 2014-04-30 | 河南省民兴茧丝绸有限责任公司 | Refining process for tussah cut cocoon |
| CN104695199A (en) * | 2015-02-11 | 2015-06-10 | 海门市润圣纺织品有限公司 | Tussah spun silk textile as well as manufacturing method and application thereof |
-
2017
- 2017-01-22 CN CN201710045005.XA patent/CN106894099A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1084908A (en) * | 1992-09-29 | 1994-04-06 | 东台绢纺厂 | Improve the process of basinetto silk and refined silk quality |
| CN102965871A (en) * | 2012-12-19 | 2013-03-13 | 安徽源牌实业（集团）有限责任公司 | Production technique for colorful cocoon silk cotton |
| CN103757713A (en) * | 2013-12-19 | 2014-04-30 | 河南省民兴茧丝绸有限责任公司 | Refining process for tussah cut cocoon |
| CN104695199A (en) * | 2015-02-11 | 2015-06-10 | 海门市润圣纺织品有限公司 | Tussah spun silk textile as well as manufacturing method and application thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108166076A (en) * | 2018-02-09 | 2018-06-15 | 河南民兴生物科技股份有限公司 | Mulberry silk fiber soaking technology |
| CN109811560A (en) * | 2019-01-26 | 2019-05-28 | 桐乡市钜汪家纺有限公司 | A kind of production technology of seven color silk cottons |
| CN109811560B (en) * | 2019-01-26 | 2022-06-03 | 桐乡市钜汪家纺有限公司 | Production process of colorful silk floss |
| CN111304756A (en) * | 2020-03-06 | 2020-06-19 | 邹仁员 | A eiderdown belt cleaning device for down coat production |
| CN111304756B (en) * | 2020-03-06 | 2022-04-22 | 扬州苏油油成商贸实业有限公司 | A eiderdown belt cleaning device for down coat production |
| CN113106622A (en) * | 2021-03-30 | 2021-07-13 | 江苏苏丝丝绸股份有限公司 | Production method of high-purity short-staple cotton combed velvet quilt |
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Application publication date: 20170627 |