CN107802579A - Rosemary toothpaste and preparation method thereof - Google Patents
Rosemary toothpaste and preparation method thereof Download PDFInfo
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- CN107802579A CN107802579A CN201711283682.1A CN201711283682A CN107802579A CN 107802579 A CN107802579 A CN 107802579A CN 201711283682 A CN201711283682 A CN 201711283682A CN 107802579 A CN107802579 A CN 107802579A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/22—Peroxides; Oxygen; Ozone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses a kind of rosemary toothpaste, raw material is：20~45 parts of calcium carbonate, 0.5~1 part of sodium cellulose glycolate, 1~3 part of laruyl alcohol sodium sulfovinate, 12~20 parts of sorbierite, 1~3 part of honey, 0.5~1 part of pigment, 0.5~3 part of dandelion extract, 0.5~2 part of Baical Skullcap root P.E, 2~5 parts of tea oil, 0.5~5 part of Rosmarinus officinalis extract, 0.5~2 part of Rosemary Oil, 2~5 parts of rosemary rhizome powder, 10~30 parts of rosemary hydrosol；Rosemary toothpaste of the present invention uses the rosemary biologically active prod of variform as raw material, and it is raw material to be equipped with dandelion extract, Baical Skullcap root P.E, micronization ozone tea oil etc., product is set to be protruded in the effect of antibacterial, anti-inflammatory fermentation, and product has the special flavor of rosemary；In addition, the lotion of the toothpaste prepared using the inventive method is uniform, fine and smooth, the delicate fragrance of rosemary is especially given out when in use, can effectively remove peculiar smell in oral cavity, maintains oral health.
Description
Technical field
The invention belongs to toothpaste processing technique field, and in particular to rosemary toothpaste and preparation method thereof.
Background technology
Rosemary (Rosmarinus officinalis) is Labiatae shrub, the entitled Rosemary of English, originates in ground
Middle sea basin, the Spain northwestward and Portugal.Stem, leaf, the fragrance of a flower gas of rosemary are strong, refresh the mind, strengthen memory,
The effect of stimulating circulation, there is therapeutic action to nerve, digestion and respiratory disease；Europe in eruption and prevalence disease,
Often burned in hospital to sterilize and purify air；Mole people thinks rosemary energy pest repelling, therefore is largely planted around orchard
Kind rosemary.Visible above, utilization history of the people to rosemary is very long.Modern study shows that rosemary contains
The various active compositions such as monoterpene, sequiterpene, diterpene, triterpene, flavones, aliphatic acid, multibranched paraffin, boots matter and amino acid,
Separation identifies 5 kinds of diterpene and diterpene-kind compound from rosemary root；Separated from cauline leaf and identify 29 flavones
Class compound, 12 kinds of Phenolic Diterpenoids, 3 kinds of diterpene-kind compounds.Therefore, rosemary has benefited from the various active that it is rich in
Material, its develop scope just constantly widened, as rosemary essence can be used for spices, air freshener, driving ants and
The daily-use chemical industry industry such as sterilization, desinsection.
Toothpaste is the cleaning supplies commonly used in daily life, there is very long history.With the continuous hair of science and technology
Exhibition, technological equipment update and it is perfect, various types of toothpaste are come out one after another, and the quality and class of product improve constantly,
Present toothpaste variety develops into great variety of goods, vdiverse in function by single clean type toothpaste, individual brands up to a hundred it is multi-functional
Type toothpaste, meet the needs of the different levels level of consumption.Prior art has been disclosed using Rosmarinus officinalis extract as raw material, for making
Standby mouth sprays, Dentrifice composition etc..Planted as Chinese patent (application number 200510010952.2) discloses containing rosemary
The mouth sprays of thing extract, Rosemary Oil or other rosemary extracts are configured to molten by it in proportion with ethanol and auxiliary material
Liquid, and add the essence of suitable concentration, preservative is auxiliary material.Such as Chinese patent (please number 200580048033.2) dentifrice combination
Add the Rosmarinus officinalis extract containing a large amount of ursolic acid and carnosic acid in thing thus using when be discharged into the amount in oral cavity can be effective
Produce antibacterial, anti-oxidant and/or antiphlogistic effects.Although Rosmarinus officinalis extract or its active ingredient are used to make by above-mentioned technical proposal
In standby oral cavity daily chemical product, but only it is intended merely to play the health-care efficacy of itself such as rosemary antibacterial, anti-oxidant, and for most
For whole oral cavity daily chemical product, its product does not have the advantage of uniqueness, is easily replaced by the more preferable product of other health-care effects
Generation.
The content of the invention
In view of the above-mentioned problems, it is an object of the invention to provide a kind of rosemary toothpaste and preparation method thereof.Present invention fan
Repeatedly fragrant toothpaste uses the rosemary biologically active prod of variform as raw material, and is equipped with dandelion extract, Baical Skullcap root P.E, surpasses
Miniaturization ozone tea oil etc. is raw material, product is protruded in the effect of antibacterial, anti-inflammatory fermentation, and product has rosemary special
Flavor；In addition, the lotion of the toothpaste prepared using the inventive method is uniform, fine and smooth, fan is especially given out when in use and is changed
Fragrant delicate fragrance, peculiar smell in oral cavity can be effectively removed, maintain oral health.
Technical solution of the present invention is as follows.
Rosemary toothpaste, it is characterised in that raw material is：20~45 parts of calcium carbonate, 0.5~1 part of sodium cellulose glycolate, the moon
1~3 part of cinnamic alcohol sodium sulfovinate, 12~20 parts of sorbierite, 1~3 part of honey, 0.5~1 part of pigment, dandelion extract 0.5~3
Part, 0.5~2 part of Baical Skullcap root P.E, 2~5 parts of tea oil, 0.5~5 part of Rosmarinus officinalis extract, 0.5~2 part of Rosemary Oil, fan changes
2~5 parts of cus-cus stem powder, 10~30 parts of rosemary hydrosol；The Rosmarinus officinalis extract is by weight containing 5%~15% black bearberry
Acid and 8~15% carnosic acid；The Rosemary Oil contains 30%~50% 1,8- Cineoles and 10%- by weight
30% australene；The rosemary hydrosol is prepared using following methods：Take rosemary fresh leaf and rosemary fresh flower by weight
5:0.5~1 mixing, and in less than -35 DEG C 10~36h of pre-freeze, Freezing smashing to granularity is 40~100 mesh afterwards, then by material
Liquid weight is than 1:5~15kg/kg is added containing 0.25%~0.5% (weight) vitamin C, 0.5%~1% (weight) citric acid
Distilled water is evaporated under reduced pressure, and is collected the aqueous solution distillated and is produced rosemary hydrosol；The rosemary rhizome powder is rosemary
After crushing, addition pectase, the mixed enzyme solution of cellulase are digested new fresh quench stem, and enzymolysis terminates rear centrifuging and taking supernatant
Spray drying gained；In above-mentioned raw materials, ursolic acid that Rosmarinus officinalis extract contains, carnosic acid make tooth paste product have antibacterial,
Anti-inflammatory, anti-oxidant, anti-aging effect, while dandelion extract, Baical Skullcap root P.E are to common oral inflammation, tooth disease
Disease has good therapeutic action；Rosemary hydrosol is using rosemary fresh leaf and rosemary fresh flower as raw material, the fragrance rich in rosemary
Composition, and prepared using Freezing smashing and the distillation that is concentrated under reduced pressure, it can preferably retain original delicate fragrance of rosemary, additionally by
Distilled water adds vitamin C and protected, add the pH of appropriate citric acid regulation distilled water with accelerate to soften rosemary fresh leaf with
Rosemary fresh flower, the dissolution of active material in raw material, the rosemary liquid distilled from honeysuckle flowers or lotus leaves of preparation and the distillation side of product can be facilitated and speeded up
Formula is compared, and it contains more active ingredients and aroma-producing substance, has stronger rosemary flavor；Rosemary rhizome powder leads to
After crossing enzymolysis, the cellulose rich in small molecule is not soluble in water, and will not be absorbed in oral cavity, alternative tooth paste product inside points
Rubbing agent uses, and increases the health degree of product.
As optimal technical scheme, the raw material is：30 parts of calcium carbonate, 0.75 part of sodium cellulose glycolate, laruyl alcohol sulphur
2 parts of acid esters sodium, 15 parts of sorbierite, 2 parts of honey, 0.75 part of pigment, 2 parts of dandelion extract, 1 part of Baical Skullcap root P.E, tea oil 3
Part, 2 parts of Rosmarinus officinalis extract, 1 part of Rosemary Oil, 2 parts of rosemary rhizome powder, 20 parts of rosemary hydrosol.
As optimal technical scheme, the Rosmarinus officinalis extract is the stem of rosemary, leaf through drying, crushing, extraction, mistake
After filter, concentration, take concentrate to add cyclodextrine and be well mixed, be made by being spray-dried；The dandelion extract is Pu
The leaf of public English takes concentrate to add cyclodextrine and is well mixed after drying, crushing, extraction, filtering, concentration, dry by spraying
It is dry to be made；The Baical Skullcap root P.E for radix scutellariae root after drying, crushing, extraction, filtering, concentration, take concentrate add ring-type
Dextrin is well mixed, and is made by being spray-dried；In above-mentioned raw materials, Rosmarinus officinalis extract, dandelion extract, Baical Skullcap root P.E
Embedded using spray drying process, the active ingredient in rosemary, dandelion, radix scutellariae can be wrapped up protection, can avoided
Active component is by considerable damage and loss during subsequently preparing toothpaste.
As optimal technical scheme, the tea oil is micronization ozone tea oil, i.e., tea oil is first passed through into nanometer ram machine
In 150~180MPa processing, its granularity is less than 100nm, after being passed through ozone in tea oil, ozone intake is with tea oil weight
It is calculated as 2~5g/kg；In order to further enhance the antibacterial of tooth paste product, antiinflammation, pass through ultra micro as the tea oil that raw material uses
Particle diameter is greatly reduced after thin processing, the enhancing of product mobility, and moisturizing, anti-inflammatory, the bactericidal action of tea oil are more preferable；Because ozone is in list
There is preferable dissolubility, especially tea oil after ultra tiny processing in unrighted acid, the dissolubility of ozone significantly carries
Rise, therefore drop ozone can be passed through tea oil, the anti-inflammatory bactericidal effect of tea oil can be strengthened.
The preparation method of rosemary toothpaste, comprises the following steps：
1) by sodium cellulose glycolate, sorbierite, honey, rosemary hydrosol, dandelion extract, Baical Skullcap root P.E, fan
Repeatedly fragrant extract carries out high-speed stirred mixing, carry out afterwards it is high-pressure homogeneous, homogeneous terminate after using nanometer ram machine in pressure 120
~180MPa carries out ultra high pressure treatment, and handling 2~4 times repeatedly makes its granularity be below 300nm, is placed in supersonic wave cleaning machine afterwards
It is interior, 10~30min is handled under conditions of 200~400W of power, 40~60Hz of frequency；Above-mentioned raw materials first pass through it is high-pressure homogeneous,
Ultra high pressure treatment is carried out by nanometer ram machine again, the particle diameter that can make to obtain material is in nanoscale, makes to be formed uniform, fine and smooth
Intermediate products, the generation of bubble can also be reduced in addition；Further material is handled using ultrasonic wave, can thoroughly be gone
Except the residual bubbles in material, the difficulty that subsequent technique eliminates bubble is reduced；
2) material that step (1) obtains is pumped into vacuum cream tank, then sequentially adds calcium carbonate, bay alcohol sulfuric ester
Sodium, rosemary rhizome powder, 60~70 DEG C of tea oil is preheated to, carries out high-speed stirred mixing, stop stirring in vacuum afterwards
20~60min of vacuum outgas is carried out under conditions of 0.90~0.98MPa；
3) pigment, Rosemary Oil is sequentially added in the material obtained after step (2) vacuum outgas, and are stirred
It is even, it is placed in afterwards in supersonic wave cleaning machine, 10~30min is handled under conditions of 200~400W of power, 40~60Hz of frequency；
Because Rosemary Oil is small molecule volatile substances, therefore adds Rosemary Oil in final step and be stirred mixing
It is even, and by ultrasonication slough whipping process formed bubble；
4) material for obtaining step (3) carries out sterile filling.
Beneficial effect of the present invention：
1) Rosmarinus officinalis extract, rosemary hydrosol, rosemary rhizome powder etc. is used to prepare toothpaste for raw material, what product contained
The species of rosemary active material is more and enriches, and especially finished product has the special fragrant of plant rosemary；In addition, product
It is raw material to have used Baical Skullcap root P.E, dandelion extract, micronization ozone tea oil etc., make product have prominent antibacterial,
The effect of anti-inflammatory, there is the effect of fine for patients such as mouth disease, periodontal diseases.
2) preparation technology of product carries out ultra high pressure treatment using nanometer ram machine, and is deaerated by too many levels, multimode,
The product finally prepared is fine and smooth, uniform, and usage experience sense is good, especially gives out the delicate fragrance of rosemary, Ke Yiyou when in use
Peculiar smell in the removal oral cavity of effect, maintain oral health.
Embodiment
With reference to embodiment, the present invention is described further, it is pointed out that implementation below is only
It is the indicative explaination done in the form of enumerating to the present invention, but protection scope of the present invention is not limited to that, Suo Youben
The equivalent replacement that the technical staff in field is done with the spirit of the present invention to the present invention each falls within protection scope of the present invention.
Embodiment 1
Rosemary toothpaste, raw material are：20~45 parts of calcium carbonate, 0.5~1 part of sodium cellulose glycolate, bay alcohol sulfuric ester
1~3 part of sodium, 12~20 parts of sorbierite, 1~3 part of honey, 0.5~1 part of pigment, 0.5~3 part of dandelion extract, radix scutellariae extraction
0.5~2 part of thing, 2~5 parts of tea oil, 0.5~5 part of Rosmarinus officinalis extract, 0.5~2 part of Rosemary Oil, rosemary rhizome powder 2~
5 parts, 10~30 parts of rosemary hydrosol；The Rosmarinus officinalis extract is by weight containing 5%~15% ursolic acid and 8~15%
Carnosic acid；The Rosemary Oil contains 30%~50% 1,8- Cineoles and 10%-30% australene by weight；
The rosemary hydrosol is prepared using following methods：Take rosemary fresh leaf with rosemary fresh flower by weight 5:0.5~1 mixing,
And in less than -35 DEG C 10~36h of pre-freeze, Freezing smashing to granularity is 40~100 mesh afterwards, then by feed liquid weight than 1:5~
15kg/kg adds to be subtracted containing 0.25%~0.5% (weight) vitamin C, the distilled water of 0.5%~1% (weight) citric acid
Pressure distillation, collects the aqueous solution distillated and produces rosemary hydrosol；The rosemary rhizome powder is broken for the new fresh quench stem warp of rosemary
After broken, addition pectase, the mixed enzyme solution of cellulase are digested, and enzymolysis terminates rear centrifuging and taking supernatant spray drying institute
.
Embodiment 2
Rosemary toothpaste, raw material are：20 parts of calcium carbonate, 0.5 part of sodium cellulose glycolate, 1 part of laruyl alcohol sodium sulfovinate, mountain
20 parts of pears alcohol, 3 parts of honey, 0.5 part of pigment, 0.5 part of dandelion extract, 0.5 part of Baical Skullcap root P.E, 2 parts of tea oil, rosemary carries
Take 5 parts of thing, 2 parts of Rosemary Oil, 5 parts of rosemary rhizome powder, 30 parts of rosemary hydrosol；The Rosmarinus officinalis extract is by weight
Carnosic acid containing 5%~15% ursolic acid and 8~15%；The Rosemary Oil is by weight containing 30%~50%
The australene of 1,8- Cineoles and 10%-30%；The rosemary hydrosol is prepared using following methods：Take rosemary fresh leaf and fan
Repeatedly fragrant fresh flower is by weight 5:0.5~1 mixing, and in less than -35 DEG C 10~36h of pre-freeze, Freezing smashing to granularity is 40 afterwards
~100 mesh, then by feed liquid weight than 1:5~15kg/kg add containing 0.25%~0.5% (weight) vitamin C, 0.5%~
The distilled water of 1% (weight) citric acid is evaporated under reduced pressure, and is collected the aqueous solution distillated and is produced rosemary hydrosol；The rosemary
Rhizome powder for rosemary new fresh quench stem after crushing, add pectase, the mixed enzyme solution of cellulase and digested, enzymolysis knot
Centrifuging and taking supernatant spray drying gained after beam.
Embodiment 3
Rosemary toothpaste, raw material are：45 parts of calcium carbonate, 1 part of sodium cellulose glycolate, 3 parts of laruyl alcohol sodium sulfovinate, sorb
12 parts of alcohol, 13 parts of honey, 1 part of pigment, 3 parts of dandelion extract, 2 parts of Baical Skullcap root P.E, 5 parts of tea oil, Rosmarinus officinalis extract 0.5
Part, 0.5 part of Rosemary Oil, 2 parts of rosemary rhizome powder, 10 parts of rosemary hydrosol；The Rosmarinus officinalis extract contains by weight
There are 5%~15% ursolic acid and 8~15% carnosic acid；The Rosemary Oil contains the 1 of 30%~50% by weight,
The australene of 8- Cineoles and 10%-30%；The rosemary hydrosol is prepared using following methods：Rosemary fresh leaf is taken to be changed with fan
Fragrant fresh flower is by weight 5:0.5~1 mixing, and in less than -35 DEG C 10~36h of pre-freeze, afterwards Freezing smashing to granularity for 40~
100 mesh, then by feed liquid weight than 1:5~15kg/kg is added containing 0.25%~0.5% (weight) vitamin C, 0.5%~1%
The distilled water of (weight) citric acid is evaporated under reduced pressure, and is collected the aqueous solution distillated and is produced rosemary hydrosol；The rosemary root
Stem powder for rosemary new fresh quench stem after crushing, add pectase, the mixed enzyme solution of cellulase and digested, enzymolysis terminates
Centrifuging and taking supernatant spray drying gained afterwards.
Embodiment 4
Rosemary toothpaste, raw material are：30 parts of calcium carbonate, 0.75 part of sodium cellulose glycolate, 2 parts of laruyl alcohol sodium sulfovinate,
15 parts of sorbierite, 2 parts of honey, 0.75 part of pigment, 2 parts of dandelion extract, 1 part of Baical Skullcap root P.E, 3 parts of tea oil, rosemary carries
Take 2 parts of thing, 1 part of Rosemary Oil, 2 parts of rosemary rhizome powder, 20 parts of rosemary hydrosol；The Rosmarinus officinalis extract is by weight
Carnosic acid containing 5%~15% ursolic acid and 8~15%；The Rosemary Oil is by weight containing 30%~50%
The australene of 1,8- Cineoles and 10%-30%；The rosemary hydrosol is prepared using following methods：Take rosemary fresh leaf and fan
Repeatedly fragrant fresh flower is by weight 5:0.5~1 mixing, and in less than -35 DEG C 10~36h of pre-freeze, Freezing smashing to granularity is 40 afterwards
~100 mesh, then by feed liquid weight than 1:5~15kg/kg add containing 0.25%~0.5% (weight) vitamin C, 0.5%~
The distilled water of 1% (weight) citric acid is evaporated under reduced pressure, and is collected the aqueous solution distillated and is produced rosemary hydrosol；The rosemary
Rhizome powder for rosemary new fresh quench stem after crushing, add pectase, the mixed enzyme solution of cellulase and digested, enzymolysis knot
Centrifuging and taking supernatant spray drying gained after beam.
Embodiment 5
Rosemary toothpaste, raw material are：20~45 parts of calcium carbonate, 0.5~1 part of sodium cellulose glycolate, bay alcohol sulfuric ester
1~3 part of sodium, 12~20 parts of sorbierite, 1~3 part of honey, 0.5~1 part of pigment, 0.5~3 part of dandelion extract, radix scutellariae extraction
0.5~2 part of thing, 2~5 parts of tea oil, 0.5~5 part of Rosmarinus officinalis extract, 0.5~2 part of Rosemary Oil, rosemary rhizome powder 2~
5 parts, 10~30 parts of rosemary hydrosol；The Rosmarinus officinalis extract is by weight containing 5%~15% ursolic acid and 8~15%
Carnosic acid；The Rosemary Oil contains 30%~50% 1,8- Cineoles and 10%-30% australene by weight；
The rosemary hydrosol is prepared using following methods：Take rosemary fresh leaf with rosemary fresh flower by weight 5:0.5~1 mixing,
And in less than -35 DEG C 10~36h of pre-freeze, Freezing smashing to granularity is 40~100 mesh afterwards, then by feed liquid weight than 1:5~
15kg/kg adds to be subtracted containing 0.25%~0.5% (weight) vitamin C, the distilled water of 0.5%~1% (weight) citric acid
Pressure distillation, collects the aqueous solution distillated and produces rosemary hydrosol；The rosemary rhizome powder is broken for the new fresh quench stem warp of rosemary
After broken, addition pectase, the mixed enzyme solution of cellulase are digested, and enzymolysis terminates rear centrifuging and taking supernatant spray drying institute
；The Rosmarinus officinalis extract is the stem of rosemary, leaf after drying, crushing, extraction, filtering, concentration, take concentrate to add ring
Shape dextrin is well mixed, and is made by being spray-dried；The dandelion extract for dandelion leaf through drying, crushing, extraction,
After filtering, concentration, take concentrate to add cyclodextrine and be well mixed, be made by being spray-dried；The Baical Skullcap root P.E is Huang
The root of a kind of reed mentioned in ancient books takes concentrate to add cyclodextrine and is well mixed, pass through spray drying after drying, crushing, extraction, filtering, concentration
It is made；
Embodiment 5
Rosemary toothpaste, raw material are：20~45 parts of calcium carbonate, 0.5~1 part of sodium cellulose glycolate, bay alcohol sulfuric ester
1~3 part of sodium, 12~20 parts of sorbierite, 1~3 part of honey, 0.5~1 part of pigment, 0.5~3 part of dandelion extract, radix scutellariae extraction
0.5~2 part of thing, 2~5 parts of tea oil, 0.5~5 part of Rosmarinus officinalis extract, 0.5~2 part of Rosemary Oil, rosemary rhizome powder 2~
5 parts, 10~30 parts of rosemary hydrosol；The Rosmarinus officinalis extract is by weight containing 5%~15% ursolic acid and 8~15%
Carnosic acid；The Rosemary Oil contains 30%~50% 1,8- Cineoles and 10%-30% australene by weight；
The rosemary hydrosol is prepared using following methods：Take rosemary fresh leaf with rosemary fresh flower by weight 5:0.5~1 mixing,
And in less than -35 DEG C 10~36h of pre-freeze, Freezing smashing to granularity is 40~100 mesh afterwards, then by feed liquid weight than 1:5~
15kg/kg adds to be subtracted containing 0.25%~0.5% (weight) vitamin C, the distilled water of 0.5%~1% (weight) citric acid
Pressure distillation, collects the aqueous solution distillated and produces rosemary hydrosol；The rosemary rhizome powder is broken for the new fresh quench stem warp of rosemary
After broken, addition pectase, the mixed enzyme solution of cellulase are digested, and enzymolysis terminates rear centrifuging and taking supernatant spray drying institute
；The tea oil is micronization ozone tea oil, i.e., tea oil is first passed through into nanometer ram machine in 150~180MPa processing, make it
Granularity is less than 100nm, after being passed through ozone in tea oil, ozone intake is calculated as 2~5g/kg with tea oil weight.
Embodiment 6
1) by sodium cellulose glycolate, sorbierite, honey, rosemary hydrosol, dandelion extract, Baical Skullcap root P.E, fan
Repeatedly fragrant extract carries out high-speed stirred mixing, carry out afterwards it is high-pressure homogeneous, homogeneous terminate after using nanometer ram machine in pressure 120
~180MPa carries out ultra high pressure treatment, and handling 2~4 times repeatedly makes its granularity be below 300nm, is placed in supersonic wave cleaning machine afterwards
It is interior, 10~30min is handled under conditions of 200~400W of power, 40~60Hz of frequency；
2) material that step (1) obtains is pumped into vacuum cream tank, then sequentially adds calcium carbonate, bay alcohol sulfuric ester
Sodium, rosemary rhizome powder, 60~70 DEG C of tea oil is preheated to, carries out high-speed stirred mixing, stop stirring in vacuum afterwards
20~60min of vacuum outgas is carried out under conditions of 0.90~0.98MPa；
3) pigment, Rosemary Oil is sequentially added in the material obtained after step (2) vacuum outgas, and are stirred
It is even, it is placed in afterwards in supersonic wave cleaning machine, 10~30min is handled under conditions of 200~400W of power, 40~60Hz of frequency；
4) material for obtaining step (3) carries out sterile filling.
Claims (7)
1. rosemary toothpaste, it is characterised in that raw material is：20~45 parts of calcium carbonate, 0.5~1 part of sodium cellulose glycolate, bay
1~3 part of alcohol sulfuric ester sodium, 12~20 parts of sorbierite, 1~3 part of honey, 0.5~1 part of pigment, 0.5~3 part of dandelion extract,
0.5~2 part of Baical Skullcap root P.E, 2~5 parts of tea oil, 0.5~5 part of Rosmarinus officinalis extract, 0.5~2 part of Rosemary Oil, rosemary
2~5 parts of rhizome powder, 10~30 parts of rosemary hydrosol；The Rosmarinus officinalis extract is by weight containing 5%~15% ursolic acid
With 8~15% carnosic acid；The Rosemary Oil by weight containing 30%~50% 1,8- Cineoles and 10%~
30% australene；The rosemary hydrosol is prepared using following methods：Take rosemary fresh leaf and rosemary fresh flower by weight
5:0.5~1 mixing, and in less than -35 DEG C 10~36h of pre-freeze, Freezing smashing to granularity is 40~100 mesh afterwards, then by material
Liquid weight is than 1:5~15kg/kg is added containing 0.25%~0.5% (weight) vitamin C, 0.5%~1% (weight) citric acid
Distilled water is evaporated under reduced pressure, and is collected the aqueous solution distillated and is produced rosemary hydrosol；The rosemary rhizome powder is rosemary
After crushing, addition pectase, the mixed enzyme solution of cellulase are digested new fresh quench stem, and enzymolysis terminates rear centrifuging and taking supernatant
Spray drying gained.
2. rosemary toothpaste as claimed in claim 1, it is characterised in that raw material is：30 parts of calcium carbonate, sodium cellulose glycolate
0.75 part, 2 parts of laruyl alcohol sodium sulfovinate, 15 parts of sorbierite, 2 parts of honey, 0.75 part of pigment, 2 parts of dandelion extract, radix scutellariae carries
Take 1 part of thing, 3 parts of tea oil, 2 parts of Rosmarinus officinalis extract, 1 part of Rosemary Oil, 2 parts of rosemary rhizome powder, 20 parts of rosemary hydrosol.
3. the rosemary toothpaste as described in claim 1~2 is any, it is characterised in that the Rosmarinus officinalis extract is rosemary
Stem, leaf take concentrate to add cyclodextrine and are well mixed, made by being spray-dried after drying, crushing, extraction, filtering, concentration
.
4. the rosemary toothpaste as described in claim 1~2 is any, it is characterised in that the dandelion extract is dandelion
Ye Jing is dry, crushes, extracts, filtering, after concentration, takes concentrate to add cyclodextrine and is well mixed, obtained by being spray-dried.
5. the rosemary toothpaste as described in claim 1~2 is any, it is characterised in that the Baical Skullcap root P.E passes through for the root of radix scutellariae
Dry, crush, extracting, filtering, after concentration, taking concentrate to add cyclodextrine and be well mixed, it is obtained by being spray-dried.
6. the rosemary toothpaste as described in claim 1~2 is any, it is characterised in that the tea oil is micronization ozone tea
Oil, i.e., tea oil is first passed through into nanometer ram machine in 150~180MPa processing, its granularity is less than 100nm, after leading in tea oil
Enter ozone, ozone intake is calculated as 2~5g/kg with tea oil weight.
7. the preparation method of rosemary toothpaste, it is characterised in that comprise the following steps：
1) by sodium cellulose glycolate, sorbierite, honey, rosemary hydrosol, dandelion extract, Baical Skullcap root P.E, rosemary
Extract carry out high-speed stirred mixing, carry out afterwards it is high-pressure homogeneous, homogeneous terminate after using nanometer ram machine in pressure 120~
180MPa carries out ultra high pressure treatment, and handling 2~4 times repeatedly makes its granularity be below 300nm, is placed in supersonic wave cleaning machine afterwards
It is interior, 10~30min is handled under conditions of 200~400W of power, 40~60Hz of frequency；
2) material that step (1) obtains is pumped into vacuum cream tank, then sequentially add calcium carbonate, laruyl alcohol sodium sulfovinate,
Rosemary rhizome powder, is preheated to 60~70 DEG C of tea oil, carries out high-speed stirred mixing, stop stirring afterwards in vacuum 0.90~
20~60min of vacuum outgas is carried out under conditions of 0.98MPa；
3) pigment, Rosemary Oil is sequentially added in the material obtained after step (2) vacuum outgas, and is uniformly mixed,
It is placed in afterwards in supersonic wave cleaning machine, 10~30min is handled under conditions of 200~400W of power, 40~60Hz of frequency；
4) material for obtaining step (3) carries out sterile filling.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711283682.1A CN107802579A (en) | 2017-12-06 | 2017-12-06 | Rosemary toothpaste and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711283682.1A CN107802579A (en) | 2017-12-06 | 2017-12-06 | Rosemary toothpaste and preparation method thereof |
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| CN107802579A true CN107802579A (en) | 2018-03-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201711283682.1A Pending CN107802579A (en) | 2017-12-06 | 2017-12-06 | Rosemary toothpaste and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114557932A (en) * | 2022-03-03 | 2022-05-31 | 李时珍医药集团有限公司 | Toothpaste containing folium artemisiae argyi and rosemary leaf extracts and preparation method thereof |
| CN114681382A (en) * | 2022-05-07 | 2022-07-01 | 云南花王生物科技有限公司 | Flower toothpaste and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101115531A (en) * | 2004-12-17 | 2008-01-30 | 高露洁-棕榄公司 | Oral compositions containing extracts of rosmarinus and related methods |
| CN106929153A (en) * | 2016-04-29 | 2017-07-07 | 深圳市大百汇技术有限公司 | A kind of preparation method and applications of rosemary hydrosol |
| US20170224609A1 (en) * | 2004-12-29 | 2017-08-10 | Evangelia S. Arvanitidou | Oxidation resistant dentifrice compositions |
| CN107028816A (en) * | 2017-06-08 | 2017-08-11 | 安徽嘉宝诺生物科技有限公司 | Ozone vegetable oil emulsifier composition for toothpaste and preparation method thereof |
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2017
- 2017-12-06 CN CN201711283682.1A patent/CN107802579A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101115531A (en) * | 2004-12-17 | 2008-01-30 | 高露洁-棕榄公司 | Oral compositions containing extracts of rosmarinus and related methods |
| US20170224609A1 (en) * | 2004-12-29 | 2017-08-10 | Evangelia S. Arvanitidou | Oxidation resistant dentifrice compositions |
| CN106929153A (en) * | 2016-04-29 | 2017-07-07 | 深圳市大百汇技术有限公司 | A kind of preparation method and applications of rosemary hydrosol |
| CN107028816A (en) * | 2017-06-08 | 2017-08-11 | 安徽嘉宝诺生物科技有限公司 | Ozone vegetable oil emulsifier composition for toothpaste and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114557932A (en) * | 2022-03-03 | 2022-05-31 | 李时珍医药集团有限公司 | Toothpaste containing folium artemisiae argyi and rosemary leaf extracts and preparation method thereof |
| CN114681382A (en) * | 2022-05-07 | 2022-07-01 | 云南花王生物科技有限公司 | Flower toothpaste and preparation method thereof |
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Application publication date: 20180316 |