CN110227056A - A kind of propolis oral cleansing lotion and preparation method thereof - Google Patents

A kind of propolis oral cleansing lotion and preparation method thereof Download PDF

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Publication number
CN110227056A
CN110227056A CN201910684954.1A CN201910684954A CN110227056A CN 110227056 A CN110227056 A CN 110227056A CN 201910684954 A CN201910684954 A CN 201910684954A CN 110227056 A CN110227056 A CN 110227056A
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propolis
acid
peppermint
oral cleansing
cleansing lotion
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CN201910684954.1A
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Chinese (zh)
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陆群芳
裴文
沈忱
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Huzhou Tianbaozhen Biotechnology Co Ltd
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Huzhou Tianbaozhen Biotechnology Co Ltd
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Priority to CN201910684954.1A priority Critical patent/CN110227056A/en
Publication of CN110227056A publication Critical patent/CN110227056A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/362Polycarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/368Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/732Starch; Amylose; Amylopectin; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/524Preservatives

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Zoology (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Jellies, Jams, And Syrups (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of propolis oral cleansing lotions and preparation method thereof, the propolis oral cleansing lotion is prepared by propolis alcohol extract, honey, peppermint alcohol extracting thing, sweetener, acid and preservative, propolis alcohol extract is that propolis is extracted through edible ethanol, then is made into the propolis alcohol extract that propolis mass concentration is 10~20% with edible ethanol;Peppermint alcohol extracting thing is that peppermint extracts to obtain through edible ethanol, is first made into the peppermint alcohol extract that menthol extract quality concentration is 1~10% with distilled water using preceding;Honey, peppermint alcohol extracting thing, sweetener, acid and preservative quality dosage be respectively 5~15%, 1~5%, 10~15%, 5~10% and 0.5~1% of propolis quality dosage in propolis alcohol extract;The pH value of the propolis oral cleansing lotion is 3~8.The oral cleansing lotion is integrally in good taste, nonirritant, can be liked and be received by the majority of consumers.

Description

A kind of propolis oral cleansing lotion and preparation method thereof
Technical field
The present invention relates to a kind of propolis oral cleansing lotions and preparation method thereof.
Background technique
Propolis is honeybee herborization resin, is mixed into its glandula secretion, beeswax and pollen etc., is process through chewing A kind of viscous substance, wherein containing the multiple compounds such as flavones, fatty acid, aromatic acid, alcohol, aldehyde, alkene, terpene, furthermore mineral Matter rich content.Propolis has effects that following: 1, bactericidal antiphlogistic is antiviral, eliminates pathogenic microorganism.For bacterium, virus, true Various infection class diseases caused by bacterium, such as tuberculosis, gastritis, bronchitis, skin disease have good effect;2, calm, Nervous system is repaired, insomnia, menopausal syndrome effect are obvious when sedation.Office Shao's anesthetic effect lining toothache, wound only Pain effect is pretty good, while repairing nerve, activates nerve cell, can eliminate diarrhea constipation, numbness in hands and feet, skin are fullyed recover from an illness the diseases such as itch;3, Promote tissue repair effect, Shi Yuqing ulcer, sore, wound effect are rapid.In particular for the elimination of diabetes B lower limb gangrene, even more Compensate for the blank of modern medicine;4, soften blood vessel, improve blood circulation, reduce blood twist and platelet aggregation, bidirectional modulation Blood stake, blood pressure, the dry indices of blood lipid;5, liver protection, protect liver, solution liver poison, can be effectively reduced the third paddy and turn atmosphere enzyme;6, enhance body Anti-tumor capacity;7, free radical is removed, artery sclerosis is stopped by team, the plurality kinds of health care function such as increase immunity of organisms, promotion regeneration Effect.Flavonoid substances in propolis are one of main actives of propolis, and healthcare function and clinical treatment effect are just gradually Recognized and paid close attention to by people.
With the improvement of people ' s living standards and the movable increase of social interactions, chewing gum receive people one period Welcome and use.But whether chewing gum can have an impact to the health of oral cavity and tooth, people produce query.In addition, Residue after chewing-gum chewing is thrown out without care by people, affects the beauty of environment.Therefore, oral cleansing lotion has obtained people in recent years Favor.Propolis has clinically been used widely as anti-inflammatory preparation and preparation for callouse mouth disease, propolis mouth Chamber freshener has been subjected to domestic and international market and the welcome of consumer.But propolis smell is heavier, there is certain stimulation to oral cavity Effect, part propolis extract is easily adhered in tooth or oral cavity, so as to cause a part of consumer groups in use by Certain restrictions.Therefore, it is necessary to be adjusted and improve to process recipe.
Summary of the invention
It is nonirritant the technical problem to be solved by the invention is to provide a kind of in good taste, it can be liked by the majority of consumers Love and the novel propolis oral cleansing lotion received and preparation method thereof.
In order to solve the above technical problems, the present invention discloses a kind of propolis oral cleansing lotion first, the propolis oral cavity fresh and cool Agent is prepared by propolis alcohol extract, honey, peppermint alcohol extracting thing, sweetener, acid and preservative,
The propolis alcohol extract is that propolis is extracted through edible ethanol, then being made into propolis mass concentration with edible ethanol is 10 ~20% propolis alcohol extract;The peppermint alcohol extracting thing is that peppermint extracts to obtain through edible ethanol, using preceding first with distillation Water is made into the peppermint alcohol extract that menthol extract quality concentration is 1~10%;
The honey, peppermint alcohol extracting thing, sweetener, acid and preservative quality dosage be respectively propolis alcohol extracting 5~15%, 1~5%, 10~15%, 5~10% and the 0.5~1% of propolis quality dosage in liquid;
The pH value of the propolis oral cleansing lotion is 3~8.
Further, the sweetener is glucose, fructose, sucrose, maltose, starch sugar, lactose, stevioside, Radix Glycyrrhizae The mixing of one or more of acid disodium, tripotassium glycyrrhetate or trisodium glycyrrhetinate.
Further, the acid is citric acid, lactic acid, tartaric acid, malic acid, acetic acid, adipic acid, fumaric acid, lemon The mixing of one or more of lemon acid sodium or citric acid tri potassium.
Further, the preservative is benzoic acid or sorbic acid.
Further, the honey is commodity honey, i.e. commercial product.
The invention also discloses a kind of preparation method of aforementioned propolis oral cleansing lotion, this method includes
(1), it prepares propolis alcohol extract: propolis and edible ethanol, stirring, in 10~100 DEG C of temperature being added in container Under, extract 50~100 hours, after filtered, then it is 10~20% spare for being adjusted to propolis mass concentration with edible ethanol;Not Extracted propolis, contains impurity;
(2), it prepares mint extract: after peppermint crushes, being placed in container and stir, after being extracted 5 hours at a temperature of 30 DEG C, Filtering, obtains mint extract, then with distilled water to be made into the peppermint extracting solution that mint extract mass concentration is 1~10% spare; The peppermint directlys adopt natural plants;
(3), propolis alcohol extract, honey, peppermint alcohol extract, sweetener, acid and preservative is weighed in proportion to exist It is uniformly mixed in container, then with acid tune pH value to 3~8, filters and propolis oral cleansing lotion is made.
Further, edible ethanol mass concentration used is 70% in step (1), the weight of propolis used and the edible ethanol Amount is than being 1:5~10.
Further, propolis first progress Freezing smashing processing before extraction used in step (1).
Further, edible ethanol mass concentration used is 70% in step (2), the weight of peppermint used and the edible ethanol Amount is than being 1:1~3.
The present invention extends the extraction time to propolis, is added to acid and sweetener, improves propolis to oral cavity Irritation.Due to being added to acid, adjusts the pH value of mouthwass with can be convenient, has effectively acted as antisepsis, The antibacterial effect of the preservatives such as benzoic acid, sorbic acid is increased again.It is whole in good taste, it is nonirritant, it can be by the majority of consumers Like and receives.
Specific embodiment
Below with reference to embodiment, more specifically the elaboration contents of the present invention.Implementation of the invention is not limited to following reality Example is applied, the accommodation in any form made to the present invention or changed all should be within the scope of the present invention.
The preparation of 1 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 1000 milliliters of flask, the edible second that mass concentration is 70% is added 500 grams of alcohol, 10 DEG C at a temperature of, extract 100 hours, filtering, it is spare to be adjusted to propolis mass concentration 10% with edible ethanol.
The preparation of 2 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 1000 milliliters of flask, the edible second that mass concentration is 70% is added 250 grams of alcohol, 30 DEG C at a temperature of, extract 50 hours, filtering, it is spare to be adjusted to propolis mass concentration 20% with edible ethanol.
The preparation of 3 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 1000 milliliters of flask, the edible second that mass concentration is 70% is added 300 grams of alcohol, 100 DEG C at a temperature of, extract 60 hours, filtering, it is spare to be adjusted to propolis mass concentration 15% with edible ethanol.
The preparation of 4 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 1000 milliliters of flask, the edible second that mass concentration is 70% is added 400 grams of alcohol, 50 DEG C at a temperature of, extract 80 hours, filtering, it is spare to be adjusted to propolis mass concentration 10% with edible ethanol.
The preparation of 5 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 3000 milliliters of flask, the edible second that mass concentration is 70% is added 350 grams of alcohol, 80 DEG C at a temperature of, extract 80 hours, filtering, it is spare to be adjusted to propolis mass concentration 14% with edible ethanol.
The preparation of 6 natural plants peppermint alcohol extract of embodiment
Take 50 grams of natural plants peppermint, be put into after crushing in 500 milliliters of flask, be added mass concentration be 70% it is edible 150 grams of ethyl alcohol, 30 DEG C at a temperature of, extract 5 hours, filter to obtain peppermint alcohol extracting thing, be diluted to peppermint alcohol extracting with distilled water Taking amount of substance concentration is 5% spare.
The preparation of 7 peppermint alcohol extract of embodiment
50 grams of peppermint are taken, is put into after crushing in 500 milliliters of flask, the edible ethanol 50 that mass concentration is 70% is added Gram, 30 DEG C at a temperature of, extract 5 hours, filter to obtain peppermint alcohol extracting thing, be diluted to menthol extract quality with distilled water Concentration is 10% spare.
The preparation of 8 peppermint alcohol extract of embodiment
50 grams of peppermint are taken, is put into after crushing in 500 milliliters of flask, the edible ethanol 100 that mass concentration is 70% is added Gram, 30 DEG C at a temperature of, extract 5 hours, filter to obtain peppermint alcohol extracting thing, be diluted to menthol extract quality with distilled water Concentration is 1% spare.
The preparation of 9 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 1, the natural plants peppermint of embodiment 6 10 grams of alcohol extract, 0.5 gram of acid citric acid, 1 gram of sweetener glucose, 0.05 gram of preservative benzoic acid, 1.5 grams of honey, It in the mixing container at a temperature of 30 DEG C, is stirred, after being 3 with acid tune pH value, filters finished product.
The preparation of 10 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 1, the natural plants peppermint of embodiment 6 10 grams of alcohol extract, 0.5 gram of acid lactic acid, 1 gram of sweetener fructose, 0.05 gram of preservative benzoic acid, 1.5 grams of honey, mixed It in conjunction container at a temperature of 30 DEG C, is stirred, after adjusting pH value to be 3, filters finished product.
The preparation of 11 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 2, the natural plants peppermint of embodiment 6 20 grams of alcohol extract, 0.5 gram of acid citric acid, 1.5 grams of malic acid, 1 gram of sweetener glucose, 1 gram of sucrose, 1 gram of lactose, prevent 0.1 gram of rotten agent benzoic acid, in the mixing container at a temperature of 30 DEG C, is stirred by 1 gram of honey, is separately 5 with acid tune pH value Afterwards, finished product is filtered.
The preparation of 12 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 3, the peppermint alcohol extract of embodiment 7 4.5 grams, 0.5 gram of acid tartaric acid, 0.7 gram of citric acid tri potassium, 1 gram of sweetener glucose,Starch sugar0.5 gram, preservative mountain 0.15 gram of pears acid, in the mixing container at a temperature of 30 DEG C, is stirred by 0.75 gram of honey, after being separately 8 with acid tune pH value, Filter finished product.
The preparation of 13 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 4, the peppermint alcohol extract of embodiment 8 50 grams, 0.5 gram of acid adipic acid, 1 gram of sweetener stevioside, 0.05 gram of preservative benzoic acid, 1.5 grams of honey, hold in mixing It in device at a temperature of 30 DEG C, is stirred, after being separately 7 with acid tune pH value, filters finished product.
The preparation of 14 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 5, the peppermint alcohol extract of embodiment 8 42 grams, 0.26 gram of acid adipic acid, 0.5 gram of citric acid, 0.5 gram of sodium citrate, 0.68 gram of sweetener stevioside, glycyrrhizic acid three It 1 gram of sodium, 0.07 gram of preservative benzoic acid, 1.4 grams of honey, in the mixing container at a temperature of 30 DEG C, is stirred, separately uses acid After tune pH value is 7, finished product is filtered.
The preparation of 15 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 5, the day peppermint alcohol extracting of embodiment 8 42 grams of liquid, 0.26 gram of acid acetic acid, 0.5 gram of citric acid, 0.5 gram of sodium citrate, 0.68 gram of sweetener tripotassium glycyrrhetate, Radix Glycyrrhizae 1 gram of sour trisodium, 1.4 grams of honey, in the mixing container at a temperature of 30 DEG C, is stirred by 0.07 gram of preservative sorbic acid, another acid After taste agent tune pH value is 6, finished product is filtered.

Claims (9)

1. a kind of propolis oral cleansing lotion, it is characterised in that: the propolis oral cleansing lotion is by propolis alcohol extract, honey, peppermint Alcohol extracting thing, sweetener, acid and preservative are prepared,
The propolis alcohol extract be propolis extracted through edible ethanol, then with edible ethanol be made into propolis mass concentration be 10~ 20% propolis alcohol extract;The peppermint alcohol extracting thing is that peppermint extracts to obtain through edible ethanol, first uses distilled water using preceding It is made into the peppermint alcohol extract that menthol extract quality concentration is 1~10%;
The honey, peppermint alcohol extracting thing, sweetener, acid and preservative quality dosage be respectively in propolis alcohol extract 5~15%, 1~5%, 10~15%, 5~10% and the 0.5~1% of propolis quality dosage;
The pH value of the propolis oral cleansing lotion is 3~8.
2. propolis oral cleansing lotion according to claim 1, it is characterised in that: the sweetener is glucose, fructose, sugarcane One or both of sugar, maltose, starch sugar, lactose, stevioside, disodium glycyrrhizinate, tripotassium glycyrrhetate or trisodium glycyrrhetinate Above mixing.
3. propolis oral cleansing lotion according to claim 1, it is characterised in that: the acid is citric acid, lactic acid, winestone The mixing of one or more of acid, malic acid, acetic acid, adipic acid, fumaric acid, sodium citrate or citric acid tri potassium.
4. propolis oral cleansing lotion according to claim 1, it is characterised in that: the preservative is benzoic acid or sorbic acid.
5. propolis oral cleansing lotion according to claim 1, it is characterised in that: the honey is commodity honey.
6. a kind of preparation method for preparing claim 1-5 any one claim propolis oral cleansing lotion, it is characterised in that: This method includes
(1), it prepares propolis alcohol extract: propolis and edible ethanol being added in container, stirring at a temperature of 10~100 DEG C, mentions Take 50~100 hours, after filtered, then it is 10~20% spare for being adjusted to propolis mass concentration with edible ethanol;
(2), it prepares mint extract: after peppermint crushes, being placed in container and stir, after being extracted 5 hours at a temperature of 30 DEG C, mistake Filter, obtains mint extract, then with distilled water to be made into the peppermint extracting solution that mint extract mass concentration is 1~10% spare;
(3), propolis alcohol extract, honey, peppermint alcohol extract, sweetener, acid and preservative are weighed in proportion in container In be uniformly mixed, then with acid tune pH value to 3~8, filter and propolis oral cleansing lotion be made.
7. the preparation method of propolis oral cleansing lotion according to claim 6, it is characterised in that: used edible in step (1) Ethyl alcohol mass concentration is 70%, and the weight ratio of propolis used and the edible ethanol is 1:5~10.
8. the preparation method of propolis oral cleansing lotion according to claim 6, it is characterised in that: propolis used in step (1) Freezing smashing processing is first carried out before extraction.
9. the preparation method of propolis oral cleansing lotion according to claim 6, it is characterised in that: used edible in step (2) Ethyl alcohol mass concentration is 70%, and the weight ratio of peppermint used and the edible ethanol is 1:1~3.
CN201910684954.1A 2019-07-26 2019-07-26 A kind of propolis oral cleansing lotion and preparation method thereof Pending CN110227056A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111329930A (en) * 2020-04-30 2020-06-26 云南风联科技有限公司 Plant tobacco-flavored oral cavity atomized liquid and preparation method thereof
CN112370477A (en) * 2020-11-03 2021-02-19 广东启美生物科技有限公司 Antibacterial oral preparation for refreshing breath, strengthening teeth and protecting gingiva and equipment thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103610726A (en) * 2013-11-21 2014-03-05 江苏江大源生态生物科技有限公司 Compound propolis oral disinfection spray and preparation method thereof
CN107875243A (en) * 2017-11-24 2018-04-06 张龙兵 Spray liquid for fresh breath
CN108464965A (en) * 2018-06-15 2018-08-31 沈阳药科大学 A kind of propolis mouthwash and preparation method thereof containing active skull cap components

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103610726A (en) * 2013-11-21 2014-03-05 江苏江大源生态生物科技有限公司 Compound propolis oral disinfection spray and preparation method thereof
CN107875243A (en) * 2017-11-24 2018-04-06 张龙兵 Spray liquid for fresh breath
CN108464965A (en) * 2018-06-15 2018-08-31 沈阳药科大学 A kind of propolis mouthwash and preparation method thereof containing active skull cap components

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111329930A (en) * 2020-04-30 2020-06-26 云南风联科技有限公司 Plant tobacco-flavored oral cavity atomized liquid and preparation method thereof
CN112370477A (en) * 2020-11-03 2021-02-19 广东启美生物科技有限公司 Antibacterial oral preparation for refreshing breath, strengthening teeth and protecting gingiva and equipment thereof

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Application publication date: 20190913