CN106509982B - Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof - Google Patents
Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof Download PDFInfo
- Publication number
- CN106509982B CN106509982B CN201611014630.XA CN201611014630A CN106509982B CN 106509982 B CN106509982 B CN 106509982B CN 201611014630 A CN201611014630 A CN 201611014630A CN 106509982 B CN106509982 B CN 106509982B
- Authority
- CN
- China
- Prior art keywords
- parts
- dripping pill
- solution
- weight
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000006187 pill Substances 0.000 title claims abstract description 54
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 34
- 239000003205 fragrance Substances 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 38
- 239000002826 coolant Substances 0.000 claims abstract description 38
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 125000005456 glyceride group Chemical group 0.000 claims abstract description 12
- 239000002253 acid Substances 0.000 claims abstract description 11
- 235000019441 ethanol Nutrition 0.000 claims abstract description 11
- 241000196324 Embryophyta Species 0.000 claims abstract description 10
- 239000002904 solvent Substances 0.000 claims abstract description 10
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims description 19
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 9
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 9
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- 150000001408 amides Chemical class 0.000 claims description 8
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 6
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 6
- 239000003240 coconut oil Substances 0.000 claims description 6
- 235000019864 coconut oil Nutrition 0.000 claims description 6
- 229940041616 menthol Drugs 0.000 claims description 6
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 150000004665 fatty acids Chemical class 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 239000003921 oil Substances 0.000 claims description 3
- 235000019198 oils Nutrition 0.000 claims description 3
- 244000246386 Mentha pulegium Species 0.000 abstract description 11
- 235000016257 Mentha pulegium Nutrition 0.000 abstract description 11
- 235000004357 Mentha x piperita Nutrition 0.000 abstract description 11
- 235000001050 hortel pimenta Nutrition 0.000 abstract description 11
- 239000008157 edible vegetable oil Substances 0.000 abstract description 7
- 239000004094 surface-active agent Substances 0.000 abstract description 7
- 239000000654 additive Substances 0.000 abstract description 3
- 230000000996 additive effect Effects 0.000 abstract description 3
- 238000007493 shaping process Methods 0.000 abstract description 3
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 238000009472 formulation Methods 0.000 abstract description 2
- 235000019477 peppermint oil Nutrition 0.000 abstract 1
- 235000019640 taste Nutrition 0.000 description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- 229920000136 polysorbate Polymers 0.000 description 4
- NFLGAXVYCFJBMK-RKDXNWHRSA-N (+)-isomenthone Natural products CC(C)[C@H]1CC[C@@H](C)CC1=O NFLGAXVYCFJBMK-RKDXNWHRSA-N 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- NFLGAXVYCFJBMK-UHFFFAOYSA-N Menthone Chemical compound CC(C)C1CCC(C)CC1=O NFLGAXVYCFJBMK-UHFFFAOYSA-N 0.000 description 3
- UJNOLBSYLSYIBM-WISYIIOYSA-N [(1r,2s,5r)-5-methyl-2-propan-2-ylcyclohexyl] (2r)-2-hydroxypropanoate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(=O)[C@@H](C)O UJNOLBSYLSYIBM-WISYIIOYSA-N 0.000 description 3
- DNSISZSEWVHGLH-UHFFFAOYSA-N butanamide Chemical compound CCCC(N)=O DNSISZSEWVHGLH-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 229930007503 menthone Natural products 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 description 2
- 235000019482 Palm oil Nutrition 0.000 description 2
- 235000019483 Peanut oil Nutrition 0.000 description 2
- 235000019484 Rapeseed oil Nutrition 0.000 description 2
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 description 2
- 235000019658 bitter taste Nutrition 0.000 description 2
- 235000005687 corn oil Nutrition 0.000 description 2
- 239000002285 corn oil Substances 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000004006 olive oil Substances 0.000 description 2
- 235000008390 olive oil Nutrition 0.000 description 2
- 239000002540 palm oil Substances 0.000 description 2
- 239000000312 peanut oil Substances 0.000 description 2
- 229950008882 polysorbate Drugs 0.000 description 2
- 239000003507 refrigerant Substances 0.000 description 2
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 description 1
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 description 1
- VUNOFAIHSALQQH-UHFFFAOYSA-N Ethyl menthane carboxamide Chemical class CCNC(=O)C1CC(C)CCC1C(C)C VUNOFAIHSALQQH-UHFFFAOYSA-N 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 240000007817 Olea europaea Species 0.000 description 1
- DFNKJCJNMXTBCC-UHFFFAOYSA-N acetic acid;butanamide Chemical compound CC(O)=O.CCCC(N)=O DFNKJCJNMXTBCC-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 229940068968 polysorbate 80 Drugs 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 230000014860 sensory perception of taste Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Landscapes
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of cool degree fragrance solution of the height for cigarette dripping pill and preparation method thereof.The cool degree fragrance solution of height is mixed by the coolant agent solution of 1~70 parts by weight and the dripping pill oil-soluble solution of 30~99 parts by weight, wherein described coolant agent solution is formed by 5~60 parts of menthols, 5~80 parts of coolant agents, 2~20 parts of peppermint oil dementholizeds and 2~10 parts of ethyl alcohol mixed preparings, and the oil-soluble solution of the dripping pill is formed by 5~90 portions of edible vegetable oils, 5~90 parts of pungent certain herbaceous plants with big flowers acid glycerides, 0.01~10 part of surfactant formulatory.On the one hand the formula and preparation method of the present invention can improve the additive amount of peppermint, in addition coordinate coolant agent, greatly enhance the cool degree of cigarette dripping pill, promote cigarette smoking quality；On the other hand the coolant agent solvent formula of configuration can dissolve coolant agent, and the shaping beneficial to dripping pill and guarantee dripping pill stable quality well.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of cool degree fragrance solution of height for cigarette dripping pill and its system
Preparation Method.
Background technology
At present, on consumption market there are many cigarette product using dripping pill, wherein popularize the most package be peppermint by essence.
It can make cigarette smoking that can bring consumer to one refrigerant taste and preferably aspirate experience using peppermint.But peppermint
On the one hand essence is not easily dissolved into the oil-based solvent used in dripping pill, if another aspect concentration is excessive, can generate stimulation, bitter taste
And the negative effects such as pleasant impression is uncomfortable, while if Mint Essence increasing concentrations, also affect dripping and the shaping of dripping pill, lead
Cause dripping pill production yield rate is low, presentation quality is bad.Therefore in dripping pill product the usage amount of peppermint generally 2% -20%,
It is difficult to increase the additive amount of peppermint again.It is ice-cold to feel it is inadequate for the consumer for wanting to experience the cool degree impression of ultimate attainment height
's.
The new coolant agent as obtained from being modified the molecular structure to menthol had much in recent years, such as：Second
Sour menthyl ester, menthyl lactate, menthone glycerol ketals, amide of mint etc..In numerous products, with amide of mint (i.e. WS-
3, English name N-ethyl-p-menthane-3-carboxamides) cool taste effect it is most strong, sense of taste stop it is most long, can be with
Give people a kind of pleasant and lasting pure and fresh pleasantly cool sensation.The chemical name of coolant agent WS-23 be N, 2,3- trimethyls -2- (1- first
Base ethyl) butyramide or N, 2,3. trimethyl -2- butanamides, English name N, 2,3-trimethyl-
2isopropl butanamide, feature is clear happy, lasting, fresh, nonirritant pungent, low without bitter taste, dosage.Both
Coolant agent commercialized degree highest, application effect are best.
Peppermint oil dementholized is colourless or flaxen supernatant liquid.There is special refrigerant fragrance, it is pungent, rear cool at the beginning of taste.It can be with peppermint
Alcohol, ethyl alcohol and a variety of oil-dissolving solvents dissolve each other.
The content of the invention
For the above-mentioned deficiency of the prior art, the technical problem to be solved in the present invention is to provide a kind of for cigarette dripping pill
High cool degree fragrance solution and preparation method thereof, is the coolant agent amide of mint of peppermint several times by using cool degree, and using peppermint
Vegetable oil, ethyl alcohol equal solvent solve the problems of dissolution of menthol, and the package concentration of the coolant agents such as peppermint in dripping pill is greatly improved, so as to
A kind of cigarette dripping pill of high cool degree is prepared, and can ensure that the production of dripping pill and presentation quality are stablized.
Technical solution provided by the invention is：A kind of cool degree fragrance solution of height for cigarette dripping pill, feature exist
In the cool degree fragrance solution of the height be coolant agent solution by 1~70 parts by weight and the dripping pill oil-soluble solution of 30~99 parts by weight
It mixes, wherein the coolant agent solution is made of the following raw material that total weight is 100 parts：
Wherein, the coolant agent includes：Amide of mint, N, 2,3- trimethyls -2- (1- Methylethyls) butyramide acetic acid are thin
Any one or a few in lotus ester (WS-23), menthyl lactate, menthone glycerol ketals；
The purity of alcohol 70%~99%.
The oil-soluble solution of the dripping pill is made of the following raw material that total weight is 100 parts：
Edible vegetable oil 5~90
Pungent certain herbaceous plants with big flowers acid glyceride 5~90
Surfactant 0.01~10.
The present invention preferably technical solution：Edible vegetable oil in the oil-soluble solution formula of the dripping pill includes：Olive
Any one or a few in oil, coconut oil, rapeseed oil, palm oil, corn oil, peanut oil；
The present invention preferably technical solution：Surfactant in the oil-soluble solution formula of the dripping pill includes：Fat
Acid glyceride, fatty acid sorbitan (Span), any one or a few in polysorbate (tween).
The present invention provides a kind of preparation method of the cool degree fragrance solution of the height for cigarette dripping pill, it is characterised in that specific step
It is rapid as follows：
(1) raw material is prepared according to the formula of following coolant agent solution：5~60 parts by weight menthols, 5~80 coolant agents, 2~
The ethyl alcohol of the peppermint oil dementholized of 20 parts by weight, 2~10 parts by weight, the total weight of the raw material is 100 parts；The coolant agent includes：
Amide of mint, N, 2,3- trimethyls -2- (1- Methylethyls) butyramide menthyl acetate, menthyl lactate, menthone glycerin contracting
Any one or a few in ketone；The solvent includes：Any one in peppermint oil dementholized, ethyl alcohol or two kinds；
(2) whole peppermint oil dementholized and ethyl alcohol are first hybridly prepared into solvent, it is then that whole menthols and coolant agent are molten
In solvent, coolant agent solution is configured to when stirring 0.5-2 is small under 5 DEG C-15 DEG C of cryogenic conditions；
(3) according to the edible vegetable oil of 5~90 parts by weight, the pungent certain herbaceous plants with big flowers acid glyceride of 5~90 parts by weight, 0.01~10 weight
The surfactant of part is uniformly mixed the dripping pill oil-soluble solution for being configured to that total weight is 100 parts；Wherein described edible vegetable oil
For any one or a few in olive oil, coconut oil, rapeseed oil, palm oil, corn oil, peanut oil；The surfactant
Including：Fatty glyceride, fatty acid sorbitan (Span), any one or a few in polysorbate (tween)；It is described pungent
Certain herbaceous plants with big flowers acid glyceride viscosity is 20mPa.s~60mPa.s；
(4) the coolant agent solution prepared in 1~70 parts by weight step (2) is weighed with matching somebody with somebody in 30~99 parts by weight steps (3)
The oil-soluble solution of the dripping pill of system is mixed according to total weight parts for 100 parts, and when stirring at normal temperature 0.5-2 is small after, stand
0.5-2 defoam the height cool degree fragrance solution being made for cigarette dripping pill when small.
Advantages of the present invention：On the one hand the formula and preparation method of the present invention can improve the additive amount of peppermint, in addition match somebody with somebody
Coolant agent is closed, greatly enhances the cool degree of cigarette dripping pill, promotes cigarette smoking quality；On the other hand the coolant agent solvent of configuration is matched somebody with somebody
Coolant agent, and the shaping beneficial to dripping pill and guarantee dripping pill stable quality can be dissolved well in side.
Specific embodiment
The specific embodiment of the present invention is described in further detail with reference to embodiment.Following embodiment is
Laboratory data.
Embodiment 1：A kind of cool degree fragrance solution of height for cigarette dripping pill, specific preparation method are as follows：
(1) raw material is prepared according to the formula of following coolant agent solution：
After above-mentioned raw materials are mixed coolant agent solution is configured to when stirring 0.5 is small in a low temperature of 5 DEG C；
(2) raw material in formula as below is uniformly mixed to the oil-soluble solution for being configured to dripping pill, specific formula such as following table：
| Raw material type | Specification | Parts by weight |
| Edible vegetable oil | Coconut oil | 80 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Viscosity 20mPa.s | 19.5 |
| Surfactant | Span 80 | 0.5 |
(3) dripping pill that will be prepared in the coolant agent solution mixed in 20 parts by weight steps (1) and 80 parts by weight steps (2)
Oil-soluble solution mix, and under normal temperature condition stirring 0.5 it is small when after, then stand 0.5 it is small when defoam, be configured to for cigarette use
The cool degree fragrance solution of height of dripping pill.
The cool degree of height prepared using the cool taste fragrance solution prepared in embodiment 1 according to existing cigarette method for preparing drop pills
Cigarette is good with dripping pill exterior quality, is added in cigarette and pinches brokenly suction, can experience certain cool taste breath, but flue gas stimulates
Property increase, pleasant impression is relatively comfortable.
Embodiment 2：A kind of cool degree fragrance solution of height for cigarette dripping pill, specific preparation method are as follows：
(1) raw material is prepared according to the formula of following coolant agent solution：
| Raw material type | Specification | Parts by weight |
| Menthol | Purity 99.5% | 20 |
| Coolant agent (WS-23) | Purity 99% | 60 |
| Peppermint oil dementholized | Determination of menthol 50% | 15 |
| Ethyl alcohol | 90% | 5 |
Above-mentioned raw materials are stirred under 10 DEG C of cryogenic conditions 1 it is small when, be configured to coolant agent solution；
(2) raw material in formula as below is uniformly mixed to the oil-soluble solution for being configured to dripping pill, specific formula such as following table：
(4) dripping pill that will be prepared in the coolant agent solution mixed in 40 parts by weight steps (1) and 60 parts by weight steps (2)
Oil-soluble solution mixes, and when stirring 1 is small under normal temperature condition after, then stand 1 it is small when defoam, be configured to for cigarette dripping pill
The cool degree fragrance solution of height.
The cool degree of height prepared using the cool taste fragrance solution prepared in embodiment 2 according to existing cigarette method for preparing drop pills
Cigarette is good with dripping pill exterior quality, is added in cigarette and pinches brokenly suction, can experience apparent cool taste breath, flue gas irritation
Slightly increase, pleasant impression is relatively comfortable.
Embodiment 3：A kind of cool degree fragrance solution of height for cigarette dripping pill, specific preparation method are as follows：
(1) raw material is prepared according to the formula of following coolant agent solution：
After above-mentioned raw materials are mixed when low temperature stirring 1.5 is small under the conditions of 15 DEG C, coolant agent solution is configured to；
(2) raw material in formula as below is uniformly mixed to the oil-soluble solution for being configured to dripping pill, specific formula such as following table：
| Raw material type | Specification | Parts by weight |
| Edible vegetable oil | Olive oil：Coconut oil is 1：1 | 50 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Viscosity 45mPa.s | 48 |
| Surfactant | Span 80：POLYSORBATE 80 is 1：1 | 2 |
(4) dripping pill that will be prepared in the coolant agent solution mixed in 60 parts by weight steps (1) and 40 parts by weight steps (2)
Oil-soluble solution mix, and under normal temperature condition stirring 1.5 it is small when after, then stand 2 it is small when defoam, be configured to for cigarette drop
The cool degree fragrance solution of height of ball.
The cool degree of height prepared using the cool taste fragrance solution prepared in embodiment 3 according to existing cigarette method for preparing drop pills
Cigarette dripping pill appearance collapses and to break pearl more, is added in cigarette and pinches brokenly suction, can experience obviously cool taste
Breath, the increase of flue gas irritation, pleasant impression are deteriorated.
Claims (2)
1. a kind of cool degree fragrance solution of height for cigarette dripping pill, it is characterised in that the cool degree fragrance solution of the height is by 20 weight
The coolant agent solution and the dripping pill oil-soluble solution of 80 parts by weight of part mix, wherein the coolant agent solution is by following heavy
Measure part raw material composition：
Menthol 58
Amide of mint 20
Peppermint oil dementholized 20
Ethyl alcohol 2
The purity of alcohol 70%~99%；
The oil-soluble solution of the dripping pill is made of the following raw material that total weight is 100 parts：
Coconut oil 80
Pungent certain herbaceous plants with big flowers acid glyceride 19.5
Fatty acid sorbitan 0.5；
Wherein, the pungent certain herbaceous plants with big flowers acid glyceride viscosity is 20 mPa.s.
2. the preparation method of the cool degree fragrance solution of a kind of height for cigarette dripping pill, it is characterised in that be as follows：
（1）Prepare raw material according to the formula of following coolant agent solution：The menthol of 58 parts by weight, 20 parts by weight amide of mint,
The ethyl alcohol of the peppermint oil dementholized of 20 parts by weight, 2 parts by weight；
（2）Whole peppermint oil dementholized and ethyl alcohol are first hybridly prepared into solvent, are then dissolved in whole menthols and amide of mint
In solvent, coolant agent solution is configured to when stirring 0.5-2 is small under 5 DEG C-15 DEG C of cryogenic conditions；
（3）The fatty acid sorbitan of the coconut oil of 80 parts by weight, the pungent certain herbaceous plants with big flowers acid glyceride of 19.5 parts by weight and 0.5 parts by weight is mixed
Close the dripping pill oil-soluble solution for being uniformly configured to that total weight number is 100 parts；The pungent certain herbaceous plants with big flowers acid glyceride viscosity is 20 mPa.s；
（4）Weigh 20 parts by weight steps（2）The coolant agent solution of middle preparation and 80 parts by weight steps（3）The dripping pill oil of middle preparation is molten
Property solution mixed according to total weight parts for 100 parts, and when stirring 0.5-2 is small at normal temperatures after, stand 0.5-2 it is small when disappear
It is brewed to the cool degree fragrance solution of height for cigarette dripping pill.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611014630.XA CN106509982B (en) | 2016-11-18 | 2016-11-18 | Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611014630.XA CN106509982B (en) | 2016-11-18 | 2016-11-18 | Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106509982A CN106509982A (en) | 2017-03-22 |
| CN106509982B true CN106509982B (en) | 2018-05-25 |
Family
ID=58352319
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611014630.XA Active CN106509982B (en) | 2016-11-18 | 2016-11-18 | Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106509982B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108179063B (en) * | 2018-01-16 | 2020-11-03 | 武汉黄鹤楼香精香料有限公司 | Cool essence for mint type cigarette tipping paper and preparation method and application thereof |
| CN110819450A (en) * | 2018-08-07 | 2020-02-21 | 江门市花芸雅香料有限公司 | Essence for solid fragrance and preparation method thereof |
| CN109619666B (en) * | 2018-11-14 | 2021-01-29 | 云南中烟工业有限责任公司 | Cool taste humectant, preparation method and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1041506A (en) * | 1973-03-22 | 1978-10-31 | David G. Rowsell | Compounds having a physiological cooling effect and compositions containing them |
| CN101002827A (en) * | 2006-12-15 | 2007-07-25 | 江南大学 | Micro-emulsion of mint oil with slow-releasing property, and its preparing method |
| CN104585880A (en) * | 2015-01-20 | 2015-05-06 | 湖北中烟工业有限责任公司 | Mint essence solvent for cigarette dropping pill |
| CN104800090A (en) * | 2015-03-11 | 2015-07-29 | 昆山市亚香日用香料有限公司 | Novel cooling agent composition formed by compounding mint amide derivatives |
| CN105168009A (en) * | 2015-09-30 | 2015-12-23 | 安徽丰乐香料有限责任公司 | Water-soluble dropping pills containing compound cooling agent and preparation method of dropping pills |
-
2016
- 2016-11-18 CN CN201611014630.XA patent/CN106509982B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1041506A (en) * | 1973-03-22 | 1978-10-31 | David G. Rowsell | Compounds having a physiological cooling effect and compositions containing them |
| CN101002827A (en) * | 2006-12-15 | 2007-07-25 | 江南大学 | Micro-emulsion of mint oil with slow-releasing property, and its preparing method |
| CN104585880A (en) * | 2015-01-20 | 2015-05-06 | 湖北中烟工业有限责任公司 | Mint essence solvent for cigarette dropping pill |
| CN104800090A (en) * | 2015-03-11 | 2015-07-29 | 昆山市亚香日用香料有限公司 | Novel cooling agent composition formed by compounding mint amide derivatives |
| CN105168009A (en) * | 2015-09-30 | 2015-12-23 | 安徽丰乐香料有限责任公司 | Water-soluble dropping pills containing compound cooling agent and preparation method of dropping pills |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106509982A (en) | 2017-03-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106281680B (en) | A kind of quick-fried pearl of peppermint cigarette cool taste Mint Essence and the preparation method and application thereof | |
| CN106753787B (en) | Bead-blasting lemon mint essential oil for cigarettes as well as preparation method and application thereof | |
| CN106509982B (en) | Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof | |
| CN102006786B (en) | Warming sensate composition | |
| EP2903627B1 (en) | Non-irritating lubricant compositions with active sensorial agents | |
| CN104585880B (en) | A kind of Mint Essence solvent for cigarette dripping pill | |
| US20150246131A1 (en) | Water-based personal lubricants with a silicone component | |
| JP5198533B2 (en) | Menthol bitterness inhibitor | |
| CN101573099B (en) | Cooling agent composition and preparative method thereof | |
| JP5220942B1 (en) | Menthol bitterness inhibitor | |
| WO2014051259A1 (en) | Cosmetic composition, containing xylitol fatty acid esters as active ingredient, having continuous cooling effect | |
| CN106456522A (en) | Formulation for personal hygiene | |
| RU2458683C2 (en) | Lubricant composition for individual application | |
| CN111568778B (en) | Three-layer essence with skin modification and nourishing effects, and preparation method and application thereof | |
| CN107950983A (en) | A kind of compounding coolant agent composition based on menthol and preparation method thereof | |
| JP6042086B2 (en) | Gelatin molding composition | |
| CN105194107A (en) | Spirit-raising and refreshing drug and preparation method thereof | |
| CN104957585A (en) | Hami melon essence for cold drink as well as preparation method and application thereof | |
| JP4941977B2 (en) | Oral jelly-like pharmaceutical composition of benzisoxazole derivative | |
| WO2012135559A1 (en) | Menthol liquids composition | |
| CN111773198A (en) | Novel soft capsule of eldecalcitol and preparation method thereof | |
| CN104940058A (en) | Essence composition and preparation method thereof | |
| CN111432842A (en) | Non-pharmaceutical teething cooling composition | |
| JP5422956B2 (en) | Cream for external use of skin | |
| JP6321100B2 (en) | Gelatin molding composition |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |