CN106509982A - High-cold-degree essence solution for cigarette dropping pill and preparation method thereof - Google Patents
High-cold-degree essence solution for cigarette dropping pill and preparation method thereof Download PDFInfo
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- CN106509982A CN106509982A CN201611014630.XA CN201611014630A CN106509982A CN 106509982 A CN106509982 A CN 106509982A CN 201611014630 A CN201611014630 A CN 201611014630A CN 106509982 A CN106509982 A CN 106509982A
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- 239000006187 pill Substances 0.000 title claims abstract description 57
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000002826 coolant Substances 0.000 claims abstract description 42
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000008157 edible vegetable oil Substances 0.000 claims abstract description 11
- 239000004094 surface-active agent Substances 0.000 claims abstract description 11
- 239000002904 solvent Substances 0.000 claims abstract description 9
- 235000006679 Mentha X verticillata Nutrition 0.000 claims abstract description 8
- 235000002899 Mentha suaveolens Nutrition 0.000 claims abstract description 8
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims abstract description 8
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims abstract description 8
- 235000019477 peppermint oil Nutrition 0.000 claims abstract description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 37
- 239000003205 fragrance Substances 0.000 claims description 23
- 239000002994 raw material Substances 0.000 claims description 20
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 14
- 125000005456 glyceride group Chemical group 0.000 claims description 13
- 244000246386 Mentha pulegium Species 0.000 claims description 11
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 11
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 11
- 235000001050 hortel pimenta Nutrition 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 10
- 241000196324 Embryophyta Species 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- 150000001408 amides Chemical class 0.000 claims description 7
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims description 6
- 239000003240 coconut oil Substances 0.000 claims description 6
- 235000019864 coconut oil Nutrition 0.000 claims description 6
- 229920000136 polysorbate Polymers 0.000 claims description 6
- NFLGAXVYCFJBMK-RKDXNWHRSA-N (+)-isomenthone Natural products CC(C)[C@H]1CC[C@@H](C)CC1=O NFLGAXVYCFJBMK-RKDXNWHRSA-N 0.000 claims description 5
- NFLGAXVYCFJBMK-UHFFFAOYSA-N Menthone Chemical compound CC(C)C1CCC(C)CC1=O NFLGAXVYCFJBMK-UHFFFAOYSA-N 0.000 claims description 5
- UJNOLBSYLSYIBM-WISYIIOYSA-N [(1r,2s,5r)-5-methyl-2-propan-2-ylcyclohexyl] (2r)-2-hydroxypropanoate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(=O)[C@@H](C)O UJNOLBSYLSYIBM-WISYIIOYSA-N 0.000 claims description 5
- DNSISZSEWVHGLH-UHFFFAOYSA-N butanamide Chemical compound CCCC(N)=O DNSISZSEWVHGLH-UHFFFAOYSA-N 0.000 claims description 5
- 229930007503 menthone Natural products 0.000 claims description 5
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 claims description 4
- 235000019482 Palm oil Nutrition 0.000 claims description 4
- 235000019483 Peanut oil Nutrition 0.000 claims description 4
- 235000019484 Rapeseed oil Nutrition 0.000 claims description 4
- 235000005687 corn oil Nutrition 0.000 claims description 4
- 239000002285 corn oil Substances 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 150000004665 fatty acids Chemical class 0.000 claims description 4
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims description 4
- 239000004006 olive oil Substances 0.000 claims description 4
- 235000008390 olive oil Nutrition 0.000 claims description 4
- 239000002540 palm oil Substances 0.000 claims description 4
- 239000000312 peanut oil Substances 0.000 claims description 4
- 229950008882 polysorbate Drugs 0.000 claims description 4
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims description 3
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 2
- 239000003292 glue Substances 0.000 claims 1
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 abstract description 5
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 abstract description 5
- 229940041616 menthol Drugs 0.000 abstract description 5
- 239000003921 oil Substances 0.000 abstract description 4
- 235000019198 oils Nutrition 0.000 abstract description 4
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 230000002349 favourable effect Effects 0.000 abstract 2
- 235000019441 ethanol Nutrition 0.000 abstract 1
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 abstract 1
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 abstract 1
- 235000019640 taste Nutrition 0.000 description 9
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 description 2
- 235000019658 bitter taste Nutrition 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000003507 refrigerant Substances 0.000 description 2
- 238000007493 shaping process Methods 0.000 description 2
- VUNOFAIHSALQQH-UHFFFAOYSA-N Ethyl menthane carboxamide Chemical class CCNC(=O)C1CC(C)CCC1C(C)C VUNOFAIHSALQQH-UHFFFAOYSA-N 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 240000007817 Olea europaea Species 0.000 description 1
- DFNKJCJNMXTBCC-UHFFFAOYSA-N acetic acid;butanamide Chemical compound CC(O)=O.CCCC(N)=O DFNKJCJNMXTBCC-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 229940068968 polysorbate 80 Drugs 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 230000014860 sensory perception of taste Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Landscapes
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention provides a high-cold-degree essence solution for a cigarette dropping pill and a preparation method thereof. The high-cold-degree essence solution is formed by mixing 1 to 70 weight parts of cooling agent solution and 30 to 99 weight parts of dropping pill oil soluble solution, wherein the cooling agent solution is prepared by mixing 5 to 60 parts of menthol, 5 to 80 parts of a cooling agent, 2 to 20 parts of dementholized peppermint oil and 2 to 10 parts of ethyl alcohol; the dropping pill oil soluble solution is formed by preparing 5 to 90 parts of edible vegetable oil, 5 to 90 parts of caprylic/capric triglyceride and 0.01 to 10 parts of a surfactant. According to a formula and the preparation method disclosed by the invention, on one hand, the adding amount of mint can be improved, and additionally, the cold degree of the cigarette dropping pill is greatly enhanced by matching the cooling agent so that the smoking quality of a cigarette is improved; on the other hand, the cooling agent can be dissolved very well by preparing a cooling agent solvent formula, the dropping pill is favourable to form, and the quality stability of the dropping pill is favourable to guarantee.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of high cool degree fragrance solution and its system for cigarette dripping pill
Preparation Method.
Background technology
At present, have the cigarette product of various use dripping pills on consumption market, wherein parcel essence popularized the most is peppermint.
Cigarette smoking can be made to one refrigerant taste using peppermint, consumer can be brought and preferably aspirate experience.But peppermint
On the one hand essence be not easily dissolved into the oil-based solvent used in dripping pill, if another aspect concentration is excessive, can produce stimulation, bitter taste
And the negative effect such as pleasant impression is uncomfortable, if while Mint Essence increasing concentrations, also affect dripping and the shaping of dripping pill, lead
Cause dripping pill production yield rate is low, presentation quality is bad.Therefore in dripping pill product the usage amount of peppermint typically 2% 20%,
It is difficult to again increase the addition of peppermint.For wanting to experience the consumer of the cool degree impression of ultimate attainment height, which is ice-cold to feel it is inadequate
's.
New coolant agent obtained from being modified by the molecular structure to menthol was had a lot, for example in recent years：Second
Sour menthyl ester, menthyl lactate, menthone glycerol ketals, amide of mint etc..In numerous products, with amide of mint (i.e. WS-
3, English name N-ethyl-p-menthane-3-carboxamides) cool taste effect it is most strong, sense of taste stop it is most long, can be with
Give people a kind of pleasant and lasting pure and fresh pleasantly cool sensation.The chemical name of coolant agent WS-23 be N, 2,3- trimethyl -2- (1- first
Base ethyl) butyramide or N, 2,3. trimethyl -2- butanamides, English name is N, 2,3-trimethyl-
2isopropl butanamide, its feature is clear happy, lasting, fresh, nonirritant pungent, low without bitter taste, consumption.Both
Coolant agent commercialized degree highest, application effect are best.
Peppermint oil dementholized is colourless or flaxen supernatant liquid.There is special refrigerant fragrance, taste is just pungent, rear cool.Can be with peppermint
Alcohol, ethanol and various oil-dissolving solvents dissolve each other.
The content of the invention
For the above-mentioned deficiency of prior art, the technical problem to be solved in the present invention is to provide a kind of for cigarette dripping pill
High cool degree fragrance solution and preparation method thereof, is the coolant agent amide of mint of peppermint several times by using cool degree, and adopts peppermint
Vegetable oil, ethanol equal solvent solve the problems of dissolution of menthol, and the parcel concentration of the coolant agent such as peppermint in dripping pill is greatly improved, so as to
A kind of cigarette dripping pill of high cool degree is prepared, and can ensure that the production of dripping pill and presentation quality are stable.
The present invention provide technical scheme be：A kind of high cool degree fragrance solution for cigarette dripping pill, its feature exist
In the height it is cool degree fragrance solution be by the dripping pill oil-soluble solution of the coolant agent solution and 30～99 weight portions of 1～70 weight portion
Mix, wherein the coolant agent solution is made up of the following raw material that gross weight is 100 parts：
Wherein, the coolant agent includes：Amide of mint, N, 2,3- trimethyl -2- (1- Methylethyls) butyramide acetic acid are thin
Any one or a few in lotus ester (WS-23), menthyl lactate, menthone glycerol ketals；
The purity of alcohol 70%～99%.
The oil-soluble solution of the dripping pill is made up of the following raw material that gross weight is 100 parts：
Edible vegetable oil 5～90
Pungent certain herbaceous plants with big flowers acid glyceride 5～90
Surfactant 0.01～10.
The present invention preferably technical scheme：Edible vegetable oil in the oil-soluble solution formula of the dripping pill includes：Olive
Any one or a few in oil, coconut oil, rapeseed oil, palm oil, corn oil, peanut oil；
The present invention preferably technical scheme：Surfactant in the oil-soluble solution formula of the dripping pill includes：Fat
Acid glyceride, fatty acid sorbitan (Span), any one or a few in polysorbate (tween).
The present invention provides a kind of preparation method of the high cool degree fragrance solution for cigarette dripping pill, it is characterised in that concrete to walk
It is rapid as follows：
(1) prepare raw material according to the formula of following coolant agent solution：5～60 weight portion menthols, 5～80 coolant agents, 2～
The ethanol of the peppermint oil dementholized of 20 weight portions, 2～10 weight portions, the gross weight of the raw material is 100 parts；The coolant agent includes：
Amide of mint, N, 2,3- trimethyl -2- (1- Methylethyls) butyramide menthyl acetate, menthyl lactate, menthone glycerin contracting
Any one or a few in ketone；The solvent includes：Any one in peppermint oil dementholized, ethanol or two kinds；
(2) whole peppermint oil dementholizeds and ethanol are hybridly prepared into into solvent first, then will be whole menthols and coolant agent molten
In solvent, the stirring under 5 DEG C 15 DEG C of cryogenic conditions is configured to coolant agent solution in 0.5 2 hours；
(3) according to the edible vegetable oil of 5～90 weight portions, the pungent certain herbaceous plants with big flowers acid glyceride of 5～90 weight portions, 0.01～10 weight
The surfactant of part is well mixed the dripping pill oil-soluble solution for being configured to that gross weight is 100 parts；Wherein described edible vegetable oil
For any one or a few in olive oil, coconut oil, rapeseed oil, palm oil, corn oil, peanut oil；The surfactant
Including：Fatty glyceride, fatty acid sorbitan (Span), any one or a few in polysorbate (tween)；It is described pungent
Certain herbaceous plants with big flowers acid glyceride viscosity is 20mPa.s～60mPa.s；
(4) match somebody with somebody in the coolant agent solution prepared in weighing 1～70 weight portion step (2) and 30～99 weight portion steps (3)
The oil-soluble solution of the dripping pill of system is mixed for 100 parts according to total weight parts, and after stirring at normal temperature 0.5 2 hours, is stood
Froth breaking makes the high cool degree fragrance solution for cigarette dripping pill within 0.5 2 hours.
Advantages of the present invention：On the one hand the formula and preparation method of the present invention can improve the addition of peppermint, match somebody with somebody in addition
Coolant agent is closed, the cool degree of cigarette dripping pill is greatly enhanced, cigarette smoking quality is lifted；On the other hand the coolant agent solvent of configuration is matched somebody with somebody
Side, can dissolve coolant agent, and the shaping beneficial to dripping pill and guarantee dripping pill steady quality well.
Specific embodiment
The specific embodiment of the present invention is described in further detail with reference to embodiment.Following examples are
Laboratory data.
Embodiment 1：A kind of high cool degree fragrance solution for cigarette dripping pill, its concrete preparation method are as follows：
(1) prepare raw material according to the formula of following coolant agent solution：
Stir in a low temperature of 5 DEG C after above-mentioned raw materials are mixed and be configured to coolant agent solution in 0.5 hour；
(2) raw material in formula as below is well mixed the oil-soluble solution for being configured to dripping pill, its Ju Ti Pei Fang such as following table：
| Raw material type | Specification | Weight portion |
| Edible vegetable oil | Coconut oil | 80 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Viscosity 20mPa.s | 19.5 |
| Surfactant | Span 80 | 0.5 |
(3) dripping pill that will be prepared in the coolant agent solution mixed in 20 weight portion steps (1) and 80 weight portion steps (2)
Oil-soluble solution mixes, and after stirring 0.5 hour under normal temperature condition, then stands 0.5 hour froth breaking, is configured to use for cigarette
The high cool degree fragrance solution of dripping pill.
The high cool degree prepared according to existing cigarette method for preparing drop pills using the cool taste fragrance solution prepared in embodiment 1
Cigarette is good with dripping pill exterior quality, and suction is pinched brokenly in being added to cigarette, can experience certain cool taste breath, but flue gas stimulates
Property increase, pleasant impression is relatively comfortable.
Embodiment 2：A kind of high cool degree fragrance solution for cigarette dripping pill, its concrete preparation method are as follows：
(1) prepare raw material according to the formula of following coolant agent solution：
| Raw material type | Specification | Weight portion |
| Menthol | Purity 99.5% | 20 |
| Coolant agent (WS-23) | Purity 99% | 60 |
| Peppermint oil dementholized | Determination of menthol 50% | 15 |
| Ethanol | 90% | 5 |
Above-mentioned raw materials are stirred 1 hour under 10 DEG C of cryogenic conditions, coolant agent solution is configured to；
(2) raw material in formula as below is well mixed the oil-soluble solution for being configured to dripping pill, its Ju Ti Pei Fang such as following table：
(4) dripping pill that will be prepared in the coolant agent solution mixed in 40 weight portion steps (1) and 60 weight portion steps (2)
Oil-soluble solution mixes, and after stirring 1 hour under normal temperature condition, then stands 1 hour froth breaking, be configured to for cigarette dripping pill
High cool degree fragrance solution.
The high cool degree prepared according to existing cigarette method for preparing drop pills using the cool taste fragrance solution prepared in embodiment 2
Cigarette is good with dripping pill exterior quality, and suction is pinched brokenly in being added to cigarette, can experience obvious cool taste breath, flue gas excitant
Slightly increase, pleasant impression is relatively comfortable.
Embodiment 3：A kind of high cool degree fragrance solution for cigarette dripping pill, its concrete preparation method are as follows：
(1) prepare raw material according to the formula of following coolant agent solution：
After above-mentioned raw materials are mixed, under the conditions of 15 DEG C, low temperature is stirred 1.5 hours, is configured to coolant agent solution；
(2) raw material in formula as below is well mixed the oil-soluble solution for being configured to dripping pill, its Ju Ti Pei Fang such as following table：
| Raw material type | Specification | Weight portion |
| Edible vegetable oil | Olive oil：Coconut oil is 1：1 | 50 |
| Pungent certain herbaceous plants with big flowers acid glyceride | Viscosity 45mPa.s | 48 |
| Surfactant | Span 80：POLYSORBATE 80 is 1：1 | 2 |
(4) dripping pill that will be prepared in the coolant agent solution mixed in 60 weight portion steps (1) and 40 weight portion steps (2)
Oil-soluble solution mixes, and after stirring 1.5 hours under normal temperature condition, then stands 2 hours froth breakings, is configured to drip for cigarette
The high cool degree fragrance solution of ball.
The high cool degree prepared according to existing cigarette method for preparing drop pills using the cool taste fragrance solution prepared in embodiment 3
Cigarette dripping pill outward appearance has that to subside and break pearl more, pinches brokenly suction, can experience obviously cool taste in being added to cigarette
Breath, the increase of flue gas excitant, pleasant impression are deteriorated.
Claims (4)
1. a kind of high cool degree fragrance solution for cigarette dripping pill, it is characterised in that the cool degree fragrance solution of the height is by 1～70
The coolant agent solution of weight portion is mixed with the dripping pill oil-soluble solution of 30～99 weight portions, wherein the coolant agent solution is
It is made up of the following raw material that gross weight is 100 parts：
Wherein, the coolant agent includes：Amide of mint, N, 2,3- trimethyl -2- (1- Methylethyls) butyramide menthyl acetate,
Any one or a few in menthyl lactate, menthone glycerol ketals；
The purity of alcohol 70%～99%.
The oil-soluble solution of the dripping pill is made up of the following raw material that gross weight is 100 parts：
Edible vegetable oil 5～90
Pungent certain herbaceous plants with big flowers acid glyceride 5～90
Surfactant 0.01～10；
Wherein, the pungent certain herbaceous plants with big flowers acid glyceride viscosity is 20mPa.s～60mPa.s.
2. a kind of high cool degree fragrance solution for cigarette dripping pill according to claim 1, it is characterised in that the dripping pill
Oil-soluble solution formula in edible vegetable oil include：Olive oil, coconut oil, rapeseed oil, palm oil, corn oil, peanut oil
In any one or a few.
3. a kind of high cool degree fragrance solution for cigarette dripping pill according to claim 1 and 2, it is characterised in that the drop
Surfactant in the oil-soluble solution formula of ball includes：Appointing in fatty glyceride, fatty acid sorbitan, polysorbate
Anticipate one or more.
4. it is a kind of for cigarette dripping pill it is high cool degree fragrance solution preparation method, it is characterised in that comprise the following steps that：
(1) prepare raw material according to the formula of following coolant agent solution：5～60 weight portion menthols, 5～80 coolant agents, 2～20 weights
The peppermint oil dementholized of amount part, the ethanol of 2～10 weight portions；The gross weight of the raw material is 100 parts, and the coolant agent includes：Peppermint
Acid amides, N, in 2,3- trimethyl -2- (1- Methylethyls) butyramide menthyl acetate, menthyl lactate, menthone glycerol ketals
Any one or a few；
(2) whole peppermint oil dementholizeds and ethanol are hybridly prepared into into solvent first, then whole menthols and coolant agent are dissolved in molten
In agent, the stirring under 5 DEG C 15 DEG C of cryogenic conditions is configured to coolant agent solution in 0.5 2 hours；
(3) by the edible vegetable oil of 5～90 weight portions, the pungent certain herbaceous plants with big flowers acid glyceride of 5～90 weight portions and 0.01～10 weight portion
Surfactant is well mixed the dripping pill oil-soluble solution for being configured to that gross weight number is 100 parts；Wherein described edible vegetable oil
For any one or a few in olive oil, coconut oil, rapeseed oil, palm oil, corn oil, peanut oil；The surfactant
For any one or a few mixing in fatty glyceride, fatty acid sorbitan, polysorbate；The pungent certain herbaceous plants with big flowers acid glyceride glues
Spend for 20mPa.s～60mPa.s；
(4) preparation in the coolant agent solution prepared in weighing 1～70 weight portion step (2) and 30～99 weight portion steps (3)
The oil-soluble solution of dripping pill is mixed for 100 parts according to total weight parts, and after stirring 0.5 2 hours at normal temperatures, is stood
Froth breaking makes the high cool degree fragrance solution for cigarette dripping pill within 0.5 2 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611014630.XA CN106509982B (en) | 2016-11-18 | 2016-11-18 | Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611014630.XA CN106509982B (en) | 2016-11-18 | 2016-11-18 | Cool degree fragrance solution of a kind of height for cigarette dripping pill and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
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| CN106509982A true CN106509982A (en) | 2017-03-22 |
| CN106509982B CN106509982B (en) | 2018-05-25 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108179063A (en) * | 2018-01-16 | 2018-06-19 | 武汉黄鹤楼香精香料有限公司 | Cool savory essence for mint type cigarette cork paper and its preparation method and application |
| CN109619666A (en) * | 2018-11-14 | 2019-04-16 | 云南中烟工业有限责任公司 | A kind of cool taste humectant, preparation method and the usage |
| CN110819450A (en) * | 2018-08-07 | 2020-02-21 | 江门市花芸雅香料有限公司 | Essence for solid fragrance and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1041506A (en) * | 1973-03-22 | 1978-10-31 | David G. Rowsell | Compounds having a physiological cooling effect and compositions containing them |
| CN101002827A (en) * | 2006-12-15 | 2007-07-25 | 江南大学 | Micro-emulsion of mint oil with slow-releasing property, and its preparing method |
| CN104585880A (en) * | 2015-01-20 | 2015-05-06 | 湖北中烟工业有限责任公司 | Mint essence solvent for cigarette dropping pill |
| CN104800090A (en) * | 2015-03-11 | 2015-07-29 | 昆山市亚香日用香料有限公司 | Novel cooling agent composition formed by compounding mint amide derivatives |
| CN105168009A (en) * | 2015-09-30 | 2015-12-23 | 安徽丰乐香料有限责任公司 | Water-soluble dropping pills containing compound cooling agent and preparation method of dropping pills |
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| CN104585880A (en) * | 2015-01-20 | 2015-05-06 | 湖北中烟工业有限责任公司 | Mint essence solvent for cigarette dropping pill |
| CN104800090A (en) * | 2015-03-11 | 2015-07-29 | 昆山市亚香日用香料有限公司 | Novel cooling agent composition formed by compounding mint amide derivatives |
| CN105168009A (en) * | 2015-09-30 | 2015-12-23 | 安徽丰乐香料有限责任公司 | Water-soluble dropping pills containing compound cooling agent and preparation method of dropping pills |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108179063A (en) * | 2018-01-16 | 2018-06-19 | 武汉黄鹤楼香精香料有限公司 | Cool savory essence for mint type cigarette cork paper and its preparation method and application |
| CN110819450A (en) * | 2018-08-07 | 2020-02-21 | 江门市花芸雅香料有限公司 | Essence for solid fragrance and preparation method thereof |
| CN109619666A (en) * | 2018-11-14 | 2019-04-16 | 云南中烟工业有限责任公司 | A kind of cool taste humectant, preparation method and the usage |
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| CN106509982B (en) | 2018-05-25 |
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