CN106245314A - 一种纯棉巾被织物的活性低温染整方法 - Google Patents
一种纯棉巾被织物的活性低温染整方法 Download PDFInfo
- Publication number
- CN106245314A CN106245314A CN201610769106.7A CN201610769106A CN106245314A CN 106245314 A CN106245314 A CN 106245314A CN 201610769106 A CN201610769106 A CN 201610769106A CN 106245314 A CN106245314 A CN 106245314A
- Authority
- CN
- China
- Prior art keywords
- fabric
- dyeing
- finishing method
- 15min
- pure cotton
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004043 dyeing Methods 0.000 title claims abstract description 48
- 239000004744 fabric Substances 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 33
- 229920000742 Cotton Polymers 0.000 title claims abstract description 31
- 239000000975 dye Substances 0.000 claims abstract description 28
- 238000004061 bleaching Methods 0.000 claims abstract description 20
- 108090000790 Enzymes Proteins 0.000 claims abstract description 16
- 102000004190 Enzymes Human genes 0.000 claims abstract description 16
- 229940088598 enzyme Drugs 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000344 soap Substances 0.000 claims abstract description 15
- 238000005498 polishing Methods 0.000 claims abstract description 14
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 13
- 238000009991 scouring Methods 0.000 claims abstract description 13
- 238000005406 washing Methods 0.000 claims abstract description 13
- 230000008569 process Effects 0.000 claims abstract description 8
- 108010059892 Cellulase Proteins 0.000 claims abstract description 7
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 7
- 229940106157 cellulase Drugs 0.000 claims abstract description 7
- 238000002203 pretreatment Methods 0.000 claims abstract description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 24
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 8
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 8
- 230000007935 neutral effect Effects 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000010792 warming Methods 0.000 claims description 4
- 238000009941 weaving Methods 0.000 claims description 4
- 239000008186 active pharmaceutical agent Substances 0.000 claims description 3
- 102000016938 Catalase Human genes 0.000 claims 1
- 108010053835 Catalase Proteins 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 238000001035 drying Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 5
- 239000000835 fiber Substances 0.000 description 4
- 239000000985 reactive dye Substances 0.000 description 4
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 3
- 229910001882 dioxygen Inorganic materials 0.000 description 3
- 230000003213 activating effect Effects 0.000 description 2
- 238000004134 energy conservation Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- PXRKCOCTEMYUEG-UHFFFAOYSA-N 5-aminoisoindole-1,3-dione Chemical compound NC1=CC=C2C(=O)NC(=O)C2=C1 PXRKCOCTEMYUEG-UHFFFAOYSA-N 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- 108010029541 Laccase Proteins 0.000 description 1
- 241000222065 Lycoperdon Species 0.000 description 1
- 241000768494 Polymorphum Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000013351 cheese Nutrition 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000011086 high cleaning Methods 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 238000009940 knitting Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/008—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/66—Natural or regenerated cellulose using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
Abstract
本发明公开了一种纯棉巾被织物的活性低温染整方法，包括以下步骤：(1)前处理：在水浴中，加入助剂，升温到82℃‑88℃，碱性条件下练漂50min；然后，加入纤维素酶，进行酶洗抛光处理30min；(2)染色：在38℃‑42℃水浴中，依次加入低温活性染料、元明粉和纯碱，恒温染色30min；(3)皂洗：将所述染色后的织物生坯在38℃‑42℃下水洗1‑3次，每次15min；然后皂洗15min；最后分别依次在58℃‑62℃，48℃‑52℃下热洗15min；最后，加软烘干。该染整方法全程低温处理，节能减排，节约水资源，且上染率高。
Description
技术领域
本发明涉及纺织染整技术领域，尤其涉及一种纯棉巾被织物的活性低温染整方法。
背景技术
纯棉巾被织物的染整包括前处理、染色和皂洗三大工艺。传统的染色整理工艺普遍采用高温前处理，并且传统染料大都存在上染率，浮色重等问题。
在前处理过程中，传统用的95-100℃高温练漂工艺温度高，耗时长，加入助剂多，不利于操作，而且得到的毛效仅能达到基本的染色要求。
在染色工艺中，活性染料是反应性染料，上染机理是通过活性染料所带的活性基团，在碱性条件下与纤维素纤维-OH发生交链反应，从而牢固的固着在纤维上。因传统的纯棉巾被织物活性染色工艺选用的常规的染料大都只有一个活性基团，上染率只有60％左右，浮色重，同时传统染料染色温度60-80℃，纯棉巾被织物，因带有毛圈，织物厚重，染色过程中带液量高达400％，因此常规皂洗必须在95-100℃度下进行，且皂洗前后水洗次数多，耗能耗水较大，皂洗色度高，对环境污染严重。
针对水资源一直短缺的现状，国家严格控制产品水吨耗和污水排放，因此急需推广应用新型节能的染整方法
发明内容
本发明所要解决的技术问题是：针对现有技术存在的不足，提供一种纯棉巾被织物的活性低温染整方法，该染整方法全程低温处理，节能减排，节约水资源，且上染率高。
为解决上述技术问题，本发明的技术方案是：
一种纯棉巾被织物的活性低温染整方法，包括以下步骤：
(1)前处理：首先将织造后的织物生坯加入水浴中，加入助剂，升温到82℃-88℃，碱性条件下练漂50min；然后，加入纤维素酶，在中性、47℃-52℃条件下对所述练漂后的织物生坯进行酶洗抛光处理30min。
(2)染色：将所述酶洗抛光后织物生坯放入38℃-42℃水浴中，浴比为1:6-20，依次加入低温活性染料、元明粉和纯碱，其中低温活性染料进料时间15-30min，然后循环10min；元明粉进料时间15-30min，然后循环10min；纯碱进料30min，然后循环10min；全部加料完毕再循环5min，以1-2℃/min的升温速率升温至60℃，恒温染色30min。
(3)皂洗：将所述染色后的织物生坯在38℃-42℃下水洗1-3次，每次15min；然后在58℃-62℃下皂洗15min；最后分别依次在58℃-62℃，48℃-52℃下热洗15min；最后，加软烘干。
作为一种优选的方案，所述步骤(1)的酶洗抛光中，抛光酶又称纤柔酶，加酸调PH值至6-8；柠檬酸用量可根据PH值适量调整，中性纤柔酶用量约1-1.5g/l；脱氧酶0.12ml/l，染色后酵洗之后必须用80℃以上的热水洗，否则会导致织物强力下降。染前酵洗因后面还有染色、皂洗等工序，因此不必灭活。
作为一种优选的方案，所述步骤(1)中，所述练漂，所述助剂为火碱、棉丽净和双氧水，首先火碱和棉丽净同时进料15min，循环10min；然后40℃-60℃下，双氧水进料15min，循环10min；最后升温到82℃-88℃，开始练漂。
作为一种优选的方案，所述步骤(1)中，所述练漂在喷射式溢流机中进行，浴比1:6-15，滚筒转速60-70m/min，主泵压力60-70％。
作为一种优选的方案，所述步骤(1)中，纤维素酶的加入量为所述织物生坯烘干重的1wt％。
作为一种优选的方案，所述步骤(2)中，所述低温活性染料为系列或诺威克隆的FN系列。
作为一种优选的方案，所述步骤(3)中，染色深度高于3％时，皂洗后，在58℃-62℃热洗前，先78℃-82℃热洗15min。
作为一种优选的方案，所述步骤(3)中，所述皂洗选用皂洗剂为阿白特斯DS。
作为一种优选的方案，所述步骤(2)中，所述纯碱进料采用进料曲线为70％，先慢后快，为防止刚开始时因加碱过快，导致的PH值上升高过快，在染料没有充分匀染的情况下过早固色而造成的色花。
由于采用了上述技术方案，本发明的有益效果是：
1)本发明涉及的低温前处理工艺，采用棉丽净是漆酶模拟物与特殊表面活性剂的复配物，适用于全棉散纤维、毛巾布、筒子纱、绞纱、纯棉针织物等的低温练漂加工。能够在85℃下活化双氧水进行有效练漂，且对棉籽壳具有很强的去除效果，经处理的织物白度高，润湿性好，手感柔软。反应温和，纤维的保形好，强力保留率高，避免高温造成细皱纹、纤维脆损等疵病。与传统高温练漂工艺相比，降低10℃,节能30％以上，且操作简单，可缩短加工时间，降低综合成本。所有高温高压溢流机节省降温用冷却水100％，产品失重不高于5％。
2)控制练漂全过程的滚筒转速为60-70m/min，主泵压力为60-65％，以减少产品表面毛羽出现。采用染色前酶洗抛光，省去传统染色后酶洗抛光的80℃灭活步骤，节省成本。
3)纯棉巾被织物带液率高达400％，选用的低温活性染料(系列、诺威克隆的FN系列)含有2-3个活性基团，上染率高达90％以上。低温活性染料具有极高的匀染性、实现染色重现性，从而减低返修率，具有高上染率、易清洗的特性，具有90％以上的上染率和固色率，各项色牢度性能达到4级以上，同时采用60℃的染色加工工艺，极易清洗，为减少皂洗遍数带来可能。
4)采用依次加入染料、助剂的加料顺序，且纯碱的进料曲线为70％，所加工的染色产品获得极高的匀染性、颜色重现性和极低的返修率。
5)采用的低温高效皂洗工艺，高效皂洗剂选用阿白特斯DS，用于纤维素纤维活性染料染色后清洗，具有高清洗力、防沾性和脱盐性，与AVITERA SE染料一起在较低温度60℃能达到需要的水洗效果和柔软手感、透亮布面效果，能使水解染料保持在水中并排出，防止水解染料回沾到纤维上。将常规皂洗温度由95℃皂洗两遍降低为60℃皂洗一遍，且后续水洗次数减少3-4遍，同时避免了常规皂洗工艺因减少水洗次数带来的手感发硬的问题，进一步提高了水洗牢度，从而改善纯棉巾被织物的内在牢度指标与外在手感、蓬松顺滑度等指标。
本发明采用的全流程低温环保高效的染整方法，将上述几个工序有机组合，保证省水、减排、节能、高效的同时获得高质量的产品，提高性价比。
具体实施方式
下面结合实施例，进一步阐述本发明。应理解，这些实施例仅用于说明本发明而不用于限制本发明的范围。此外应理解，在阅读了本发明讲授的内容之后，本领域技术人员可以对本发明作各种改动或修改，这些等价形式同样落于本申请所附权利要求书所限定的范围。
实施例1
颜色：深蓝色
染料配方：
AVITERA SE RED:0.27％,
AVITERA SE YELLOW:0.7％
AVITERA SE DEEP BLUE:2.3％
包括以下步骤：
(1)前处理：首先将织造后的织物生坯加入喷射式溢流机中，浴比1:6,滚筒转速60m/min，主泵压力70％；加入火碱和棉丽净同时进料10min，循环10min；然后40℃下，双氧水进料10min，循环10min；最后升温到85℃，碱性条件下练漂50min。最后，加入纤维素酶，在中性、50℃条件下对所述练漂后的织物生坯进行酶洗抛光处理30min，火碱用量5.33ml/l，棉丽净用量1ml/l。
(2)染色：将所述酶洗抛光后织物生坯放入40℃水浴中，浴比为1:10，依次加入低温活性染料、元明粉和纯碱，循环5min，以1℃/min的升温速率升温至60℃，恒温染色30min；所述低温活性染料进料20min，循环10min；元明粉进料20min，循环10min；纯碱以70％加料曲线进料30min，循环10min。元明粉用量60g/L，纯碱用量20g/L，水位6000L。
(3)皂洗：将所述染色后的织物生坯在40℃下水洗2次，每次15min；然后在60℃下皂洗15min；最后分别依次在60℃，50℃下热洗15min；最后，加软烘干。
实施例2
颜色：灰色,
染料配方：
AVITERA SE RED:0.27％,
AVITERA SE YELLOW:0.39％
AVITERA SE DEEP BLUE:0.3％
包括以下步骤：
(1)前处理：首先将织造后的织物生坯加入喷射式溢流机中，浴比1:11,滚筒转速60m/min，主泵压力70％；加入火碱和棉丽净同时进料10min，循环10min；然后40℃下，双氧水进料10min，循环10min；最后升温到85℃，碱性条件下练漂50min。最后，加入纤维素酶，在中性、50℃条件下对所述练漂后的织物生坯进行酶洗抛光处理30min。火碱用量5.33ml/l，棉丽净用量1ml/l。
(2)染色：将所述酶洗抛光后织物生坯放入40℃水浴中，浴比为1:12，依次加入低温活性染料、元明粉和纯碱，循环5min，以1.5℃/min的升温速率升温至60℃，恒温染色30min；所述低温活性染料进料15min，循环10min；元明粉进料15min，循环10min；纯碱以70％加料曲线进料30min，循环10min。元明粉用量40g/L，纯碱用量15g/L，水位6000L。
(3)皂洗：将所述染色后的织物生坯在40℃下水洗2次，每次15min；然后在60℃下皂洗15min；最后分别依次在60℃，50℃下热洗15min；最后，加软烘干。
以上实施例仅用以说明本发明的技术方案，而非对其进行限制；尽管参照前述实施例对本发明进行了详细的说明，对于本领域的普通技术人员来说，依然可以对前述实施例所记载的技术方案进行修改，或者对其中部分技术特征进行等同替换；而这些修改或替换，并不使相应技术方案的本质脱离本发明所要求保护的技术方案的精神和范围。
Claims (8)
1.一种纯棉巾被织物的活性低温染整方法，其特征在于，包括以下步骤：
(1)前处理：首先将织造后的织物生坯加入水浴中，加入助剂，升温到82℃-88℃，碱性条件下练漂50min；然后，加入纤维素酶，在中性、47℃-52℃条件下对所述练漂后的织物生坯进行酶洗抛光处理30min；
(2)染色：将所述酶洗抛光后织物生坯放入38℃-42℃水浴中，浴比为1:6-20，依次加入低温活性染料、元明粉和纯碱，其中低温活性染料进料时间15-30min，然后循环10min；元明粉进料时间15-30min，然后循环10min；纯碱进料30min，然后循环10min；全部加料完毕再循环5min，以1-2℃/min的升温速率升温至60℃，恒温染色30min；
(3)皂洗：将所述染色后的织物生坯在38℃-42℃下水洗1-3次，每次15min；然后在58℃-62℃下皂洗15min；之后分别依次在58℃-62℃，48℃-52℃下热洗15min；最后，加软烘干。
2.如权利要求1所述的纯棉巾被织物的活性低温染整方法，其特征在于，所述步骤(1)中，所述酶洗抛光，将练漂后的织物生坯放入水浴中，加入柠檬酸，调节PH值至6-8；并加入中性纤柔酶1-1.5g/l和过氧化氢酶0.10-0.15ml/l处理，然后用80℃-95℃热水洗。
3.如权利要求1所述的纯棉巾被织物的活性低温染整方法，其特征在于，所述步骤(1)中，所述练漂中，所述助剂为火碱、棉丽净和双氧水，首先火碱和棉丽净同时进料15min，循环10min；然后40℃-60℃下，双氧水进料15min，循环10min；最后升温到82℃-88℃，开始练漂。
4.如权利要求1所述的纯棉巾被织物的活性低温染整方法，其特征在于，所述步骤(1)中，所述练漂在喷射式溢流机中进行，浴比1:6-15，滚筒转速60-70m/min，主泵压力60-70％。
5.如权利要求1所述的纯棉巾被织物的活性低温染整方法，其特征在于，所述步骤(1)中，所述纤维素酶的加入量为所述织物生坯烘干重的1wt％。
6.如权利要求1所述的纯棉巾被织物的活性低温染整方法，其特征在于，所述步骤(2)中，所述低温活性染料为SE系列或诺威克隆的FN系列。
7.如权利要求1所述的纯棉巾被织物的活性低温染整方法，其特征在于，所述步骤(3)中，染色深度高于3％时，皂洗后，在58℃-62℃热洗前，先78℃-82℃热洗15min。
8.如权利要求1所述的纯棉巾被织物的活性低温染整方法，其特征在于，所述步骤(3)中，所述皂洗选用的皂洗剂为阿白特斯DS。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610769106.7A CN106245314A (zh) | 2016-08-30 | 2016-08-30 | 一种纯棉巾被织物的活性低温染整方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610769106.7A CN106245314A (zh) | 2016-08-30 | 2016-08-30 | 一种纯棉巾被织物的活性低温染整方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106245314A true CN106245314A (zh) | 2016-12-21 |
Family
ID=58079527
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610769106.7A Pending CN106245314A (zh) | 2016-08-30 | 2016-08-30 | 一种纯棉巾被织物的活性低温染整方法 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106245314A (zh) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106491029A (zh) * | 2016-12-30 | 2017-03-15 | 孚日集团股份有限公司 | 一种耐漂花灰毛巾的制造工艺 |
| CN107201679A (zh) * | 2017-06-13 | 2017-09-26 | 淄博大染坊丝绸集团有限公司 | 一种活性染料染纤维素纤维低温皂洗工艺 |
| CN109629267A (zh) * | 2018-12-22 | 2019-04-16 | 利郎(中国)有限公司 | 高光汗色牢度的活性染料染色工艺 |
| CN109680518A (zh) * | 2019-01-26 | 2019-04-26 | 孚日集团股份有限公司 | 一种单面巾被织物的染色方法 |
| CN110359296A (zh) * | 2019-07-02 | 2019-10-22 | 福建凤竹纺织科技股份有限公司 | 一种中小学生校服面料的绿色染色工艺 |
| CN112695535A (zh) * | 2020-12-23 | 2021-04-23 | 互太(番禺)纺织印染有限公司 | 一种涤棉混纺织物的抛光方法及其应用 |
| CN113834786A (zh) * | 2021-08-09 | 2021-12-24 | 鲁丰织染有限公司 | 前处理下布色差品质的快速检测方法 |
| CN114000363A (zh) * | 2020-07-28 | 2022-02-01 | 青岛富润达纺织有限公司 | 一种活性染料低温加料染色方法 |
| CN114197223A (zh) * | 2022-02-08 | 2022-03-18 | 青岛华绵水洗制衣有限公司 | 一种适用于汗布的染色处理工艺 |
| CN114892426A (zh) * | 2022-03-31 | 2022-08-12 | 河北三利毛纺有限公司 | 一种活性染料染色氧漂方法 |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6083739A (en) * | 1997-09-29 | 2000-07-04 | Novo Nordisk Biochem North America, Inc. | Treatment of cellulose fabrics with cellulases |
| CN102121197A (zh) * | 2010-12-31 | 2011-07-13 | 山东滨州亚光毛巾有限公司 | 一种毛巾处理工艺 |
| CN102561064A (zh) * | 2010-12-23 | 2012-07-11 | 福建凤竹纺织科技股份有限公司 | 一种纯棉织物的低温染色工艺 |
| CN103276582A (zh) * | 2013-04-02 | 2013-09-04 | 广东德美精细化工股份有限公司 | 一种棉针织物练漂、染色、皂洗全流程低温染整加工工艺 |
| CN103469619A (zh) * | 2013-09-12 | 2013-12-25 | 湖州金塔地纺织厂 | 一种纺织品的染整工艺 |
-
2016
- 2016-08-30 CN CN201610769106.7A patent/CN106245314A/zh active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6083739A (en) * | 1997-09-29 | 2000-07-04 | Novo Nordisk Biochem North America, Inc. | Treatment of cellulose fabrics with cellulases |
| CN102561064A (zh) * | 2010-12-23 | 2012-07-11 | 福建凤竹纺织科技股份有限公司 | 一种纯棉织物的低温染色工艺 |
| CN102121197A (zh) * | 2010-12-31 | 2011-07-13 | 山东滨州亚光毛巾有限公司 | 一种毛巾处理工艺 |
| CN103276582A (zh) * | 2013-04-02 | 2013-09-04 | 广东德美精细化工股份有限公司 | 一种棉针织物练漂、染色、皂洗全流程低温染整加工工艺 |
| CN103469619A (zh) * | 2013-09-12 | 2013-12-25 | 湖州金塔地纺织厂 | 一种纺织品的染整工艺 |
Non-Patent Citations (4)
| Title |
|---|
| 吴黎丽等: "天丝毛绒混纺织物印花工艺研究", 《针织工业》 * |
| 宋心: "全棉针织物低温全流程工艺研究", 《中国优秀硕士学位论文全文数据库 工程科技I辑》 * |
| 谢峥等: "节能降本的染整技术", 《印染》 * |
| 豆丁: "低温练漂剂棉丽净应用实例", 《HTTP://WWW.DOCIN.COM/P-970037149.HTML》 * |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106491029A (zh) * | 2016-12-30 | 2017-03-15 | 孚日集团股份有限公司 | 一种耐漂花灰毛巾的制造工艺 |
| CN107201679A (zh) * | 2017-06-13 | 2017-09-26 | 淄博大染坊丝绸集团有限公司 | 一种活性染料染纤维素纤维低温皂洗工艺 |
| CN107201679B (zh) * | 2017-06-13 | 2019-06-21 | 淄博大染坊丝绸集团有限公司 | 一种活性染料染纤维素纤维低温皂洗工艺 |
| CN109629267A (zh) * | 2018-12-22 | 2019-04-16 | 利郎(中国)有限公司 | 高光汗色牢度的活性染料染色工艺 |
| CN109629267B (zh) * | 2018-12-22 | 2022-06-03 | 利郎(中国)有限公司 | 高光汗色牢度的活性染料染色工艺 |
| CN109680518A (zh) * | 2019-01-26 | 2019-04-26 | 孚日集团股份有限公司 | 一种单面巾被织物的染色方法 |
| CN110359296A (zh) * | 2019-07-02 | 2019-10-22 | 福建凤竹纺织科技股份有限公司 | 一种中小学生校服面料的绿色染色工艺 |
| CN114000363A (zh) * | 2020-07-28 | 2022-02-01 | 青岛富润达纺织有限公司 | 一种活性染料低温加料染色方法 |
| CN112695535A (zh) * | 2020-12-23 | 2021-04-23 | 互太(番禺)纺织印染有限公司 | 一种涤棉混纺织物的抛光方法及其应用 |
| CN113834786A (zh) * | 2021-08-09 | 2021-12-24 | 鲁丰织染有限公司 | 前处理下布色差品质的快速检测方法 |
| CN113834786B (zh) * | 2021-08-09 | 2024-04-12 | 鲁丰织染有限公司 | 前处理下布色差品质的快速检测方法 |
| CN114197223A (zh) * | 2022-02-08 | 2022-03-18 | 青岛华绵水洗制衣有限公司 | 一种适用于汗布的染色处理工艺 |
| CN114197223B (zh) * | 2022-02-08 | 2023-12-19 | 青岛华绵水洗制衣有限公司 | 一种适用于汗布的染色处理工艺 |
| CN114892426A (zh) * | 2022-03-31 | 2022-08-12 | 河北三利毛纺有限公司 | 一种活性染料染色氧漂方法 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106245314A (zh) | 一种纯棉巾被织物的活性低温染整方法 | |
| CN104762839B (zh) | 尼龙/涤纶弹力针织面料的低温染色工艺 | |
| CN106368014B (zh) | 一种莫代尔/棉混纺织物染色工艺 | |
| CN104018369B (zh) | 蚕丝交织提花织物染色工艺 | |
| CN104911929A (zh) | 棉或黏胶/锦纶/氨纶无缝内衣一浴法染色工艺 | |
| CN101328688B (zh) | 纯棉布料活性染料湿短蒸染深色方法 | |
| CN102162197A (zh) | 涤粘（棉）织物或纱线分散和活性染料同浴浸渍染色方法 | |
| CN103215829A (zh) | 一种棉针织物活性染料练染同浴的方法 | |
| CN107604692A (zh) | 一种涤纶仿麂皮织物染整工艺 | |
| CN103938465A (zh) | 一种化纤长丝的高温染色工艺 | |
| CN101413207B (zh) | 海藻纤维面料的染整工艺 | |
| CN104878619A (zh) | 天然水晶棉纤维及其与其他纤维混纺或交织制品的前处理和染色方法 | |
| CN102444033A (zh) | 锦/人棉/氨纶针织面料的染整方法 | |
| CN104499311A (zh) | 德绒/棉混纺织物一浴一步染色方法 | |
| CN101538806A (zh) | 棉针织物及棉纱线活性染料一浴二步练染方法 | |
| CN102363924A (zh) | 织物抛光染色同浴法 | |
| CN105908532A (zh) | 涤棉或涤黏/锦纶/氨纶多组份面料一浴二步法染色工艺 | |
| CN101509204B (zh) | 麂皮绒面料的新型染整工艺 | |
| CN103924463A (zh) | 一种一浴一步法染中深色棉/锦织物的工艺 | |
| CN101413220B (zh) | 一氯均三嗪及乙烯砜双活性基团活性染料双温染色方法 | |
| CN103526607A (zh) | 拉细羊毛混纺织物的活性染料染色工艺 | |
| CN105088823A (zh) | 棉针织物的练染一浴短流程工艺 | |
| CN104947469A (zh) | 一种涤棉斜纹印染布的漂染同浴处理工艺 | |
| CN1635213A (zh) | 大豆纤维散纤维染色加工方法 | |
| CN108118540A (zh) | 一种涤棉混纺纤维的染色工艺 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161221 |
|
| RJ01 | Rejection of invention patent application after publication |