CN105475385B - A method of preparing the pesticide of prevention bradysia odoriphaga using biogas slurry - Google Patents
A method of preparing the pesticide of prevention bradysia odoriphaga using biogas slurry Download PDFInfo
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- A—HUMAN NECESSITIES
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A01N65/40—Liliopsida [monocotyledons]
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- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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Abstract
The invention discloses a kind of methods for the pesticide preparing prevention bradysia odoriphaga using biogas slurry, to crossing in the biogas slurry after 200 mesh sieve, it is added after flocculant stirs evenly and stands 5 8h, then take supernatant, addition herb liquid, which is uniformly mixed, in supernatant obtains pesticide, and the volume ratio of the supernatant and herb liquid is 3:1‑4:3.The beneficial effects of the invention are as follows：The control method biogas slurry of low cost generated using kitchen garbage solves the process problem of product after garbage disposal, of low cost, turn waste into wealth；Biogas slurry plants effective organic fertilizer source as leek, and the nutrient needed for supply leek growth effectively raises leek yield and quality.Nontoxic to people and animals, green pollution-free can replace domestic chemistry used at present, chemical industry synthesis pesticide to the not broken ring of the Nature, free from environmental pollution.The control method is tested by large area, it was demonstrated that the control effect of bradysia odoriphaga is preferable, not existing visible bradysia odoriphaga harm, while can increase the yield of leek.
Description
Technical field
The present invention relates to technical field of pesticide, more particularly to the method for a kind of pesticide preparing prevention bradysia odoriphaga using biogas slurry.
Background technology
Bradysia odoriphaga is the larva of Diptera category Bradysia odoriphaga.Bradysia odoriphaga foraging territories are wider, can endanger Liliaceae, Chenopodiaceae,
30 various vegetables such as composite family, Curcurbitaceae, Cruciferae, Umbelliferae, the wherein aggrieved most serious of leek.The master that leek is planted in China
More universal, occurring area up to 90% occurs for producing region, the worm.Leek field attacked trees rate causes fragrant-flowered garlic generally 20% or more
Dish production loss is between 30%~80%.Statistics shows the probability that is infected by bradysia odoriphaga of leek after growth 2 years up to 80%
Left and right, in particular with the increase of anti-season leek and hotbed chives production, leek is increased year by year by the probability that bradysia odoriphaga infects, some ground
Area nearly reaches 100%.Bradysia odoriphaga is a kind of subterranean pest-insect of stubbornness, is the crushing pest for endangering leek growth.Bradysia odoriphaga larva master
It is clustered in underground, on the bulb of leek underground part, moth food bulb and tender shoots.After leek is aggrieved, commodity value is gently then influenced,
It is heavy then leek bulb is caused partly or wholly to rot, make the ground blade of leek it is thin and weak it is withered and yellow, wilt and rot or even dead in flakes,
Greatly compromise the interests of fragrant-flowered garlic agriculture.
A large amount of generations of bradysia odoriphaga are rapid plus its breeding, seriously affected the economic benefit of leek.It is carried to effect a radical cure bradysia odoriphaga
Root is gone out and has dialled native Disinsection method, fly net and sugar-vinegar liquid trapping method, foundation earthing, the decomposed deep placement of organic fertilizer, pick root at crop rotation
Cool soil, plant ash pull out dry, bioanalysis etc., and still, these methods have heavy workload, and efficiency is low, and input cost is high, goes out except fragrant-flowered garlic
The deficiencies of less effective of maggot.Killing bradysia odoriphaga at present, quickly and effectively method is still chemical method.The profession of national approved applications is anti-
The drug of bradysia odoriphaga is controlled mostly based on the strong phoxim of absorbability (organophosphorus insecticide) and chlopyrifos, but the harvest time of leek
It is short, not up to safety interval of pesticide pollution when leek is gathered in, and fragrant-flowered garlic agriculture has also been unable to get using the quantity and frequency of such drug
Effect control；While killing bradysia odoriphaga, soil causes its degradation speed slow the strong adsorptivity of pesticide, on the leek of some areas
Excessive pesticide residues also tend to be absorbed into vivo by leek.With the application of such pesticide, bradysia odoriphaga is also more next to the resistance of pesticide
It is stronger, force fragrant-flowered garlic agriculture go to apply more high poison in violation of rules and regulations, more effective 3911,1605 etc. pesticides form vicious circle, lead to leek agriculture
Medicine residual is exceeded.The leek after bradysia odoriphaga is killed due to the use of highly toxic pesticide, growth and development is unaffected, meanwhile, in leek
Can not also it differentiate in appearance, therefore, often this " malicious leek " is eaten in daily life, malicious leek event takes place frequently in recent years, even
Continuous malicious leek exposure event causes human body greatly to injure severe patient's even threat to life so that consumer " talks fragrant-flowered garlic color
Become ", seriously affect the economic interests of vegetable grower and the food security of consumer.
In addition the applications of pesticide have been arrived in natural environment, although having achieved the purpose that want, also bring pollution simultaneously
Problem.If environment and Pesticide Residues amount are exceeded, the mankind, other organisms or even the entire ecosystem can be caused
Harmful effect.Pesticide enters after natural ecological environment, can enter human body by approach such as respiratory tract, alimentary canal, skins.Such as
Fruit reagent toxicity is larger, it is possible to cause acute poisoning or subacute poisoning, or even cause life danger.Although some medicaments
Acute toxicity is little, but if property is stablized, is not easily decomposed, disappears after use, will remain in water, air, crops, agricultural production
In product or aquatic products, livestock products, human body is eventually entered into, slow poisoning is caused.Meanwhile pollution by pesticides can also cause other biological
Poisoning is even dead, so that destroying the ecological balance, it is therefore necessary to residual and the pollution for controlling pesticide, to reduce to human society
Influence and harm.
In addition, the yield of China's kitchen garbage is increasing in recent years, estimation account for the 50% of domestic waste total amount with
On；It endangers the appearance of the city health for directly affecting city, leads to insect pest, the plague of rats or even transmission；More seriously, part
Kitchen garbage is unprocessed and is processed into " gutter oil " into market or flows to underground farm as feed, seriously threatens people
The life and health of the people.The main processing ways of kitchen garbage include both at home and abroad at present：Burning, compost, landfill, Fodder making and detest
Aerobe fermentation.A variety of different processing methods and equipment have also been invented in people.Such as application number：201010224280.6 specially
The sharp entitled integrated conduct method using kitchen garbage gas system fertilizer.Application number：201110339482.X patent name is a kind of
Municipal organic waste combined anaerobic treatment process and equipment.Application number 201210532285.4, the recycling of patent name kitchen garbage
Using method etc. be disclose will rubbish carry out anaerobic fermentation after be divided into biogas, biogas slurry and biogas residue handle application respectively.
Biogas slurry is otherwise known as anaerobic fermented liquid, is the various organic matters such as people, animal excrement and agricultural crop straw, weeds through anaerobism
Liquid residue after fermentation.The conventional nutrients that crops need in biogas slurry have the multiple elements such as nitrogen, phosphorus, potassium, magnesium, calcium few
Amount trace element, active organic component have the plant hormones such as humic acid, heteroauxin, lactic acid bacteria, gibberellin, the basic element of cell division, B
Family vitamin has B1, B2, B5, B6, B11, B12, also contain there are many amino acid, protein, hydrolase and a variety of inorganic acids and
The organic molecules such as certain antibiotic, coordinative role is present in the form of available nutrient and biological pesticide mutually between these ingredients
In biogas slurry, it directly can rapidly be absorbed and kill harmful levels of pathogens and worm's ovum and promote the growth of the plants such as crops and flowers,
Therefore biogas slurry could also say that a kind of medicine fertilizer.
But these effective component contents are relatively low in biogas slurry, for concentration generally 10% or so, remaining is all free state
Water and plant fiber, silt, bacterium, clay, colloid, pesticide residue, suspended matter and the organic matter containing fishy odor, are used as
Often dosage is big when Crop fertilizer, and effect is poor, thus peasant is unwilling to make fertilizer using biogas slurry more.If biogas slurry is arranged everywhere
It puts, not only waste of resource, but also pollutes environment, it is of high cost if handled by sewage, and be difficult to handle.Crops and flower
The plants such as grass directly apply this biogas slurry, do not meet agricultural health standard, can cause the secondary pollution in farmland, can also be to growth conditions
And growing environment adversely affects, also the amount of directly this biogas slurry of application is also bigger, and this certainly will increase biogas slurry
Transportation cost and labor intensity still more use fertile season, biogas slurry that cannot be fully used, the unordered discharge of extra biogas slurry non-
The pollution and waste for causing environment need further processed in order to avoid transmission and soil pollution as fertilizer
Rear is handled to can be used.
The great attention of the leek safety in production of people is aroused in poisoning caused by a large amount of excessive problems of pesticide residue.It is many
More agriculture practitioners also recognizes the seriousness of such event, also has lofty ideals for finding environmentally friendly method, also work out
The biological agent of some prevention bradysia odoriphagas, but since cost is higher, effect does not obtain on a large scale not as good as reasons such as chemical pesticides
It is effective to promote and apply.
Therefore, how it is cheap effectively kill bradysia odoriphaga, improve the safety of food, people made to trust that edible leek is ability
One of the important topic of field technique personnel research.And the generation of kitchen garbage, current environment ability to bear is seriously tested, it will
Classify after rubbish timely processing and rationally utilize, turns waste into wealth extremely urgent.
Invention content
In order to meet the needs of administering bradysia odoriphaga and making full use of biogas slurry, biogas slurry system is utilized an embodiment of the present invention provides a kind of
The method of the pesticide of standby prevention bradysia odoriphaga.
In order to achieve the above-mentioned object of the invention, the present invention provides a kind of sides for the pesticide preparing prevention bradysia odoriphaga using biogas slurry
Method is added after flocculant stirs evenly to crossing in the biogas slurry after 200 mesh sieve and stands 5-8h, supernatant is then taken, in supernatant
Middle addition herb liquid, which is uniformly mixed, obtains pesticide, and the volume ratio of the supernatant and herb liquid is 3:1-4:3.
Carrying out the biogas slurry of processing generation using kitchen garbage in the prior art can use, but biogas slurry must be taken from just
The marsh gas fermentation pool of normal aerogenesis 3 months or more to be fermented using kitchen garbage.
Chinese medicine in the herb liquid includes following raw medicinal material：Humulus grass, rhizoma atractylodis, honeysuckle, purslane, juglandis folia, phoenix
It is preced with grass, swallow tail, cannalike dona rhizome and pinkflower ecdysanthera root and leaf.
The mass parts of each raw medicinal material are in the herb liquid：15-20 parts of humulus grass, 5-10 parts of rhizoma atractylodis, honeysuckle 20-26
Part, 13-18 parts of purslane, 5-12 parts of juglandis folia, 3-8 parts of sword brake herb, 12-21 parts of swallow tail, 7-14 parts of cannalike dona rhizome and pinkflower ecdysanthera
12-16 parts of rattan.
The mass parts of each raw medicinal material are in the herb liquid：15 parts of humulus grass, 8 parts of rhizoma atractylodis, 26 parts of honeysuckle, purslane 18
Part, 11 parts of juglandis folia, 3 parts of sword brake herb, 16 parts of swallow tail, 14 parts of cannalike dona rhizome and 12 parts of pinkflower ecdysanthera root and leaf.
The mass parts of each raw medicinal material are in the herb liquid：18 parts of humulus grass, 10 parts of rhizoma atractylodis, 23 parts of honeysuckle, purslane
14 parts of 15 parts, 5 parts of juglandis folia, 6 parts of sword brake herb, 21 parts of swallow tail, 7 parts of cannalike dona rhizome and pinkflower ecdysanthera root and leaf.
The mass parts of each raw medicinal material are in the herb liquid：20 parts of humulus grass, 5 parts of rhizoma atractylodis, 20 parts of honeysuckle, purslane 13
Part, 12 parts of juglandis folia, 8 parts of sword brake herb, 12 parts of swallow tail, 10 parts of cannalike dona rhizome and 16 parts of pinkflower ecdysanthera root and leaf.
The biogas slurry is derived from the fermentation vat to ferment using kitchen garbage of normal gas producing 3 months or more.
The flocculant is aluminium polychloride and polyacrylamide, and aluminium polychloride addition in biogas slurry is 3.2-
3.3g/L, polyacrylamide addition in biogas slurry is 0.01-0.015g/L.
The preparation method of the herb liquid includes the following steps：The first step presses humulus grass, swallow tail, rhizoma atractylodis and honeysuckle
Ratio mixes to obtain mixture one, uses the ethyl alcohol that determining alcohol is 70%~80% as solvent, uses percolation with 0.3- per minute
Slowly diacolation, collection percolate are concentrated under reduced pressure simultaneously drying, obtain dry cream, be ground into powder one, be added the speed of 0.8ml
The quality of ethyl alcohol is 3~5 times of one mass of mixture；
Second step mixes purslane, juglandis folia, sword brake herb, cannalike dona rhizome and pinkflower ecdysanthera root and leaf in proportion, obtains mixture two,
The distilled water relative to 9~10 times of two mass of mixture is added, decocts 2~4 hours, filtering obtains the first filtered fluid；By filter residue
The distilled water relative to 3~5 times of filter residue quality is added, decocts 1~2 hour, filtering obtains the second filtered fluid；Merge the first mistake
Filtrate and the second filtered fluid are concentrated under reduced pressure, dry, obtain dry cream, are ground into powder two；
Third walks, and the powder two that powder one and second step that the first step obtains obtain is mixed, is added relative to mixed powder
The distilled water of 3~5 times of amounts of last quality, 0.5~0.8 times of honey measured, stir evenly acquisition herb liquid.
The preparation method of the herb liquid includes the following steps：
Step 1：It by the raw medicinal material, is mixed in the ratio, it is the 6- of raw material gross weight to add suitable water, water consumption
It 10 times, impregnates 1-2 hours；
Step 2：Soaked raw medicinal material elder generation intense fire is fried open, turns that slow boiling is continuous to be decocted, after decocting 1-2 hour, filters to obtain and filter
The water of 3-4 times of the filter residue weight is added into filter residue for liquid one and filter residue, after decocting 0.5-1 hours, filters to take filtrate and obtains filtrate
Two, filtrate one and filtrate two are uniformly mixed to the herb liquid of the as present invention.
The advantageous effect that technical solution provided in an embodiment of the present invention is brought is：
The control method biogas slurry of low cost generated using kitchen garbage solves the process problem of product after garbage disposal,
It is of low cost, turn waste into wealth.Biogas slurry plants effective organic fertilizer source as leek, and supply leek grows required nutrient,
Effectively raise leek yield and quality.It is nontoxic to people and animals, green pollution-free, to the not broken ring of the Nature, not dirty
Environment is contaminated, domestic chemistry used at present, chemical industry synthesis pesticide can be replaced.The raw material sources of the present invention are extensive, manufacture craft letter
Single, energy consumption is small, and manufacturing cost is cheap.Leek solves without any pesticide residue, the edible safety problem of leek.
Control effect is stablized, which tests by large area, after this method, it was demonstrated that the control effect of bradysia odoriphaga
Preferably, not existing visible bradysia odoriphaga harm, while the yield of leek can be increased, it can be used in each period of farming growth,
Meet farmers'application habit, is not necessarily to safety interval.
Specific implementation mode
Bad for current pesticide improvement bradysia odoriphaga effect, pesticide residue is high, and problem of high cost, the present invention provides a kind of
The method that the pesticide of prevention bradysia odoriphaga is prepared using biogas slurry.
The pharmacology of each Chinese medicine material medicinal material is as follows in pesticide：
Humulus grass：Alias uproots plants after their edible portions have been harvested, draws and draw rattan, cairo morningglory root or leaf, le grass, great Ye cairo morningglory root or leafs, draw dog egg, cut people rattan.Source Moraceae
The herb of humulus plants humulus grass.Nature and flavor are sweet, bitter, tremble with fear.It is clearing heat and detoxicating, inducing diuresis to remove edema.For pulmonary tuberculosis hectic fever, enterogastritis, dysentery
Disease, cold, fever, difficult urination, pyelonephritis, acute nephritis, cystitis, stone in urinary system；Carbuncle furuncle poison is controlled in external application, eczema,
Venomous snake bite.
Rhizoma atractylodis：The red art of alias（Tao Hongjing）, Ma Ji（《Say that text system passes》）, green art（Open ceremonial dress for royalty《Water south writing brush note》）, magic arts（《Guiding principle
Mesh》）.For the rhizome of feverfew RHIZOMA ATRACTYLODIS IANCEAE or Atractylis chinensis etc..Returns spleen, stomach.Major function invigorating the spleen, eliminating dampness, Xie Yu are warded off dirty.
Wet soreness, burnout are controlled, gastral cavity ruffian abdominal distension is lost the appetite, vomiting, diarrhea, dysentery, malaria, phlegm and retained fluid, oedema, feel cold,
Wind-cold-dampness arthralgia, atrophy, yctalopia.
Honeysuckle：It is sweet, it trembles with fear.Return lung, the heart, stomach.It is clearing heat and detoxicating, wind-heat dissipating.For carbuncle swells furunculosis, larynx numbness, erysipelas, heat
Malicious bloody flux, anemopyretic cold, warm disease heating.
Purslane：Acid is trembled with fear.Clearing heat and promoting diuresis, removing pattogenic heat from the blood and toxic material from the body.For bacillary dysentery, acute gastroenteritis, acute appendicitis,
Mastitis, hemorrhoid hemorrhage, leukorrhea；Furuncle swelling toxin, eczema, herpes zoster are controlled in external application.
Juglandis folia：Medicine elementary source：For the leaf of juglandaceae plant English walnut.It is bitter；It is puckery；It is mild-natured.Restrain stop-band；Desinsection is subsided a swelling.It is main
Women leukorrhea；Mange；Elephantiasis crus.
Sword brake herb：Alias phoenix grass（《Sward pharmacological property is standby to be wanted》）, phoenix-tail fern（《The south of the Five Ridges is gathered medicinal herbs record》）, trident grass（《It plants in Guangzhou
Object will》）, small phoenix tail, Uncinata Spikemoss Herb（《South of the Five Ridges herbal》）, mountain phoenix tail, well side are alizarin（《Guangdong Chinese medicine》）.For Pteridaceae plant sword
The herb of leaf brake fern.Lightly seasoned slight bitter, it is cold in nature.Heat-clearing, dampness removing, cool blood, removing toxic substances.Control dysentery, malaria, jaundice, gonorrhoea, lower blood,
Metrorrhagia, traumatic injury, tonsillitis, parotitis, sore, eczema.
Swallow tail：Alias slice leaf, mouse bell.Passifloraceae swallow tail, with all herbal medicine.Bitter, micro- sweet, warm.Tonifying lung benefit
Gas, anti-inflammatory, sterilization.Cure mainly dysentery, pulmonary tuberculosis, bronchitis.Input manure pit sump kills maggot, wriggler.
Cannalike dona rhizome：Alias dagger-axe swallow [Dai Nationality's name].Marantaceae cannalike dona rhizome, is used as medicine with root tuber or stem.It is light, it is cool.It is clearing heat and detoxicating, cough-relieving
Dingchuan, anti-inflammation and sterilization.Cure mainly pulmonary tuberculosis, tracheitis, bronchitis, asthma, high fever, children's measles, merging pneumonia, flu, hair
Heat, various skin diseases.
Pinkflower ecdysanthera root and leaf：Alias head woods oozes（《Guangzhou flora》）, Prunella vulgaris（《Luchuan book on Chinese herbal medicine》）, Caulis Fissistigmae, the wind certain kind of berries, sour rattan
（《Guangxi Chinese medicinal herbal》）.For the root and leaf of apocynaceae plant acid leaf glue rattan.Acid;It is mild-natured.Return liver warp.It is clearing heat and detoxicating;Dampness removing
It is stagnant;Activating blood circulation and reducing swelling.Main abscess of throat；Stomatitis；Enteritis；Chronic nephritis；Food stagnation turgor；Carbuncle sore tumefacting virus；Arthralgia pain due to rheumatism；Bruise is swollen
Bitterly.
PB1 gene：Purchased from Zhen Yu water-purifying materials factory of Gongyi City, yellow powdery solid, Al2O3 mass fractions are about
It is 30%.
Polyacrylamide PAM：Purchased from Chinese medicines group, relative molecular mass>3000000, active ingredient>85%.
The present invention will be described in detail below with reference to the drawings of preferred embodiments, whereby to the present invention how applied technology method
Technical problem is solved, and the realization process for reaching technique effect can fully understand and implement.
Embodiment 1
A method of flocculation is added to crossing in the biogas slurry after 200 mesh sieve in the pesticide preparing prevention bradysia odoriphaga using biogas slurry
Agent stands 5h after stirring evenly, then take supernatant, and addition herb liquid, which is uniformly mixed, in supernatant obtains pesticide, the supernatant
The volume ratio of liquid and herb liquid is 2:1.
The quality of each raw medicinal material is in herb liquid：Humulus grass 15kg, rhizoma atractylodis 8kg, honeysuckle 26kg, purslane 18kg, Hu
Peach leaf 11kg, sword brake herb 3kg, swallow tail 16kg, cannalike dona rhizome 14kg and pinkflower ecdysanthera root and leaf 12kg.
What biogas slurry was derived from sub- kitchen garbage treatment plant normal gas producing of Chongqing City's black stone 3 months or more utilizes kitchen garbage to carry out
The fermentation vat of fermentation.
Flocculant be aluminium polychloride and polyacrylamide, aluminium polychloride in biogas slurry addition be 3.2g/L, poly- third
Acrylamide addition in biogas slurry is 0.012g/L.
The preparation method of herb liquid includes the following steps：The first step, in proportion by humulus grass, swallow tail, rhizoma atractylodis and honeysuckle
Mix to obtain mixture one, use the ethyl alcohol that determining alcohol is 70% as solvent, use percolation with the speed of 0.8ml per minute slowly
Diacolation collects percolate, is concentrated under reduced pressure and dry, obtains dry cream, be ground into powder one, and the quality for the ethyl alcohol being added is mixing
5 times of one mass of object；
Second step mixes purslane, juglandis folia, sword brake herb, cannalike dona rhizome and pinkflower ecdysanthera root and leaf in proportion, obtains mixture two,
The distilled water relative to 10 times of two mass of mixture is added, decocts 2 hours, filtering obtains the first filtered fluid；Phase is added in filter residue
It for 5 times of distilled water of filter residue quality, decocts 2 hours, filtering obtains the second filtered fluid；Merge the first filtered fluid and the second mistake
Filtrate is concentrated under reduced pressure, dry, obtains dry cream, is ground into powder two；
Third walks, and the powder two that powder one and second step that the first step obtains obtain is mixed, is added relative to mixed powder
The distilled water of 3 times of amounts of last quality, 0.5 times of honey measured, stir evenly acquisition herb liquid.
Embodiment 2
A method of flocculation is added to crossing in the biogas slurry after 200 mesh sieve in the pesticide preparing prevention bradysia odoriphaga using biogas slurry
Agent stands 6h after stirring evenly, then take supernatant, and addition herb liquid, which is uniformly mixed, in supernatant obtains pesticide, the supernatant
The volume ratio of liquid and herb liquid is 4:3.
The quality of each raw medicinal material is in herb liquid：Humulus grass 18kg, rhizoma atractylodis 10kg, honeysuckle 23kg, purslane 15kg, Hu
Peach leaf 5kg, sword brake herb 6kg, swallow tail 21kg, cannalike dona rhizome 7kg and pinkflower ecdysanthera root and leaf 14kg.
What biogas slurry was derived from sub- kitchen garbage treatment plant normal gas producing of Chongqing City's black stone 3 months or more utilizes kitchen garbage to carry out
The fermentation vat of fermentation.
Flocculant be aluminium polychloride and polyacrylamide, aluminium polychloride in biogas slurry addition be 3.3g/L, poly- third
Acrylamide addition in biogas slurry is 0.015g/L.
The preparation method of the herb liquid includes the following steps：The first step presses humulus grass, swallow tail, rhizoma atractylodis and honeysuckle
Ratio mixes to obtain mixture one, uses the ethyl alcohol that determining alcohol is 80% as solvent, uses percolation with the speed of 0.3ml per minute
Slowly diacolation collects percolate, is concentrated under reduced pressure and dry, obtains dry cream, be ground into powder one, the quality for the ethyl alcohol being added is
3 times of one mass of mixture；
Second step mixes purslane, juglandis folia, sword brake herb, cannalike dona rhizome and pinkflower ecdysanthera root and leaf in proportion, obtains mixture two,
The distilled water relative to 9 times of two mass of mixture is added, decocts 4 hours, filtering obtains the first filtered fluid；Phase is added in filter residue
It for 3 times of distilled water of filter residue quality, decocts 1 hour, filtering obtains the second filtered fluid；Merge the first filtered fluid and the second mistake
Filtrate is concentrated under reduced pressure, dry, obtains dry cream, is ground into powder two；
Third walks, and the powder two that powder one and second step that the first step obtains obtain is mixed, is added relative to mixed powder
Distilled water, 0.8 times of the honey of 5 times of amounts of last quality, stir evenly acquisition herb liquid.
Embodiment 3
A method of flocculation is added to crossing in the biogas slurry after 200 mesh sieve in the pesticide preparing prevention bradysia odoriphaga using biogas slurry
Agent stands 8h after stirring evenly, then take supernatant, and addition herb liquid, which is uniformly mixed, in supernatant obtains pesticide, the supernatant
The volume ratio of liquid and herb liquid is 3:1.
The quality of each raw medicinal material is in herb liquid：Humulus grass 20kg, rhizoma atractylodis 5kg, honeysuckle 20kg, purslane 13kg, Hu
Peach leaf 12kg, sword brake herb 8kg, swallow tail 12kg, cannalike dona rhizome 10kg and pinkflower ecdysanthera root and leaf 16kg.
What biogas slurry was derived from sub- kitchen garbage treatment plant normal gas producing of Chongqing City's black stone 3 months or more utilizes kitchen garbage to carry out
The fermentation vat of fermentation.
Cationic polyacrylamide addition in biogas slurry is the 0.1% of biogas slurry quality.
The flocculant is aluminium polychloride and polyacrylamide, and aluminium polychloride addition in biogas slurry is 3.2g/L,
Polyacrylamide addition in biogas slurry is 0.01g/L.
The preparation method of herb liquid includes the following steps：Step 1：By the raw medicinal material, mixes, add in the ratio
Suitable water, water consumption are 8 times of raw material gross weight, are impregnated 2 hours；
Step 2：Soaked raw medicinal material elder generation intense fire is fried open, turns that slow boiling is continuous to be decocted, after decocting 1 hour, is filtered to get filtrate
One and filter residue, the water that 3 times of the filter residue weight is added in filter residue filters to take filtrate and obtains filtrate two, by filtrate after decocting 1 hour
One and filtrate two be uniformly mixed be the present invention herb liquid.
1, test method
In Qingdao Vegetable Base, experiment leek kind is that the only son and heir is red, and experiment sets 20 cells, and 5 processing are each to handle
4 repetitions, each plot experiment ground area are 0.5 mu.
1-3 processing is respectively the pesticide prepared using embodiment 1-3 in 5 processing,
Wherein processing 4 directly uses biogas slurry treatment for control group 1；
Processing 5 is blank control group 2, and blank is handled without any method；
Pouring mode is to be poured along root.
2, investigation content
Aggrieved strain rate investigation：With each 10 pier of 2 row of center of housing estate, statistics healthy tree and (, the lodging yellow, soft with blade tip of aggrieved strain number
Subject to).5 before dispenser and after dispenser, 12,20,30d respectively investigate 1 time, investigate 5 times altogether.
Insect population is investigated：The insect population of random searching check plot before dispenser.
Insect population of surviving is investigated：The heart digs 5 pier leek, the inside and outside maggot number of surviving of statistics bulb in the cell for last 1 investigation.Note
Insect population number is recorded, Revision insect recluced rate is calculated.
Investigate total strain number in attacked trees rate (%)=aggrieved strain number × 100/；
Control effect (%)=（The aggrieved aggrieved strain rate of strain rate-treatment region in check plot）The aggrieved strain rate in × 100/ check plot；
Insect population control effect (%)=（Check plot work borer population-treatment region work borer population）× 100/ check plot work borer population；
For each processing prevention bradysia odoriphaga field control effectiveness test result referring to table 1, each embodiment uses the per mu yield of rear leek
（kg）Referring to table 2
1 each processing of table prevents bradysia odoriphaga field control effectiveness test result
The yield of 1 mu of leek after 2 each embodiment use of table（kg）
| 1st batch of non-medication | 2nd batch | 3rd batch | 4th batch | |
| Embodiment 1 | 1286 | 2720 | 2708 | 2695 |
| Embodiment 2 | 1279 | 2746 | 2723 | 2678 |
| Embodiment 3 | 1320 | 2802 | 2759 | 2714 |
| Control group 1 | 1295 | 1856 | 1947 | 1854 |
| Control group 2 | 1335 | 1267 | 1204 | 1092 |
Prevention bradysia odoriphaga effect is can be seen that by above-mentioned data clearly, and leek plant strain growth is vigorous, significantly increases
Production.Using the treatment effect after pesticide of the present invention all it is obvious that the control group for wherein only applying biogas slurry handles insect population control effect
Reach 88.69%.But 1 pesticide of embodiment administers bradysia odoriphaga effect highly significant, it might even be possible to completely kill bradysia odoriphaga.
The per mu yield of leek is than before by the apparent volume increase of the per mu yield of bradysia odoriphaga insect pest after applying pesticides, volume increase reach 100% with
On, than 40% or more the leek per mu yield volume increase for only applying biogas slurry.It can be seen that the synergy of the pesticide of the present invention is remarkably reinforced.
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all the present invention spirit and
Within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention.
Claims (7)
1. a kind of method for the pesticide preparing prevention bradysia odoriphaga using biogas slurry, which is characterized in that into the biogas slurry after the sieve of 200 mesh excessively,
It is added after flocculant stirs evenly and stands 5-8h, then take supernatant, addition herb liquid, which is uniformly mixed, in supernatant obtains agriculture
The volume ratio of medicine, the supernatant and herb liquid is 3:1-4:3；
The flocculant is aluminium polychloride and polyacrylamide, and aluminium polychloride addition in biogas slurry is 3.2-3.3g/L,
Polyacrylamide addition in biogas slurry is 0.01-0.015g/L；
The mass parts of each raw medicinal material are in the herb liquid：15-20 parts of humulus grass, 5-10 parts of rhizoma atractylodis, 20-26 parts of honeysuckle, horse
13-18 parts of bitterroot, 5-12 parts of juglandis folia, 3-8 parts of sword brake herb, 12-21 parts of swallow tail, 7-14 parts of cannalike dona rhizome and pinkflower ecdysanthera root and leaf 12-
16 parts.
2. according to the method described in claim 1, it is characterized in that, the mass parts of each raw medicinal material are in the herb liquid：Humulus
15 parts of grass, 8 parts of rhizoma atractylodis, 26 parts of honeysuckle, 18 parts of purslane, 11 parts of juglandis folia, 3 parts of sword brake herb, 16 parts of swallow tail, cannalike dona rhizome 14
12 parts of part and pinkflower ecdysanthera root and leaf.
3. according to the method described in claim 1, it is characterized in that, the mass parts of each raw medicinal material are in the herb liquid：Humulus
18 parts of grass, 10 parts of rhizoma atractylodis, 23 parts of honeysuckle, 15 parts of purslane, 5 parts of juglandis folia, 6 parts of sword brake herb, 21 parts of swallow tail, cannalike dona rhizome 7
14 parts of part and pinkflower ecdysanthera root and leaf.
4. according to the method described in claim 1, it is characterized in that, the mass parts of each raw medicinal material are in the herb liquid：Humulus
20 parts of grass, 5 parts of rhizoma atractylodis, 20 parts of honeysuckle, 13 parts of purslane, 12 parts of juglandis folia, 8 parts of sword brake herb, 12 parts of swallow tail, cannalike dona rhizome 10
16 parts of part and pinkflower ecdysanthera root and leaf.
5. according to the method described in claim 1, it is characterized in that, the biogas slurry is derived from the fermentation of normal gas producing 3 months or more
Pond.
6. according to any methods of claim 1-5, which is characterized in that the preparation method of the herb liquid includes following step
Suddenly：
Humulus grass, swallow tail, rhizoma atractylodis and honeysuckle are mixed to obtain mixture one by the first step in proportion, are 70%~80% with determining alcohol
Ethyl alcohol as solvent, use percolation with the speed of 0.3-0.8ml per minute slowly diacolation, collect percolate, be concentrated under reduced pressure
And it is dry, dry cream is obtained, is ground into powder one, the quality for the ethyl alcohol being added is 3~5 times of one mass of mixture；
Second step mixes purslane, juglandis folia, sword brake herb, cannalike dona rhizome and pinkflower ecdysanthera root and leaf in proportion, obtains mixture two, is added
It relative to two mass of mixture, 9~10 times of distilled water, decocts 2~4 hours, filtering obtains the first filtered fluid；Filter residue is added
It relative to 3~5 times of distilled water of filter residue quality, decocts 1~2 hour, filtering obtains the second filtered fluid；Merge the first filtered fluid
With the second filtered fluid, it is concentrated under reduced pressure, it is dry, dry cream is obtained, powder two is ground into；
Third walks, and the powder two that powder one and second step that the first step obtains obtain is mixed, is added relative to mixed-powder matter
The distilled water of 3~5 times of amounts of amount, 0.5~0.8 times of honey measured, stir evenly acquisition herb liquid.
7. according to any methods of claim 1-5, which is characterized in that the preparation method of the herb liquid includes following step
Suddenly：
Step 1：By the raw medicinal material, mixed in the ratio, it is 6-10 times of raw material gross weight to add suitable water, water consumption,
It impregnates 1-2 hours；
Step 2：Soaked raw medicinal material elder generation intense fire is fried open, turns that slow boiling is continuous to be decocted, after decocting 1-2 hours, filters to get filtrate one
And filter residue, the water of 3-4 times of the filter residue weight is added into filter residue, after decocting 0.5-1 hours, filters to take filtrate and obtains filtrate two,
Filtrate one and filtrate two are uniformly mixed to the herb liquid of the as present invention.
Priority Applications (3)
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| CN201810084268.6A CN108283190B (en) | 2016-01-28 | 2016-01-28 | Pesticide liquid for preventing and treating Chinese chive maggots and preparation method and application thereof |
| CN201810084867.8A CN108283191B (en) | 2016-01-28 | 2016-01-28 | Preparation method of pesticide for preventing and treating Chinese chive maggots |
| CN201610057665.5A CN105475385B (en) | 2016-01-28 | 2016-01-28 | A method of preparing the pesticide of prevention bradysia odoriphaga using biogas slurry |
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| CN201810084867.8A Division CN108283191B (en) | 2016-01-28 | 2016-01-28 | Preparation method of pesticide for preventing and treating Chinese chive maggots |
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| CN108863552A (en) * | 2018-07-25 | 2018-11-23 | 王其俊 | A kind of selenium-rich biogas slurry Biocidal microbial inoculum and preparation method |
| CN109526999A (en) * | 2018-11-26 | 2019-03-29 | 钱巍 | A kind of biological pesticide and preparation method thereof for crop root part |
| CN109627111A (en) * | 2019-02-26 | 2019-04-16 | 刘立军 | A kind of liquid compound organic fertilizer and preparation method thereof |
| CN110463726A (en) * | 2019-09-16 | 2019-11-19 | 刘善勇 | A kind of leek green production pharmaceutical agent combinations |
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| CN108283191B (en) | 2021-02-02 |
| CN105475385A (en) | 2016-04-13 |
| CN108283190A (en) | 2018-07-17 |
| CN108283191A (en) | 2018-07-17 |
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