CN105193663B - Chinese medicinal liquor soap and preparation method thereof - Google Patents

Chinese medicinal liquor soap and preparation method thereof Download PDF

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Publication number
CN105193663B
CN105193663B CN201510695315.7A CN201510695315A CN105193663B CN 105193663 B CN105193663 B CN 105193663B CN 201510695315 A CN201510695315 A CN 201510695315A CN 105193663 B CN105193663 B CN 105193663B
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soap
chinese medicine
medicine extract
pressure
medicinal liquor
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CN105193663A (en
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郑艳
王洋
史姣姣
庄红
王雪
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Anhui Normal University
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Anhui Normal University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Dermatology (AREA)
  • Microbiology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses Chinese medicinal liquor soap and preparation method thereof, the liquid soap contains following substance:Natural soap kind, alkyl glycosides, methyl orthophosphoric acid, amino acid foaming agent, Chinese medicine extract, sodium chloride, the present invention is compared with prior art, the present invention relies on Chinese herbal medicine extract, does not add alcohol and artificial synthetic essence and preservative and reaches decontamination, sterilization and anticorrosion, the integrated purpose of natural flavouring, with good decontamination, moisturizing, fungistatic effect, product is suitable for human body clean.

Description

Chinese medicinal liquor soap and preparation method thereof
Technical field:
The invention belongs to liquid soaps and preparation method thereof, particularly belong to Chinese medicinal liquor soap and preparation method thereof.
Background technology:
Soap and washing powder can play cleaning, the effect of sterilization to a certain extent, but to the stimulation crowd institute of skin It is known.The such product of long-time service may result in pachylosis, be chapped from the cold and even peel.In comparison, by natural oil and Not only acid-base value is partial to neutrality for product that caustic potash is reacted and manufactured liquid soap, but also contains natural skin care moisturizer Glycerine thus it is even better, also increasingly market is subject to approve.But existing liquid soap in terms of decontamination, antibacterial, anti-corrosion very Difficulty is shown consideration for.In existing product, used decontamination active ingredient is mostly soap, easily generates soap scum and to human body spinosity Swash;Bactericidal, preservative are mostly chemical industry synthesis product such as triclosan, triclocarban, ethyl alcohol, Kathon CG etc. or even including methyl Preservative including isothiazolinone, Form aldehyde release body etc., there are healthy and safe hidden danger.Such as Chinese patent (application number 201210492046.0) the corrosion-resistant mesh of prepared liquid soap product is reached using methyl p-hydroxybenzoate.Chinese patent A kind of Solid/liquid two purpose sterilizing skin moistening perfumed soap that (application number 201310353551.1) provides and preparation method thereof, the fungicide used Can be the one or more in 2- methvl-propionic acid methyl estes, 2 Methylpropionic acid, diethofencarb for fungicide, while using natural flowers Perfume (or spice) replaces compound essence.A kind of liquid soap that Chinese patent (application number 201310663283.3) provides is by adding the dihydro moon Osmanthus enol achievees the purpose that flavouring and contains ethyl alcohol.Chinese patent (application number 201110278332.2) provide liquid soap and its Preparation method, although all using natural constituents, prepared product does not possess bactericidal effect.
The content of the invention:
For the prior art by soap as decontamination active ingredient, by addition compound essence flavouring, by change It learns composite and reaches antiseptic and inhibiting bacteria function purpose.
The 1st purpose offer of the present invention is a kind of to be relied on Chinese herbal medicine extract, not to add alcohol and artificial synthetic essence With preservative and reach decontamination, sterilization and anticorrosion, the natural integrated Traditional Chinese medicine bacteriostatic liquid soap of flavouring.
The 2nd purpose of the present invention is the preparation method of aforesaid liquid soap.
The present invention solve technical problem technical solution be:Chinese medicinal liquor soap, the substance containing following parts by weight:
The natural soap kind is prepared by the following method:
The potassium hydroxide solution of saturation is added in tea oil, is put into high-pressure sterilizing pot, temperature maintain 110-126 DEG C, Pressure 0.01-0.25MPa is reacted 15-45 minutes, is cooled to room temperature, and is sufficiently stirred after its hardening, is placed again into high pressure sterilization Kettle temperature maintain 110-126 DEG C, pressure 0.01-0.25MPa, reaction 15-45 minutes, be cooled to room temperature, being sufficiently stirred makes It is hardened, you can, the volume ratio of potassium hydroxide solution and tea oil is 2-7:8-20.
The Chinese medicine extract is prepared by the following method:
By (0.1-5.0:0.1-5.0:0.1-5.0:0.1-5.0:0.1-5.0:0.1-70.0:0.1-70.0:0.1- 70.0:0.1-70.0) ratio weighs the coptis, radix scutellariae, Cortex Magnoliae Officinalis, the root bark of tree peony, rheum officinale, dried orange peel, Jasmine, tea, rose;By the coptis, Radix scutellariae, Cortex Magnoliae Officinalis, the root bark of tree peony, rheum officinale, after mixing plus water is cooked by slow fire three times, and each amount of water is 5-15 times of Chinese medicine total weight, often Secondary decoction 20-30min merges filtrate three times, is concentrated into 0.5-3.5g/mL;By dried orange peel, Jasmine, tealeaves, rose it is a kind of or Several mixtures, adds in 2-10 times of the water of one or several kinds of total weight of the mixture, and condensate liquid is collected using steam distillation, Each liquid is mixed up to Chinese medicine extract.
The present invention preparation method be:By natural soap kind, methyl orthophosphoric acid, alkyl glycosides, amino acid foaming agent, traditional Chinese medicine extraction Liquid, sodium chloride are stirred at 35-70 DEG C fully, when standing 1-98 is small, you can.
Tea oil of the present invention is that China is distinctive, is that tea seed warp directly squeezes the oil produced, that is, squeezes camellia oil, Natural materials ingredient therein and trophic component has been fully retained, itself there is moisturizing, make skin with elastic and anti- The features such as aging.
The hard water resistance effect of simple tea-seed oil liquid soap is undesirable, and the present invention is substantially increased by the adjustment of formula The hard water resistance property of product of the present invention.
Compared with prior art, the present invention relies on Chinese herbal medicine extract, does not add alcohol and artificial synthetic essence with preventing Rotten agent and reach decontamination, sterilization and anticorrosion, the natural integrated purpose of flavouring, there is good decontamination, moisturizing, fungistatic effect, production Product are suitable for human body clean.
Specific embodiment
With reference to embodiment, the present invention is described in detail.
Embodiment 1:
The potassium hydroxide solution of saturation is added in tea oil, is put into high-pressure sterilizing pot, temperature maintain 110-126 DEG C, Pressure 0.05-0.1MPa, 15 minutes postcoolings of reaction are sufficiently stirred again after its hardening, are placed again into high pressure sterilization kettle temperature Maintain 110-126 DEG C, pressure 0.05-0.1MPa, reaction 15 minutes, be cooled to room temperature, being sufficiently stirred makes its hardening, obtains day The volume ratio of right soap kind 1, potassium hydroxide solution and tea oil is 1:4.
Embodiment 2:
The potassium hydroxide solution of saturation is added in tea oil, is put into high-pressure sterilizing pot, temperature maintain 110-126 DEG C, Pressure 0.05-0.1MPa is reacted 30 minutes, is cooled to room temperature, and is sufficiently stirred after its hardening, is placed again into high-pressure sterilizing pot Temperature maintain 110-126 DEG C, pressure 0.05-0.1MPa, reaction 30 minutes, be cooled to room temperature, being sufficiently stirred makes its hardening, obtains To natural soap kind 2, the volume ratio of potassium hydroxide solution and tea oil is 1:3.0.
Embodiment 3:
The potassium hydroxide solution of saturation is added in tea oil, is put into high-pressure sterilizing pot, temperature maintain 110-126 DEG C, Pressure 0.1-0.15MPa is reacted 30 minutes, is cooled to room temperature, and is sufficiently stirred after its hardening, is placed again into high-pressure sterilizing pot Temperature maintain 110-126 DEG C, pressure 0.05-0.1MPa, reaction 45 minutes, be cooled to room temperature, being sufficiently stirred makes its hardening, obtains To natural soap kind 3, the volume ratio of potassium hydroxide solution and tea oil is 1:4.
Embodiment 4:
It is 3 by the weight ratio of the coptis, radix scutellariae, Cortex Magnoliae Officinalis, the root bark of tree peony:1:1:2 weigh, and after mixing plus water is cooked by slow fire three times, often Secondary amount of water is 5 times of Chinese medicine total weight, decocts 20min every time, merges filtrate three times, is concentrated into 1.0g/mL, obtains traditional Chinese medicine extraction Liquid 1;
It is 1 by the weight ratio of radix scutellariae, Cortex Magnoliae Officinalis, the root bark of tree peony, rheum officinale:2:2:5 weigh, and after mixing plus water is cooked by slow fire three times, often Secondary amount of water is 10 times of Chinese medicine total weight, decocts 25min every time, merges filtrate three times, is concentrated into 2g/mL, obtains traditional Chinese medicine extraction Liquid 2;
It is 5 by the weight ratio of the coptis, radix scutellariae, Cortex Magnoliae Officinalis, the root bark of tree peony, rheum officinale:2:3:4:2 weigh, and after mixing plus water is cooked by slow fire Three times, each amount of water is 15 times of Chinese medicine total weight, decocts 25min every time, merges filtrate three times, 2g/mL is concentrated into, in obtaining Medicament extracting solution 3;
Embodiment 5:
2 times of the water of dried orange peel weight is added in dried orange peel, condensate liquid is collected using steam distillation, obtains Chinese medicine extract 4;
Press dried orange peel, the weight ratio 5 of Jasmine:35 weigh, and dried orange peel, Jasmine total weight are added in dried orange peel, Jasmine 5 times of water collects condensate liquid using steam distillation, obtains Chinese medicine extract 5;
Press dried orange peel, Jasmine, tealeaves, the weight ratio 0.1 of rose:70.0:70.0:70.0 weigh, in dried orange peel, jasmine Dried orange peel, Jasmine, tealeaves, 10 times of the water of rose total weight are added in flower, tealeaves, rose, is received using steam distillation Collect condensate liquid, obtain Chinese medicine extract 6.
Embodiment 6:
By natural soap kind 2, methyl orthophosphoric acid (Jining Bai Chuan Chemical Co., Ltd.s), (Jinan Bao Liyuan chemical industry has alkyl glycosides Limit company), amino acid foaming agent (Guangzhou Peng Yuan Chemical Co., Ltd.s), Chinese medicine extract 1, Chinese medicine extract 4, sodium chloride, in It is stirred at 35-40 DEG C fully, when standing 1 is small, you can.
Natural soap kind 2, methyl orthophosphoric acid, alkyl glycosides, amino acid foaming agent, Chinese medicine extract 1, Chinese medicine extract 4, chlorination The weight ratio of sodium is 8:8:8:10:3:62.5:0.5
Embodiment 7:
By natural soap kind 3, methyl orthophosphoric acid (Jining Bai Chuan Chemical Co., Ltd.s), (Jinan Bao Liyuan chemical industry has alkyl glycosides Limit company), amino acid foaming agent (Guangzhou Peng Yuan Chemical Co., Ltd.s), Chinese medicine extract 3, Chinese medicine extract 6, sodium chloride, in It is stirred at 50-60 DEG C fully, when standing 7 is small, you can.
Natural soap kind 3, methyl orthophosphoric acid, alkyl glycosides, amino acid foaming agent, Chinese medicine extract 3, Chinese medicine extract 6, chlorination The weight ratio of sodium is 8:8:12:10:4.5:56.5:1.0.
Embodiment 8:
By natural soap kind 2, methyl orthophosphoric acid (Jining Bai Chuan Chemical Co., Ltd.s), (Jinan Bao Liyuan chemical industry has alkyl glycosides Limit company), amino acid foaming agent (Guangzhou Peng Yuan Chemical Co., Ltd.s), Chinese medicine extract 5, sodium chloride, stirred at 60-70 DEG C Fully, when standing 98 is small, you can.
Natural soap kind 2, methyl orthophosphoric acid, alkyl glycosides, amino acid foaming agent, Chinese medicine extract 5, the weight ratio of sodium chloride are 8:8:8:10:65.5:0.5.
Soil removal efficiency parameter passes through in the present invention《Manual dishwashing detergent》(GB 9985-2000) " measure of detergency " Defined method measures;
Biocidal property parameter is by defending method prison hair [2002] the 229th《Disinfection technology standard》Side specified in (version in 2002) Method measures;
Hard water resistance degree is according to national standard QBT 2487-2008《Compound laundry soap》Specified in method measure;
Toxicological experiment according to《Cosmetics health specification》Prescriptive procedure measures in (version in 2007).
The technical indicator of embodiment 6,8 is as shown in table 1:
Table 1:
As shown in table 1:The herb liquid of addition for staphylococcus aureus, bacillus subtilis there is good inhibition to imitate Fruit;Hard water resistance degree is above 3.0mL;Not only soil removal efficiency is high but also good antimicrobial effect for product of the present invention;Skin irritation test reacts It integrates as 0, that is, illustrates for no skin irritation;The experiment of mouth poison shows LD50 > 5000mg/kg, belongs to real without dead mouse The nontoxic grade in border;Eye irritation experiment reaction integration is 2 points, and integration was reduced to 0 in 7 days, showed thorn of the product of the present invention to eyes It is microstimulation to swash intensity.

Claims (2)

1. Chinese medicinal liquor soap, the substance containing following parts by weight:
The Chinese medicine extract is prepared by the following method:
By (0.1-5.0:0.1-5.0:0.1-5.0:0.1-5.0:0.1-5.0:0.1-70.0:0.1-70.0:0.1-70.0: 0.1-70.0) ratio weighs the coptis, radix scutellariae, Cortex Magnoliae Officinalis, the root bark of tree peony, rheum officinale, dried orange peel, Jasmine, tealeaves, rose;By the coptis, Huang A kind of reed mentioned in ancient books, Cortex Magnoliae Officinalis, the root bark of tree peony, rheum officinale, after mixing plus water is cooked by slow fire three times, and each amount of water is 5-15 times of Chinese medicine total weight, every time 20-30min is decocted, merges filtrate three times, is concentrated into 0.5-3.5g/mL;By dried orange peel, Jasmine, tealeaves, rose one kind or number The mixture of kind, adds in 2-10 times of the water of one or several kinds of total weight of the mixture, and condensate liquid is collected using steam distillation;It is mixed Each liquid is closed up to Chinese medicine extract.
2. Chinese medicinal liquor soap according to claim 1, it is characterised in that:
The natural soap kind is prepared by the following method:
The potassium hydroxide solution of saturation is added in tea oil, is put into high-pressure sterilizing pot, temperature maintains 110-126 DEG C, pressure 0.01-0.25MPa is reacted 15-45 minutes, is cooled to room temperature, and is sufficiently stirred after its hardening, is placed again into high-pressure sterilizing pot Temperature maintain 110-126 DEG C, pressure 0.01-0.25MPa, reaction 15-45 minute, be cooled to room temperature, be sufficiently stirred make its firmly Change, you can, the volume ratio of potassium hydroxide solution and tea oil is 2-7:8-20.
CN201510695315.7A 2015-10-23 2015-10-23 Chinese medicinal liquor soap and preparation method thereof Active CN105193663B (en)

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107904051A (en) * 2017-11-08 2018-04-13 骆志明 Old ginger tuber of multiflower knotweed ferment craft hair washing liquid soap
CN107904050A (en) * 2017-11-08 2018-04-13 骆志明 Moisturizing whitening ferment face cleaning craft liquid soap
CN109825389A (en) * 2019-01-29 2019-05-31 丰益油脂科技(东莞)有限公司 A kind of amino acid soap and preparation method thereof
CN114736747A (en) * 2022-03-18 2022-07-12 山东利尔康医疗科技股份有限公司 Antibacterial soap solution containing natural plant components and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104411289A (en) * 2012-06-15 2015-03-11 卢布里佐尔先进材料有限公司 Alkyl glycoside-based micellar thickeners for surfactant systems
CN104726226A (en) * 2013-12-18 2015-06-24 江南大学 Formula of high-foam mild liquid soap

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104411289A (en) * 2012-06-15 2015-03-11 卢布里佐尔先进材料有限公司 Alkyl glycoside-based micellar thickeners for surfactant systems
CN104726226A (en) * 2013-12-18 2015-06-24 江南大学 Formula of high-foam mild liquid soap

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