CN105193663A - Traditional Chinese medicinal liquid soap and preparation method thereof - Google Patents
Traditional Chinese medicinal liquid soap and preparation method thereof Download PDFInfo
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- CN105193663A CN105193663A CN201510695315.7A CN201510695315A CN105193663A CN 105193663 A CN105193663 A CN 105193663A CN 201510695315 A CN201510695315 A CN 201510695315A CN 105193663 A CN105193663 A CN 105193663A
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- chinese medicine
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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Abstract
The invention discloses a traditional Chinese medicinal liquid soap and a preparation method thereof. The liquid soap contains the following substances: natural soap seeds, alkyl glucoside, methyl phosphate, an amino acid foaming agent, a traditional Chinese medicine extract and sodium chloride. Compared with the prior art, the traditional Chinese medicine liquid soap achieves the purposes of integration of decontamination, sterilization and corrosion prevention, and natural enhancement of aroma by depending on the Chinese herb extract without adding alcohol, artificially synthesized essences and antiseptics, has favorable decontamination, moisture preservation and bacterial inhibition effects and is applicable to cleaning of a human body.
Description
Technical field:
The invention belongs to liquid soap and preparation method thereof, belong to Chinese medicinal liquor soap and preparation method thereof especially.
Background technology:
Soap and detergent can play effect that is clean, sterilization to a certain extent, but well-known to the stimulation of skin.This series products of life-time service may cause pachylosis, be chapped from the cold and even peel.Comparatively speaking, carry out by natural oil and caustic potash the product that reacts and the liquid soap made not only acid-base value be partial to neutrality, and glycerol containing natural skin care wetting agent is thus even better, is also more and more subject to market accreditation.But existing liquid soap decontamination, antibacterial, anticorrosion in be difficult to show consideration for.In existing product, the decontamination effective ingredient used mostly is soap, easily produces soap scum and has stimulation to human body; Bactericidal, antiseptic mostly are chemical industry synthetic product as triclosan, triclocarban, ethanol, Kazon etc., even comprise the antiseptic of Methylisothiazolinone, Form aldehyde release body etc., there is healthy and safe hidden danger.As Chinese patent (application number 201210492046.0) uses methyl parahydroxybenzoate to reach the antiseptical order of prepared liquid soap product.A kind of Solid/liquid two purpose sterilizing skin moistening fancy soap that Chinese patent (application number 201310353551.1) provides and preparation method thereof, the antibacterial used can be one or more in 2-methvl-propionic acid methyl este, 2 Methylpropionic acid, the mould prestige of second for antibacterial, adopts natural flower aroma to replace compound essence simultaneously.A kind of liquid soap that Chinese patent (application number 201310663283.3) provides reaches the object of flavouring by adding dihydromyrcenol and contains ethanol.Liquid soap that Chinese patent (application number 201110278332.2) provides and preparation method thereof, although all use natural constituents, prepared product does not possess bactericidal action.
Summary of the invention:
Rely on soap as decontamination effective ingredient for prior art, rely on interpolation compound essence flavouring, rely on synthetic to reach antiseptic and inhibiting bacteria function object.
1st object of the present invention provides a kind of and rely on Chinese herbal medicine extract, do not add ethanol and synthetic essence reaches the integrated Traditional Chinese medicine bacteriostatic liquid soap of decontamination, sterilization and anticorrosion, natural flavouring with antiseptic.
2nd object of the present invention is the preparation method of aforesaid liquid soap.
The technical scheme of technical solution problem of the present invention is: Chinese medicinal liquor soap, the material containing following weight portion:
Described natural soap kind is prepared by the following method:
Saturated potassium hydroxide solution is added in Oleum Camelliae, put into high-pressure sterilizing pot, temperature maintains 110-126 DEG C, pressure 0.01-0.25MPa, and reaction 15-45 minute, is cooled to room temperature, abundant stirring is after its sclerosis, again put into autoclaving kettle temperature and maintain 110-126 DEG C, pressure 0.01-0.25MPa, reaction 15-45 minute, be cooled to room temperature, fully stir and make it harden,, the volume ratio of potassium hydroxide solution and Oleum Camelliae is 2-7:8-20.
Described Chinese medicine extraction liquid is prepared by the following method:
Rhizoma Coptidis, Radix Scutellariae, Cortex Magnoliae Officinalis, Cortex Moutan, Radix Et Rhizoma Rhei, Pericarpium Citri Reticulatae, Flos Jasmini Sambac, tea, Flos Rosae Rugosae is weighed in (0.1-5.0:0.1-5.0:0.1-5.0:0.1-5.0:0.1-5.0:0.1-70.0:0.1-70. 0:0.1-70.0:0.1-70.0) ratio; By Rhizoma Coptidis, Radix Scutellariae, Cortex Magnoliae Officinalis, Cortex Moutan, Radix Et Rhizoma Rhei, add water after mixing slow fire boiling three times, and each amount of water is 5-15 times of Chinese medicine gross weight, decocts 20-30min at every turn, merges three filtrates, be concentrated into 0.5-3.5g/mL; By Pericarpium Citri Reticulatae, Flos Jasmini Sambac, Folium Camelliae sinensis, one or several mixture of Flos Rosae Rugosae, the water 2-10 adding one or several mixture total weight amounts doubly, adopts steam distillation to collect condensed fluid, mixes each medicinal liquid and namely obtain Chinese medicine extraction liquid.
Preparation method of the present invention is: by natural soap kind, methyl orthophosphoric acid, alkyl polyglucoside, aminoacid foaming agent, Chinese medicine extraction liquid, sodium chloride, stirs fully, leave standstill 1-98 hour at 35-70 DEG C.
Oleum Camelliae of the present invention is that China is distinctive, is that Semen Camelliae warp directly squeezes the oil produced, namely squeezes Camellia oil, remain natural materials composition wherein and trophic component completely, itself have moisturizing, makes skin have elasticity and anti-ageing feature of waiting for a long time.
The anti-hard water effect of simple Oleum Camelliae liquid soap is undesirable, and the present invention, by the adjustment of formula, substantially increases the anti-water hardness tolerance of product of the present invention.
Compared with prior art, the present invention relies on Chinese herbal medicine extract, do not add ethanol and synthetic essence reaches the integrated object of decontamination, sterilization and anticorrosion, natural flavouring with antiseptic, have good decontamination, moisturizing, fungistatic effect, product is applicable to human body clean.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in detail.
Embodiment 1:
Saturated potassium hydroxide solution is added in Oleum Camelliae, put into high-pressure sterilizing pot, temperature maintains 110-126 DEG C, pressure 0.05-0.1MPa, react after 15 minutes and cool again fully stirring after its sclerosis, again put into autoclaving kettle temperature maintain 110-126 DEG C, pressure 0.05-0.1MPa, reaction 15 minutes, be cooled to room temperature, fully stir and make it harden, obtain natural soap kind 1, the volume ratio of potassium hydroxide solution and Oleum Camelliae is 1:4.
Embodiment 2:
Saturated potassium hydroxide solution is added in Oleum Camelliae, put into high-pressure sterilizing pot, temperature maintains 110-126 DEG C, pressure 0.05-0.1MPa, reacts 30 minutes, is cooled to room temperature, abundant stirring is after its sclerosis, again put into autoclaving kettle temperature maintain 110-126 DEG C, pressure 0.05-0.1MPa, reaction 30 minutes, be cooled to room temperature, fully stir and make it harden, obtain natural soap kind 2, the volume ratio of potassium hydroxide solution and Oleum Camelliae is 1:3.0.
Embodiment 3:
Saturated potassium hydroxide solution is added in Oleum Camelliae, put into high-pressure sterilizing pot, temperature maintains 110-126 DEG C, pressure 0.1-0.15MPa, reacts 30 minutes, is cooled to room temperature, abundant stirring is after its sclerosis, again put into autoclaving kettle temperature maintain 110-126 DEG C, pressure 0.05-0.1MPa, reaction 45 minutes, be cooled to room temperature, fully stir and make it harden, obtain natural soap kind 3, the volume ratio of potassium hydroxide solution and Oleum Camelliae is 1:4.
Embodiment 4:
Be that 3:1:1:2 takes by the weight ratio of Rhizoma Coptidis, Radix Scutellariae, Cortex Magnoliae Officinalis, Cortex Moutan, add water after mixing slow fire boiling three times, and each amount of water is 5 times of Chinese medicine gross weight, decocts 20min at every turn, merges three filtrates, be concentrated into 1.0g/mL, obtain Chinese medicine extraction liquid 1;
Be that 1:2:2:5 takes by the weight ratio of Radix Scutellariae, Cortex Magnoliae Officinalis, Cortex Moutan, Radix Et Rhizoma Rhei, add water after mixing slow fire boiling three times, and each amount of water is 10 times of Chinese medicine gross weight, decocts 25min at every turn, merges three filtrates, be concentrated into 2g/mL, obtain Chinese medicine extraction liquid 2;
Be that 5:2:3:4:2 takes by the weight ratio of Rhizoma Coptidis, Radix Scutellariae, Cortex Magnoliae Officinalis, Cortex Moutan, Radix Et Rhizoma Rhei, add water after mixing slow fire boiling three times, and each amount of water is 15 times of Chinese medicine gross weight, each decoction 25min, merge three filtrates, be concentrated into 2g/mL, obtain Chinese medicine extraction liquid 3;
Embodiment 5:
In Pericarpium Citri Reticulatae, add 2 times, the water of Pericarpium Citri Reticulatae weight, adopt steam distillation to collect condensed fluid, obtain Chinese medicine extraction liquid 4;
Take by the weight ratio 5:35 of Pericarpium Citri Reticulatae, Flos Jasmini Sambac, in Pericarpium Citri Reticulatae, Flos Jasmini Sambac, add 5 times, the water of Pericarpium Citri Reticulatae, Flos Jasmini Sambac gross weight, adopt steam distillation to collect condensed fluid, obtain Chinese medicine extraction liquid 5;
Take by the weight ratio 0.1:70.0:70.0:70.0 of Pericarpium Citri Reticulatae, Flos Jasmini Sambac, Folium Camelliae sinensis, Flos Rosae Rugosae, 10 times, the water of Pericarpium Citri Reticulatae, Flos Jasmini Sambac, Folium Camelliae sinensis, Flos Rosae Rugosae gross weight is added in Pericarpium Citri Reticulatae, Flos Jasmini Sambac, Folium Camelliae sinensis, Flos Rosae Rugosae, adopt steam distillation to collect condensed fluid, obtain Chinese medicine extraction liquid 6.
Embodiment 6:
By natural soap kind 2, methyl orthophosphoric acid (Jining Bai Chuan Chemical Co., Ltd.), alkyl polyglucoside (Jinan Bao Liyuan Chemical Co., Ltd.), aminoacid foaming agent (Guangzhou Peng Yuan Chemical Co., Ltd.), Chinese medicine extraction liquid 1, Chinese medicine extraction liquid 4, sodium chloride, stir fully at 35-40 DEG C, leave standstill 1 hour.
The weight ratio of natural soap kind 2, methyl orthophosphoric acid, alkyl polyglucoside, aminoacid foaming agent, Chinese medicine extraction liquid 1, Chinese medicine extraction liquid 4, sodium chloride is 8:8:8:10:3:62.5:0.5
Embodiment 7:
By natural soap kind 3, methyl orthophosphoric acid (Jining Bai Chuan Chemical Co., Ltd.), alkyl polyglucoside (Jinan Bao Liyuan Chemical Co., Ltd.), aminoacid foaming agent (Guangzhou Peng Yuan Chemical Co., Ltd.), Chinese medicine extraction liquid 3, Chinese medicine extraction liquid 6, sodium chloride, stir fully at 50-60 DEG C, leave standstill 7 hours.
The weight ratio of natural soap kind 3, methyl orthophosphoric acid, alkyl polyglucoside, aminoacid foaming agent, Chinese medicine extraction liquid 3, Chinese medicine extraction liquid 6, sodium chloride is 8:8:12:10:4.5:56.5:1.0.
Embodiment 8:
By natural soap kind 2, methyl orthophosphoric acid (Jining Bai Chuan Chemical Co., Ltd.), alkyl polyglucoside (Jinan Bao Liyuan Chemical Co., Ltd.), aminoacid foaming agent (Guangzhou Peng Yuan Chemical Co., Ltd.), Chinese medicine extraction liquid 5, sodium chloride, stir fully at 60-70 DEG C, leave standstill 98 hours.
The weight ratio of natural soap kind 2, methyl orthophosphoric acid, alkyl polyglucoside, aminoacid foaming agent, Chinese medicine extraction liquid 5, sodium chloride is 8:8:8:10:65.5:0.5.
The method that in the present invention, soil removal efficiency parameter is specified by " manual dishwashing detergent " (GB9985-2000) " mensuration of detergency " records;
Biocidal property parameter sends out regulation in [2002] No. 229 " disinfection technology standard " (version in 2002) method by defending method prison records;
Anti-hard water degree records according to the method for regulation in national standard QBT2487-2008 " compound laundry soap ";
Toxicological experiment records according to prescriptive procedure in " cosmetics health specification " (version in 2007).
The technical specification of embodiment 6,8 is as shown in table 1:
Table 1:
As shown in table 1: the herb liquid of interpolation has good inhibition for staphylococcus aureus, bacillus subtilis; Anti-hard water degree is all higher than 3.0mL; Not only soil removal efficiency is high but also good antimicrobial effect for product of the present invention; Skin irritation test reaction integration is 0, namely illustrates for no skin irritation; The experiment of mouth poison, without dead mouse, shows LD50 > 5000mg/kg, belongs to actual nontoxic level; Eye irritation experiment reaction integration is 2 points, and integration reduced to 0 in 7 days, showed that product of the present invention is microstimulation to the stimulus intensity of eyes.
Claims (4)
1. Chinese medicinal liquor soap, the material containing following weight portion:
2. Chinese medicinal liquor soap according to claim 1, is characterized in that:
Described natural soap kind is prepared by the following method:
Saturated potassium hydroxide solution is added in Oleum Camelliae, put into high-pressure sterilizing pot, temperature maintains 110-126 DEG C, pressure 0.01-0.25MPa, and reaction 15-45 minute, is cooled to room temperature, abundant stirring is after its sclerosis, again put into autoclaving kettle temperature and maintain 110-126 DEG C, pressure 0.01-0.25MPa, reaction 15-45 minute, be cooled to room temperature, fully stir and make it harden,, the volume ratio of potassium hydroxide solution and Oleum Camelliae is 2-7:8-20.
3. Chinese medicinal liquor soap according to claim 1, is characterized in that:
Described Chinese medicine extraction liquid is prepared by the following method:
Rhizoma Coptidis, Radix Scutellariae, Cortex Magnoliae Officinalis, Cortex Moutan, Radix Et Rhizoma Rhei, Pericarpium Citri Reticulatae, Flos Jasmini Sambac, tea, Flos Rosae Rugosae is weighed in (0.1-5.0:0.1-5.0:0.1-5.0:0.1-5.0:0.1-5.0:0.1-70.0:0.1-70. 0:0.1-70.0:0.1-70.0) ratio; By Rhizoma Coptidis, Radix Scutellariae, Cortex Magnoliae Officinalis, Cortex Moutan, Radix Et Rhizoma Rhei, add water after mixing slow fire boiling three times, and each amount of water is 5-15 times of Chinese medicine gross weight, decocts 20-30min at every turn, merges three filtrates, be concentrated into 0.5-3.5g/mL; By Pericarpium Citri Reticulatae, Flos Jasmini Sambac, Folium Camelliae sinensis, one or several mixture of Flos Rosae Rugosae, the water 2-10 adding one or several mixture total weight amounts doubly, adopts steam distillation to collect condensed fluid; Mix each medicinal liquid and namely obtain Chinese medicine extraction liquid.
4. the preparation method of the Chinese medicinal liquor soap described in claim 1,2,3, it is characterized in that: by natural soap kind, methyl orthophosphoric acid, alkyl polyglucoside, aminoacid foaming agent, Chinese medicine extraction liquid, sodium chloride, stir at 35-70 DEG C fully, leave standstill 1-98 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510695315.7A CN105193663B (en) | 2015-10-23 | 2015-10-23 | Chinese medicinal liquor soap and preparation method thereof |
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| CN201510695315.7A CN105193663B (en) | 2015-10-23 | 2015-10-23 | Chinese medicinal liquor soap and preparation method thereof |
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| CN105193663B CN105193663B (en) | 2018-05-25 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107904051A (en) * | 2017-11-08 | 2018-04-13 | 骆志明 | Old ginger tuber of multiflower knotweed ferment craft hair washing liquid soap |
| CN107904050A (en) * | 2017-11-08 | 2018-04-13 | 骆志明 | Moisturizing whitening ferment face cleaning craft liquid soap |
| CN109825389A (en) * | 2019-01-29 | 2019-05-31 | 丰益油脂科技（东莞）有限公司 | A kind of amino acid soap and preparation method thereof |
| CN114736747A (en) * | 2022-03-18 | 2022-07-12 | 山东利尔康医疗科技股份有限公司 | Antibacterial soap solution containing natural plant components and preparation method thereof |
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| CN104411289A (en) * | 2012-06-15 | 2015-03-11 | 卢布里佐尔先进材料有限公司 | Alkyl glycoside-based micellar thickeners for surfactant systems |
| CN104726226A (en) * | 2013-12-18 | 2015-06-24 | 江南大学 | Formula of high-foam mild liquid soap |
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2015
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104411289A (en) * | 2012-06-15 | 2015-03-11 | 卢布里佐尔先进材料有限公司 | Alkyl glycoside-based micellar thickeners for surfactant systems |
| CN104726226A (en) * | 2013-12-18 | 2015-06-24 | 江南大学 | Formula of high-foam mild liquid soap |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107904051A (en) * | 2017-11-08 | 2018-04-13 | 骆志明 | Old ginger tuber of multiflower knotweed ferment craft hair washing liquid soap |
| CN107904050A (en) * | 2017-11-08 | 2018-04-13 | 骆志明 | Moisturizing whitening ferment face cleaning craft liquid soap |
| CN109825389A (en) * | 2019-01-29 | 2019-05-31 | 丰益油脂科技（东莞）有限公司 | A kind of amino acid soap and preparation method thereof |
| CN114736747A (en) * | 2022-03-18 | 2022-07-12 | 山东利尔康医疗科技股份有限公司 | Antibacterial soap solution containing natural plant components and preparation method thereof |
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| CN105193663B (en) | 2018-05-25 |
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