CN108078815A - A kind of disposable hand cleanser of natural bacteriostatic and preparation method thereof - Google Patents
A kind of disposable hand cleanser of natural bacteriostatic and preparation method thereof Download PDFInfo
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- CN108078815A CN108078815A CN201711245641.3A CN201711245641A CN108078815A CN 108078815 A CN108078815 A CN 108078815A CN 201711245641 A CN201711245641 A CN 201711245641A CN 108078815 A CN108078815 A CN 108078815A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The present invention relates to disposable hand cleanser of a kind of natural bacteriostatic and preparation method thereof, belong to cleaning solution technical field.The present invention contains abundant saponin(e using soapberry pericarp,With stronger surface-active and dirt-removing power,Its pericarp saponin(e foaming abundancy,Feel is fine and smooth,Smell faint scent,To no skin irritation,Skin quality can be improved,Make skin exquisiteness gloss,High resilience,Reduce injury of the cationic surfactant to human skin in conventional washing agent,There is ecological, environmental protective,And utilize the moisturizing of citrus volatile oil,Anti-inflammatory,Sterilization and bacteriostasis efficacy,With reference to volatile argyi leaf oil to bacterium,The stronger inhibitory action of fungi,Instead of chemosterilant,Common hand cleanser is reduced to damage caused by skin and allergic phenomena,And it is easily biodegradable in the environment,It not can cause environmental pollution,For a long time hand skin can be kept to moisten,And with natural fragrance,It does not hurt hands,There are good washing and skin-care effect,Rear hand skin is washed without any discomfort sense.
Description
Technical field
The present invention relates to disposable hand cleanser of a kind of natural bacteriostatic and preparation method thereof, belong to cleaning solution technical field.
Background technology
Traditional solid soap becomes easily infected by bacterium and dirt on hand in use, becomes pollution source.And
Disposable hand cleanser has sterilization, low stimulation, avoids secondary pollution as traditional hand-washing article perfumed soap and the substitute products of hand cleanser
The characteristics of.In general, hand cleanser is only limitted to the contact surface of hand at the pump head of hand cleanser bottle when cleaning hand, can be effective
Avoid secondary pollution.Meanwhile the formula of hand cleanser is said with respect to perfumed soap than milder, the stimulation of opponent is smaller, to being generally stained on hand
The pathogen of dye such as Escherichia coli, staphylococcus aureus, the killing effect of Candida albicans have good killing effect.
Disposable hand cleanser plays an important role of that the i.e. cleanable hand in water source is not required, from water source as new hand cleanser
Limitation, use is extremely convenient.The kind of existing disposable hand cleanser is more, but it is most of all there is the defects of certain, have
The sterilization unit of a little disposable hand cleanser is divided into chemical composition, larger to hand skin irritation, can cause the pairs such as skin irritatin allergy
Action-reaction；Other ingredient not easily biological-degradable, hard water resistance poor-performing；More also contain inflammable constituent, deposit for a long time
It puts and unstable separated or gone bad.It is more steady to the side effect and production of hand skin how in hand cleanser disinfectant is reduced
Fixed economic hand cleanser becomes the problem for producing disposable hand cleanser research.
Meanwhile due to environmental problem etc., objectively human diseases species caused by factor was on the increase in recent years, to make
These diseases obtain medical treatment, and the usage amount of antibiotic greatly increases.With the expansion of the use scope of antibiotic element, various bacterium
The drug resistance of strain, and many antibiotics also have toxic side effect.Therefore, the R＆D work of new bacteriostatic agent
Seem increasingly important.New inhibiting-bacteria preparation should have good fungistatic effect, there is the characteristic of broad-spectrum antiseptic, resistance to drug
The bacterium received generates and significantly inhibits effect, while is not likely to produce tolerance in itself, it is made to have in medicine, food, healthcare field
Wide development prospect and market potential.
The content of the invention
The technical problems to be solved by the invention：It is divided into chemical composition, opponent for the sterilization unit of existing disposable hand cleanser
Portion's skin irritation is larger, the problem of causing skin irritatin allergy, provides a kind of disposable hand cleanser of natural bacteriostatic and its system
Preparation Method.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
A kind of disposable hand cleanser of natural bacteriostatic, each component Material Percentage are：Dodecyldimethylammonium hydroxide inner salt 1~2%, fat
Alcohol polyoxyethylene ether 1~2%, soapberry pericarp saponin(e concentrate 3~5%, absolute ethyl alcohol 40~50%, alkyl glycosides 1~3%, chlorine
Change sodium 0.6~1.2%, cocoanut fatty acid diethanolamide 1~2%, citrus volatile oil 1~2%, volatile argyi leaf oil 1~2% are gone
Ion water surplus.
The soapberry pericarp saponin(e concentrate be pretreatment soapberry fruit peel powder and mass fraction be 90% ethanol solution by
Mass ratio 1：30 mix, and are filtered after ultrasonic extraction, and reduction vaporization is concentrated into the 5~10% of former filtrate volume and is made.
The pretreatment soapberry fruit peel powder divests fruit stone after being air-dried for the washing of soapberry fruit and leaves pericarp, and is chopped into
The fragment drying and crushing of 1~3cm is made.
The citrus volatile oil is laid in crush after orange peel is air-dried on filter paper, be placed in deionized water top 3~
On stent at 5cm, steam is passed through in condenser pipe by heating deionized water to seething with excitement, and standing takes upper strata grease, and with anhydrous
Magnesium sulfate dehydration is made.
The volatile argyi leaf oil is to crush to be laid on filter paper after folium artemisiae argyi is air-dried, and is placed in 3~5cm above deionized water
On the stent at place, steam is passed through in condenser pipe by heating deionized water to seething with excitement, and standing takes upper strata grease, and with anhydrous sulphur
Sour magnesium dehydration is made.
A kind of preparation method of the disposable hand cleanser of natural bacteriostatic, concretely comprises the following steps：
（1）The washing of soapberry fruit is taken to divest fruit stone after air-drying and leaves pericarp, and is chopped into the fragment drying and crushing of 1~3cm, is obtained
Pre-process soapberry fruit peel powder；
（2）It is 90% ethanol solution in mass ratio 1 that soapberry fruit peel powder, which will be pre-processed, with mass fraction：30 mix, after ultrasonic extraction
Filtering, and be evaporated under reduced pressure and be concentrated into the 5~10% of former filtrate volume, obtain soapberry pericarp saponin(e concentrate；
（3）It crushes and is laid on filter paper after orange peel is air-dried, is placed on the stent above deionized water at 3~5cm, heating
Steam is passed through in condenser pipe by deionized water to seething with excitement, and standing takes upper strata grease, and is dehydrated with anhydrous magnesium sulfate, obtains citrus
Volatile oil；
（4）It crushes and is laid on filter paper after folium artemisiae argyi is air-dried, is placed on the stent above deionized water at 3~5cm, heating is gone
Steam is passed through in condenser pipe by ionized water to seething with excitement, and standing takes upper strata grease, and is dehydrated with anhydrous magnesium sulfate, obtains folium artemisiae argyi and waves
Hair oil；
（5）Dodecyldimethylammonium hydroxide inner salt, fatty alcohol polyoxyethylene ether, soapberry pericarp saponin(e concentrate are taken, is added in anhydrous
50~60 DEG C are heated with stirring in ethyl alcohol, adds alkyl glycosides, sodium chloride, cocoanut fatty acid diethanolamide, stirring is equal
Citrus volatile oil, volatile argyi leaf oil, 30~40min of insulated and stirred are added in after even, and pH to 7~8 is adjusted with citric acid solution, is added
Remaining deionized water obtains the disposable hand cleanser of natural bacteriostatic.
Compared with other methods, advantageous effects are the present invention：
（1）The present invention contains abundant saponin(e using soapberry pericarp, has stronger surface-active and dirt-removing power, pericarp
Saponin(e foaming abundancy, feel are fine and smooth, and smell faint scent to no skin irritation, can improve skin quality, make skin exquisiteness gloss,
High resilience reduces injury of the cationic surfactant to human skin in conventional washing agent, has the spy of ecological, environmental protective
Point；
（2）The present invention utilizes moisturizing, anti-inflammatory, sterilization and the bacteriostasis efficacy of citrus volatile oil, with reference to volatile argyi leaf oil to bacterium, true
Bacterium has stronger inhibitory action, instead of chemosterilant, reduces common hand cleanser and is damaged caused by skin and allergic phenomena,
And be easily biodegradable in the environment, it not can cause environmental pollution；
（3）The disposable hand cleanser of natural bacteriostatic prepared by the present invention can keep hand skin to moisten for a long time, and have natural fragrance,
It does not hurt hands, there is good washing and skin-care effect, wash rear hand skin without any discomfort sense；
（4）Fungicidal spectrum is narrow when the disposable hand cleanser of natural bacteriostatic prepared by the present invention compensates for the effect of one-component, germicidal efficiency
The defects of low, and achieve the effect that a kind of Synergistic biocidal, to Escherichia coli, staphylococcus aureus, pseudomonas aeruginosa, white
The bacteriostasis of color candida albicans can kill more than 99% encountered pathogenic bacteria, make this formula in a short time when cleaning hand
Disposable hand sanitizing fluid has the bactericidal effect of " the quick-acting, broad-spectrum high efficacy of strength ", and hand cleanser stability is good, and smell is mild, nontoxic,
Nonirritant, security is good, is rinsed without water, convenient for using under various conditions.
Specific embodiment
Soapberry fruit is taken to be washed with deionized in fact 2~3 times, fruit stone is divested after natural air drying and leaves pericarp, and is chopped into 1
The fragment of~3cm, is placed in drying box, dry 3~5h at 50~60 DEG C, then dried soapberry fruit leather jacket is entered to crush
Crushed in machine, cross 40 mesh sieves, must pre-process soapberry fruit peel powder, take 20~40g pre-process soapberry fruit peel powder, addition 600~
1200g mass fractions are in 90% ethanol solution, and 20~30min is stirred with 300~400r/min, then with 100W ultrasonic echographies
Extract 50~80min, filter to get filtrate, by filtrate be placed on Rotary Evaporators be evaporated under reduced pressure be concentrated into former filtrate volume 5~
10%, soapberry pericarp saponin(e concentrate is obtained, is crushed being fitted into after orange peel natural air drying in pulverizer, crosses 40 mesh sieves, take 50~
100g citrus peel meals are laid on filter paper, are placed on the stent above deionized water at 3~5cm, heating deionized water to boiling
It rises, steam is passed through in condenser pipe, continuous heating grease into condenser pipe is not further added by, and upper strata oily is taken after standing 1~2h
Object adds in 20~30g anhydrous magnesium sulfates into grease, stands filtering removal anhydrous magnesium sulfate after 20~30min, obtains citrus and wave
Hair oil is crushed being fitted into after folium artemisiae argyi natural air drying in pulverizer, crosses 40 mesh sieves, 50~100g Folium Artemisiae Argyi powders is taken to be laid on filter paper,
It is placed on the stent above deionized water at 3~5cm, steam is passed through in condenser pipe by heating deionized water to seething with excitement, and is continued
Grease in condenser pipe is heated to not to be further added by, stand 1~2h after take upper strata grease, into grease add in 20~30g without
Water magnesium sulfate stands filtering removal anhydrous magnesium sulfate after 20~30min, obtains volatile argyi leaf oil, take 1~2g dodecyl dimethyls
Glycine betaine, 1~2g fatty alcohol polyoxyethylene ether, 3~5g soapberry pericarp saponin(e concentrates are added in 40~50g absolute ethyl alcohols,
50~60 DEG C, 20~30min of insulated and stirred are heated with stirring to 300~400r/min, adds 1~3g alkyl glycosides, 0.6~
1.2g sodium chloride, 1~2g cocoanut fatty acid diethanolamides continue 20~30min of stirring, add the volatilization of 1~2g citruses
Oil, 1~2g volatile argyi leaf oils, 30~40min of insulated and stirred, and pH to 7~8 is adjusted for 5% citric acid solution with mass fraction,
Deionized water is added to obtain the disposable hand cleanser of natural bacteriostatic to 100g.
Example 1
Soapberry fruit is taken to be washed with deionized in fact 2 times, fruit stone is divested after natural air drying and leaves pericarp, and is chopped into the broken of 1cm
Block is placed in drying box, the dry 3h at 50 DEG C, then dried soapberry fruit leather jacket is entered in pulverizer to crush, and crosses 40 mesh
Sieve, must pre-process soapberry fruit peel powder, and 20g is taken to pre-process soapberry fruit peel powder, and it is 90% ethanol solution to add in 600g mass fractions
In, 20min is stirred with 300r/min, then 50min is extracted with 100W ultrasonic echographies, it filters to get filtrate, filtrate is placed in rotation
It is evaporated under reduced pressure on evaporimeter and is concentrated into the 5% of former filtrate volume, soapberry pericarp saponin(e concentrate is obtained, by orange peel natural air drying
It is fitted into pulverizer and crushes afterwards, cross 40 mesh sieves, 50g citrus peel meals is taken to be laid on filter paper, be placed in above deionized water at 3cm
Stent on, heating deionized water to seethe with excitement, steam is passed through in condenser pipe, continuous heating grease into condenser pipe no longer increases
Add, upper strata grease is taken after standing 1h, 20g anhydrous magnesium sulfates are added in into grease, stand the anhydrous sulphur of filtering removal after 20min
Sour magnesium obtains citrus volatile oil, is crushed being fitted into after folium artemisiae argyi natural air drying in pulverizer, crosses 40 mesh sieves, 50g Folium Artemisiae Argyi powders is taken to be laid in
On filter paper, it is placed on the stent above deionized water at 3cm, steam is passed through in condenser pipe by heating deionized water to seething with excitement,
Continuous heating grease into condenser pipe is not further added by, and upper strata grease is taken after standing 1h, and the anhydrous sulphur of 20g is added in into grease
Sour magnesium stands filtering removal anhydrous magnesium sulfate after 20min, obtains volatile argyi leaf oil, take 1g dodecyldimethylammonium hydroxide inner salts, 1g fat
Fat alcohol polyoxyethylene ether, 3g soapberry pericarp saponin(e concentrates are added in 40g absolute ethyl alcohols, are heated with stirring to 300r/min
50 DEG C, insulated and stirred 20min, 1g alkyl glycosides, 0.6g sodium chloride are added, 1g cocoanut fatty acid diethanolamides continue
20min is stirred, 1g citrus volatile oil, 1g volatile argyi leaf oils, insulated and stirred 30min is added, and is 5% lemon with mass fraction
Acid solution adjusts pH to 7, and deionized water is added to obtain the disposable hand cleanser of natural bacteriostatic to 100g.
Example 2
Soapberry fruit is taken to be washed with deionized in fact 2 times, fruit stone is divested after natural air drying and leaves pericarp, and is chopped into the broken of 2cm
Block is placed in drying box, the dry 4h at 55 DEG C, then dried soapberry fruit leather jacket is entered in pulverizer to crush, and crosses 40 mesh
Sieve, must pre-process soapberry fruit peel powder, and 30g is taken to pre-process soapberry fruit peel powder, and it is 90% ethanol solution to add in 900g mass fractions
In, 25min is stirred with 350r/min, then 65min is extracted with 100W ultrasonic echographies, it filters to get filtrate, filtrate is placed in rotation
It is evaporated under reduced pressure on evaporimeter and is concentrated into the 8% of former filtrate volume, soapberry pericarp saponin(e concentrate is obtained, by orange peel natural air drying
It is fitted into pulverizer and crushes afterwards, cross 40 mesh sieves, 80g citrus peel meals is taken to be laid on filter paper, be placed in above deionized water at 4cm
Stent on, heating deionized water to seethe with excitement, steam is passed through in condenser pipe, continuous heating grease into condenser pipe no longer increases
Add, upper strata grease is taken after standing 1h, 25g anhydrous magnesium sulfates are added in into grease, stand the anhydrous sulphur of filtering removal after 25min
Sour magnesium obtains citrus volatile oil, is crushed being fitted into after folium artemisiae argyi natural air drying in pulverizer, crosses 40 mesh sieves, 80g Folium Artemisiae Argyi powders is taken to be laid in
On filter paper, it is placed on the stent above deionized water at 4cm, steam is passed through in condenser pipe by heating deionized water to seething with excitement,
Continuous heating grease into condenser pipe is not further added by, and upper strata grease is taken after standing 1h, and the anhydrous sulphur of 25g is added in into grease
Sour magnesium stands filtering removal anhydrous magnesium sulfate after 25min, obtains volatile argyi leaf oil, take 1g dodecyldimethylammonium hydroxide inner salts, 1g fat
Fat alcohol polyoxyethylene ether, 4g soapberry pericarp saponin(e concentrates are added in 45g absolute ethyl alcohols, are heated with stirring to 350r/min
55 DEG C, insulated and stirred 25min, 2g alkyl glycosides, 0.9g sodium chloride are added, 1g cocoanut fatty acid diethanolamides continue
25min is stirred, 1g citrus volatile oil, 1g volatile argyi leaf oils, insulated and stirred 35min is added, and is 5% lemon with mass fraction
Acid solution adjusts pH to 7, and deionized water is added to obtain the disposable hand cleanser of natural bacteriostatic to 100g.
Example 3
Soapberry fruit is taken to be washed with deionized in fact 3 times, fruit stone is divested after natural air drying and leaves pericarp, and is chopped into the broken of 3cm
Block is placed in drying box, the dry 5h at 60 DEG C, then dried soapberry fruit leather jacket is entered in pulverizer to crush, and crosses 40 mesh
Sieve, must pre-process soapberry fruit peel powder, and 40g is taken to pre-process soapberry fruit peel powder, and it is molten for 90% ethyl alcohol to add in 1200g mass fractions
In liquid, 30min is stirred with 400r/min, then 80min is extracted with 100W ultrasonic echographies, filters to get filtrate, filtrate is placed in rotation
Turn to be evaporated under reduced pressure on evaporimeter and be concentrated into the 10% of former filtrate volume, soapberry pericarp saponin(e concentrate is obtained, by orange peel natural wind
It is fitted into pulverizer and crushes after dry, cross 40 mesh sieves, 100g citrus peel meals is taken to be laid on filter paper, be placed in above deionized water
On stent at 5cm, steam is passed through in condenser pipe, continuous heating grease into condenser pipe by heating deionized water to seething with excitement
It is not further added by, upper strata grease is taken after standing 2h, 30g anhydrous magnesium sulfates are added in into grease, removal is filtered after standing 30min
Anhydrous magnesium sulfate obtains citrus volatile oil, is crushed being fitted into after folium artemisiae argyi natural air drying in pulverizer, crosses 40 mesh sieves, takes 100g folium artemisiae argyis
Powder is laid on filter paper, is placed on the stent above deionized water at 5cm, and steam is passed through by heating deionized water to seething with excitement
In condenser pipe, continuous heating grease into condenser pipe is not further added by, and is taken upper strata grease after standing 2h, is added in into grease
30g anhydrous magnesium sulfates stand filtering removal anhydrous magnesium sulfate after 30min, obtain volatile argyi leaf oil, take 2g dodecyl dimethyl sweet teas
Dish alkali, 2g fatty alcohol polyoxyethylene ether, 5g soapberry pericarp saponin(e concentrates are added in 50g absolute ethyl alcohols, stirred with 400r/min
It mixes and is heated to 60 DEG C, insulated and stirred 30min, add 3g alkyl glycosides, 1.2g sodium chloride, 2g coco-nut oil fatty acid diethanol acyls
Amine continues to stir 30min, adds 2g citrus volatile oil, 2g volatile argyi leaf oils, insulated and stirred 40min, and be with mass fraction
5% citric acid solution adjusts pH to 8, and deionized water is added to obtain the disposable hand cleanser of natural bacteriostatic to 100g.
Reference examples：The antibacterial disposable hand cleanser of Guangzhou daily use chemicals Co., Ltd production.
The disposable hand cleanser of the natural bacteriostatic of example and reference examples is detected, specific detection is as follows：
The measure of pH：By the regulation of GB/T6368, hand cleanser pH is measured.25 DEG C of test temperature is boiled and cooled down with new
Distilled water configuration 1：10（Mass concentration）Sample solution, mixing, measure.
The measure of sterilizing rate：By GB15979-2002 Disposable Sanitary Accessory sanitary standard appendix Cs defined dense
Degree is lower to be measured.
The inspection of total plate count and excrement colibacillus group：According to《Cosmetics health specification》Part IV Micro biological Tests method
It is measured.
Specific testing result such as table 1.
1 performance characterization contrast table of table
| Detection project | Example 1 | Example 2 | Example 3 | Reference examples |
| pH | 6.5 | 6.3 | 6.1 | 4.2 |
| Sterilizing rate % | 98 | 98 | 99 | 88 |
| Total plate count CFU/g | 10 | 9 | 11 | 50 |
| Excrement colibacillus group CFU/g | 0 | 0 | 0 | 0 |
As shown in Table 1, the disposable hand cleanser pH value that prepared by the present invention does not hurt hands close to neutrality, has good sterilizing rate, meet
The standard of sterilizing rate >=90% of national Specification, total plate count and excrement colibacillus group number also all meet food security country mark
It is accurate.
Claims (6)
1. a kind of disposable hand cleanser of natural bacteriostatic, which is characterized in that each component Material Percentage is：Dodecyl dimethyl beet
Alkali 1~2%, fatty alcohol polyoxyethylene ether 1~2%, soapberry pericarp saponin(e concentrate 3~5%, absolute ethyl alcohol 40~50%, alkyl
Glucosides 1~3%, sodium chloride 0.6~1.2%, cocoanut fatty acid diethanolamide 1~2%, citrus volatile oil 1~2%, folium artemisiae argyi is waved
Hair oil 1~2%, deionized water surplus.
2. a kind of disposable hand cleanser of natural bacteriostatic as described in claim 1, which is characterized in that the soapberry pericarp saponin(e is dense
Contracting liquid is pretreatment soapberry fruit peel powder and mass fraction is 90% ethanol solution in mass ratio 1：30 mix, mistake after ultrasonic extraction
Filter, and reduction vaporization is concentrated into the 5~10% of former filtrate volume and is made.
A kind of 3. disposable hand cleanser of natural bacteriostatic as claimed in claim 2, which is characterized in that the pretreatment soapberry pericarp
Powder divests fruit stone after being air-dried for the washing of soapberry fruit and leaves pericarp, and the fragment drying and crushing for being chopped into 1~3cm is made.
4. a kind of disposable hand cleanser of natural bacteriostatic as described in claim 1, which is characterized in that the citrus volatile oil is by mandarin orange
Orange peel is crushed after air-drying and is laid on filter paper, is placed on the stent above deionized water at 3~5cm, heating deionized water is extremely
Boiling, steam is passed through in condenser pipe, and standing takes upper strata grease, and is dehydrated and be made with anhydrous magnesium sulfate.
5. a kind of disposable hand cleanser of natural bacteriostatic as described in claim 1, which is characterized in that the volatile argyi leaf oil is that will end
Leaf is crushed after air-drying and is laid on filter paper, is placed on the stent above deionized water at 3~5cm, heating deionized water to boiling
It rises, steam is passed through in condenser pipe, standing takes upper strata grease, and is dehydrated and be made with anhydrous magnesium sulfate.
6. a kind of preparation method of the disposable hand cleanser of natural bacteriostatic as claimed in any one of claims 1 to 5, wherein, feature exist
In concretely comprising the following steps：
（1）The washing of soapberry fruit is taken to divest fruit stone after air-drying and leaves pericarp, and is chopped into the fragment drying and crushing of 1~3cm, is obtained
Pre-process soapberry fruit peel powder；
（2）It is 90% ethanol solution in mass ratio 1 that soapberry fruit peel powder, which will be pre-processed, with mass fraction：30 mix, after ultrasonic extraction
Filtering, and be evaporated under reduced pressure and be concentrated into the 5~10% of former filtrate volume, obtain soapberry pericarp saponin(e concentrate；
（3）It crushes and is laid on filter paper after orange peel is air-dried, is placed on the stent above deionized water at 3~5cm, heating
Steam is passed through in condenser pipe by deionized water to seething with excitement, and standing takes upper strata grease, and is dehydrated with anhydrous magnesium sulfate, obtains citrus
Volatile oil；
（4）It crushes and is laid on filter paper after folium artemisiae argyi is air-dried, is placed on the stent above deionized water at 3~5cm, heating is gone
Steam is passed through in condenser pipe by ionized water to seething with excitement, and standing takes upper strata grease, and is dehydrated with anhydrous magnesium sulfate, obtains folium artemisiae argyi and waves
Hair oil；
（5）Dodecyldimethylammonium hydroxide inner salt, fatty alcohol polyoxyethylene ether, soapberry pericarp saponin(e concentrate are taken, is added in anhydrous
50~60 DEG C are heated with stirring in ethyl alcohol, adds alkyl glycosides, sodium chloride, cocoanut fatty acid diethanolamide, stirring is equal
Citrus volatile oil, volatile argyi leaf oil, 30~40min of insulated and stirred are added in after even, and pH to 7~8 is adjusted with citric acid solution, is added
Remaining deionized water obtains the disposable hand cleanser of natural bacteriostatic.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108542850A (en) * | 2018-06-21 | 2018-09-18 | 界首市洁净日用品有限公司 | A kind of antibacterial preserving moisture and protecting skin hand cleanser of addition indocalamus leaf flavones-soapberry pericarp total saposins |
| CN108904329A (en) * | 2018-08-17 | 2018-11-30 | 佛山市森昂生物科技有限公司 | A kind of environment friendly bacteriostatic polyacid hand cleanser and preparation method thereof |
| CN110747072A (en) * | 2019-11-21 | 2020-02-04 | 中南林业科技大学 | Environment-friendly automobile detergent |
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