CN104522876A - Persimmon extract for cigarettes and application of persimmon extract for cigarettes - Google Patents
Persimmon extract for cigarettes and application of persimmon extract for cigarettes Download PDFInfo
- Publication number
- CN104522876A CN104522876A CN201410689981.5A CN201410689981A CN104522876A CN 104522876 A CN104522876 A CN 104522876A CN 201410689981 A CN201410689981 A CN 201410689981A CN 104522876 A CN104522876 A CN 104522876A
- Authority
- CN
- China
- Prior art keywords
- cigarettes
- persimmon extract
- cigarette
- persimmon
- filtrate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses a persimmon extract for cigarettes and application of the persimmon extract for the cigarettes. After persimmons are crushed, heating reflux extraction with ethyl alcohol is carried out; heating reflux extraction with ethyl alcohol is carried out two times for the filter residues; decompressing concentration is carried out to obtain a concentrate A; and the concentrate A and the filtrate are mixed, filtered and concentrated to obtain the needed persimmon extract for the cigarettes. Persimmon extract weighing 0.05% of the weight of cut tobaccos is taken out and is diluted with four-fold ultra-pure water and the obtained product is sprayed to the cut tobaccos in an atomized manner; and the cut tobaccos are then rolled into the cigarettes according to a conventional process. The remaining taste of the cigarettes can be effectively improved; the sweetness of the cigarettes can be improved; smoke can be fine and smooth; and the fragrance concentration of the cigarettes can be improved. According to the invention, a preparation method is simple and convenient, the low in cost, and the persimmon extract has a good application prospect.
Description
Technical field
The invention belongs to cigarette additive technical field, be specifically related to a kind of preparation method of cigarette persimmon extract, the invention still further relates to the application of described persimmon extract in cigarette simultaneously.
Background technology
Persimmon, Ebenaceae plant berry fruits, the mature period is about October, fruit shapes is more, and as spherical, oblate, approximate cone-shape and square etc., different kind colors is not from light orange look to dark salmon pink etc., size is from 2 centimetres to 10 centimetres, and weight is from 100 grams to 350 grams.Original producton location is in China, and cultivation has the history of more than 1,000 year.Persimmon is sweet greasy good to eat, nutritious, contained vitamin and sugar higher than general fruit about 1 ~ 2 times, composition mainly comprises sucrose, glucose, fructose, protein, carrotene, vitamin C, citrulling, iodine, calcium, phosphorus, iron, zinc etc.
Persimmon is applied to cigarette, and be particularly the cigarette additive that development of raw materials is new with persimmon, there is not been reported in the prior art.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide a kind of cigarette persimmon extract, in order to improve the smoking quality of cigarette.
The present invention also aims to provide the embody rule of described cigarette persimmon extract in cigarette.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is percetage by weight.
A kind of cigarette persimmon extract, is prepared by following methods:
(1) pulpous state is broken into after being cleaned by persimmon; In persimmon slurry, add 85% ~ 95% ethanol of 3 times of weight, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, filter residue and filtrate retain for subsequent use respectively;
(2) add 30% ethanol of 4 times of weight to filter residue, be heated to 94 ± 2 DEG C of backflow 2h, filter while hot, repeat this operation, merge twice filtrate, under 40 ± 2 DEG C of conditions, be then evaporated to density is 1.2500 ± 0.004g/com
3, obtain concentrate A;
(3) by for subsequent use to step (2) gained concentrate A and step (1) be placed on 0 DEG C filtrate mixing at leave standstill 36h after filter, it is 1.150 ± 0.004g/com that gained filtrate is evaporated to density at 40 ± 2 DEG C
3, be required cigarette persimmon extract.
Do not need when described cigarette persimmon extract is applied to production of cigarettes to change the original processing technology of cigarette, can directly persimmon extract be added in cigarette shreds.Concrete grammar is: take described cigarette persimmon extract according to 0.05% of pipe tobacco weight, be sprayed onto on pipe tobacco, more conveniently technique rolls into cigarette with after the ultra-pure water dilution of 4 times amount in the mode of atomization.
Cigarette persimmon extract of the present invention adds in cigarette, can effectively improve cigarette pleasant impression, improves cigarette sweet moisture feeling, makes flue gas fine and smooth, improves the fragrance level of cigarette.Preparation method of the present invention is easy, with low cost, has a good application prospect.
Detailed description of the invention
The present invention is described in further detail by the following examples, but embodiment is not limited to the technical solution.
Embodiment 1
(1) take 2KG persimmon, put in juice extractor fragmentation of pulling an oar and obtain persimmon slurry.By 85% alcohol immersion of persimmon slurry by its weight 3 times amount, be heated to 92 DEG C of backflow 2h, filter while hot, filter residue is used for next step, and filtrate is for subsequent use.
(2) add 30% ethanol of its weight 4 times amount to the filter residue in step (1), be heated to 96 DEG C of backflow 2h, repeat this step after filtering while hot, at 42 DEG C, be evaporated to density after merging filtrate is 1.246g/com
3, obtain concentrate A;
(3) step (2) gained concentrate A is mixed with step (1) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 1.146g/com that filtrate is evaporated to density at 42 DEG C
3, obtain orange colour liquid 231g, be cigarette persimmon extract.
Embodiment 2
(1) take 2KG persimmon, put in juice extractor fragmentation of pulling an oar and obtain persimmon slurry.By 95% alcohol immersion of persimmon slurry by its weight 3 times amount, be heated to 88 DEG C of backflow 2h, filter while hot, filter residue is used for next step, and filtrate is for subsequent use.
(2) add 30% ethanol of its weight 4 times amount to the filter residue in step (1), be heated to 92 DEG C of backflow 2h, repeat this step after filtering while hot, at 38 DEG C, be evaporated to density after merging filtrate is 1.254g/com
3, obtain concentrate A;
(3) step (2) gained concentrate A is mixed with step (1) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 1.154g/com that filtrate is evaporated to density at 38 DEG C
3, obtain orange colour liquid 238g, be cigarette persimmon extract.
Embodiment 1 and 2 gained persimmon extract is used for cloud and mist " cloud and mist (purple) " formula, persimmon extract is got by 0.05% of cigarette shreds weight, after diluting 4 times of weight with ultra-pure water, be sprayed onto on cigarette shreds in the mode of atomization, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2%), roll into Cigarette.The cigarette of gained and blank cigarette transfer to specialty member of smoking carry out sense organ contrast smoke panel test, result is as follows:
Claims (2)
1. a cigarette persimmon extract, is prepared by following methods:
(1) pulpous state is broken into after being cleaned by persimmon; In persimmon slurry, add 85% ~ 95% ethanol of 3 times of weight, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, filter residue and filtrate retain for subsequent use respectively;
(2) add 30% ethanol of 4 times of weight to filter residue, be heated to 94 ± 2 DEG C of backflow 2h, filter while hot, repeat this operation, merge twice filtrate, under 40 ± 2 DEG C of conditions, be then evaporated to density is 1.2500 ± 0.004g/com
3, obtain concentrate A;
(3) by for subsequent use to step (2) gained concentrate A and step (1) be placed on 0 DEG C filtrate mixing at leave standstill 36h after filter, it is 1.150 ± 0.004g/com that gained filtrate is evaporated to density at 40 ± 2 DEG C
3, be required cigarette persimmon extract.
2. the application of cigarette persimmon extract according to claim 1 in production of cigarettes, be specially: take described cigarette persimmon extract according to 0.05% of pipe tobacco weight, be sprayed onto on pipe tobacco in the mode of atomization with after the ultra-pure water dilution of 4 times amount, more conveniently technique rolls into cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410689981.5A CN104522876A (en) | 2014-11-25 | 2014-11-25 | Persimmon extract for cigarettes and application of persimmon extract for cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410689981.5A CN104522876A (en) | 2014-11-25 | 2014-11-25 | Persimmon extract for cigarettes and application of persimmon extract for cigarettes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104522876A true CN104522876A (en) | 2015-04-22 |
Family
ID=52838653
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410689981.5A Pending CN104522876A (en) | 2014-11-25 | 2014-11-25 | Persimmon extract for cigarettes and application of persimmon extract for cigarettes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104522876A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113667538A (en) * | 2021-09-02 | 2021-11-19 | 成都宏亿实业集团有限公司 | Method for extracting compound spice and application thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6339574A (en) * | 1986-08-04 | 1988-02-20 | 株式会社 龍角散 | Tobacco filter |
| CN1193494A (en) * | 1997-03-17 | 1998-09-23 | 王延生 | Prescription of cigarettes without harmness to pulbic and production thereof |
| CN1715383A (en) * | 2004-07-02 | 2006-01-04 | 西北工业大学 | Method for extracting natural perfume from persimmon leaf or bark |
| CN1875795A (en) * | 2006-07-03 | 2006-12-13 | 红云烟草(集团)有限责任公司 | Algae compound addictive for cigarette and preparation method thereof |
| CN101904533A (en) * | 2010-08-02 | 2010-12-08 | 周文兴 | Persimmon fermented vinegar beverage and production method thereof |
| CN103816086A (en) * | 2014-03-04 | 2014-05-28 | 天津嘉氏堂科技有限公司 | Whitening traditional Chinese medicine composition as well as preparation method and application thereof |
-
2014
- 2014-11-25 CN CN201410689981.5A patent/CN104522876A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6339574A (en) * | 1986-08-04 | 1988-02-20 | 株式会社 龍角散 | Tobacco filter |
| CN1193494A (en) * | 1997-03-17 | 1998-09-23 | 王延生 | Prescription of cigarettes without harmness to pulbic and production thereof |
| CN1715383A (en) * | 2004-07-02 | 2006-01-04 | 西北工业大学 | Method for extracting natural perfume from persimmon leaf or bark |
| CN1875795A (en) * | 2006-07-03 | 2006-12-13 | 红云烟草(集团)有限责任公司 | Algae compound addictive for cigarette and preparation method thereof |
| CN101904533A (en) * | 2010-08-02 | 2010-12-08 | 周文兴 | Persimmon fermented vinegar beverage and production method thereof |
| CN103816086A (en) * | 2014-03-04 | 2014-05-28 | 天津嘉氏堂科技有限公司 | Whitening traditional Chinese medicine composition as well as preparation method and application thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113667538A (en) * | 2021-09-02 | 2021-11-19 | 成都宏亿实业集团有限公司 | Method for extracting compound spice and application thereof |
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|---|---|---|---|
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150422 |