CN104593150A - Preparation method of mulberry extract and application of mulberry extract in cigarettes - Google Patents

Preparation method of mulberry extract and application of mulberry extract in cigarettes Download PDF

Info

Publication number
CN104593150A
CN104593150A CN201410712230.0A CN201410712230A CN104593150A CN 104593150 A CN104593150 A CN 104593150A CN 201410712230 A CN201410712230 A CN 201410712230A CN 104593150 A CN104593150 A CN 104593150A
Authority
CN
China
Prior art keywords
cigarette
mulberries
filtrate
weight
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410712230.0A
Other languages
Chinese (zh)
Inventor
杜宇
王欣林
赵英良
杨洪明
周国福
杨建云
张天栋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Yunnan Industrial Co Ltd
Original Assignee
China Tobacco Yunnan Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Yunnan Industrial Co Ltd filed Critical China Tobacco Yunnan Industrial Co Ltd
Priority to CN201410712230.0A priority Critical patent/CN104593150A/en
Publication of CN104593150A publication Critical patent/CN104593150A/en
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A24B15/303—Plant extracts other than tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/305—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/12—Steaming, curing, or flavouring tobacco

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Seasonings (AREA)

Abstract

The invention discloses a preparation method of a mulberry extract and an application of the mulberry extract in cigarettes. The preparation method comprises the steps: crushing and pulping mulberry, then crushing cleaned mulberry into a pulpous state, adding an 85%-95% ethanol with the weight 3-4 times that of the mulberry, carrying out heating reflux for 2-3 h, filtering while being hot, using the filter residue for next step, and reserving the filtrate; adding a 30% ethanol with the weight 4-5 times that of the filter residue into the filter residue, carrying out heating reflux for 2-3 h, filtering while being hot, then repeating the step, merging the filtrates, then concentrating under reduced pressure, and thus obtaining a concentrate A; mixing the concentrate A with the initial filtrate, then placing at the temperature of 0 to -10 DEG C, standing, filtering, concentrating the filtrate under reduced pressure to obtain a dark red liquid namely the mulberry extract for the cigarettes. The preparation method is simple and practical, the operation is easy to implement, and the obtained product is used for the cigarettes, can effectively improve the cigarette remaining taste, improves the cigarette sweet moistening feeling, makes smoke gas delicate, and increases the concentration of the cigarette aroma.

Description

A kind of preparation method of mulberries extract and the application in cigarette
Technical field
The invention belongs to cigaret additive technical field, be specifically related to a kind of preparation method of mulberries extract, the invention still further relates to the application of described mulberries extract in cigarette simultaneously.
Background technology
Mulberries, have another name called sorosis, are the mature fruit of Moraceae deciduous tree mulberry tree, and fruit matter is glossy, sweet and sour taste.Mulberries fruit is nutritious, every 100 grams of mulberries moisture contents 81.8 grams, 1.8 grams, protein, 0.3 gram, fat.Mierocrystalline cellulose 4.9 grams, 10 grams, carbohydrate, ash content 1.2 grams, carotene 30 microgram, VitB1 0.02 milligram, 0.06 milligram, riboflavin, vitamin-E 6.95 milligrams, 33 milligrams, potassium, 0.27 milligram, zinc, copper 0.08 milligram, selenium 4.8 microgram.In addition, also containing tannic acid, oxysuccinic acid, vitamins C and lipid acid etc.Its fat is mainly linolic acid, oleic acid, Palmiticacid, stearic acid and sad, n-nonanoic acid, capric acid, tetradecanoic acid, linolenic acid etc. on a small quantity.Traditional Chinese medicine thinks that mulberry fruit is tonified the liver and kidney, nourishing YIN and benefiting blood, breath wind, have cure mainly palpitation and insomnia, have a dizzy spell, tinnitus, constipation night sweat, scrofula, the illness such as articular instability.
At present, there is not been reported mulberries extract to be used for tobacco industry.Be that development of raw materials develops new high-grade cigarette additive with mulberries, the suction quality of cigarette can be improved, expand its application in cigarette, there are good market outlook.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of mulberries extract and the application in cigarette.
Mulberries extract of the present invention joins in the pipe tobacco of production process, can effectively improve cigarette pleasant impression, improves cigarette sweet moisture feeling, makes flue gas fine and smooth, increases cigarette flavor concentration.
Object of the present invention is achieved by the following technical programs:
Except as otherwise noted, percentage ratio of the present invention is weight percentage.
A preparation method for mulberries extract, comprises the following steps:
(1) mulberries after clean are broken into pulpous state;
(2) in mulberries slurry, add 85% ~ 95% ethanol of its weight 3 ~ 4 times amount, be heated to 90 ± 2 DEG C of backflow 2 ~ 3h, filtered while hot, filter residue is used for next step, and filtrate retains;
(3) 30% ethanol of its weight 4 ~ 5 times amount is added to the filter residue in step (2), be heated to 90 ± 2 DEG C of backflow 2 ~ 3h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.0500 ± 0.004g/cm 3, obtain enriched material A;
(4) step (3) gained enriched material A is mixed with step (1) gained filtrate be placed on 0 ~-10 DEG C at leave standstill after 36 ~ 48h and filter, it is 0.990 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C 3, gained dark red liquid is cigarette mulberries extract.
Described mulberries extract can be applicable to production of cigarettes, does not need to change cigarette original complete processing during application, can directly be added in cigarette shreds by mulberries extract.Concrete grammar is: by mulberries extract with after the amount ultrapure water of cigarette shreds weight 0.2 ~ 0.5% dilution 3 ~ 4 times of weight, be then evenly sprayed on pipe tobacco in the mode of atomization, prepare cigarette in existing mode.
The cigarette and the blank cigarette that add mulberries extract carry out sensory evaluating smoking, and smoking result shows, mulberries extract of the present invention can improve cigarette pleasant impression, improve cigarette sweet moisture feeling, make flue gas fine and smooth, improve the effect of cigarette flavor concentration.Preparation method of the present invention is simple and practical, and operation is implemented easily.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail, but embodiment is not limited to the technical solution.
embodiment 1
(1) take 2Kg mulberries, put in juice extractor fragmentation of pulling an oar and obtain mulberries slurry.By 85% alcohol immersion of mulberries slurry by its weight 3 times amount, reflux 2h at temperature 90 DEG C, filtered while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(2) in the filter residue of step (1) gained, add 30% ethanol of its weight 4 times amount, be heated to 90 ± 2 DEG C of backflow 2h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.050 ± 0.004g/cm 3, obtain enriched material A;
(3) step (2) gained enriched material A is mixed with step (1) gained filtrate be placed on 0 DEG C at leave standstill after 48h and filter, it is 0.990 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C 3, obtain dark red liquid 213g, be cigarette mulberries extract.
Mulberries extract in above-described embodiment is used for cloud and mist tobacco leaf formulation, mulberries extract is got by 0.2% of cigarette shreds weight, after diluting 3 times of weight with ultrapure water, be sprayed onto on cigarette shreds in the mode of atomization, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2%), roll into Cigarette.
embodiment 2
(1) take 2Kg mulberries, put in juice extractor fragmentation of pulling an oar and obtain mulberries slurry.By 95% alcohol immersion of mulberries slurry by its weight 4 times amount, reflux 3h at temperature 90 DEG C, filtered while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(2) add 30% ethanol of its weight 5 times amount to the filter residue in step (1), be heated to 90 ± 2 DEG C of backflow 3h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.050 ± 0.004g/cm 3, obtain enriched material A;
(3) step (2) gained enriched material A is mixed with step (1) gained filtrate be placed on-10 DEG C at leave standstill after 36h and filter, it is 0.990 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C 3, obtain dark red liquid 235g, be cigarette mulberries extract.
Mulberries extract in above-described embodiment is used for cloud and mist tobacco leaf formulation, mulberries extract is got by 0.3% of cigarette shreds weight, after diluting 3.5 times of weight with ultrapure water, be sprayed onto on cigarette shreds in the mode of atomization, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2%), roll into Cigarette.
Embodiment 3
(1) take 2Kg mulberries, put in juice extractor fragmentation of pulling an oar and obtain mulberries slurry.By 90% alcohol immersion of mulberries slurry by its weight 3.5 times amount, reflux 2.5h at temperature 90 DEG C, filtered while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(2) add 30% ethanol of its weight 4.5 times amount to the filter residue in step (1), be heated to 90 ± 2 DEG C of backflow 2.5h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.050 ± 0.004g/cm 3, obtain enriched material A;
(3) step (2) gained enriched material A is mixed with step (1) gained filtrate be placed on-5 DEG C at leave standstill after 40h and filter, it is 0.990 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C 3, obtain dark red liquid 235g, be cigarette mulberries extract.
Mulberries extract in above-described embodiment is used for cloud and mist tobacco leaf formulation, mulberries extract is got by 0.5% of cigarette shreds weight, after diluting 4 times of weight with ultrapure water, be sprayed onto on cigarette shreds in the mode of atomization, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2%), roll into Cigarette.
Transfer to the member of smoking of specialty to carry out sense organ contrast with the cigarette of above-described embodiment gained and blank cigarette to smoke panel test, result is as follows:
Cigarette sample Sensory evaluation
Blank sample Have raw assorted gas, irritant, slightly sweet sense, pleasant impression has residual
Add mulberries extract Have the fragrant fragrance of comfortable sour-sweet head, flue gas is fine and smooth, and pungency reduces, and sweet sense strengthens, and fragrance level improves
Above content is the further description made the present invention in conjunction with concrete preferred implementation.For general technical staff of the technical field of the invention, the obvious modification made without departing from the inventive concept of the premise, performance or purposes identical, all should be considered as protection scope of the present invention.

Claims (3)

1. a preparation method for mulberries extract, is characterized in that comprising following steps:
Mulberries after clean are broken into pulpous state;
In mulberries slurry, add 85% ~ 95% ethanol of its weight 3 ~ 4 times amount, be heated to 90 ± 2 DEG C of backflow 2 ~ 3h, filtered while hot, filter residue is used for next step, and filtrate retains;
Add 30% ethanol of its weight 4 ~ 5 times amount to the filter residue in step (2), be heated to 90 ± 2 DEG C of backflow 2 ~ 3h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.0500 ± 0.004g/cm 3, obtain enriched material A;
Mixed with step (1) gained filtrate by step (3) gained enriched material A after leaving standstill 36 ~ 48h at being placed on 0 ~-10 DEG C and filter, it is 0.990 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C 3, gained dark red liquid is cigarette mulberries extract.
2. the mulberries extract prepared of the preparation method of a mulberries extract as claimed in claim 1.
3. the application of mulberries extract in cigarette as claimed in claim 2, after it is characterized in that mulberries extract is diluted 3 ~ 4 times of weight with the amount ultrapure water of cigarette shreds weight 0.2 ~ 0.5%, is sprayed onto on cigarette shreds in the mode be atomized, prepares cigarette.
CN201410712230.0A 2014-12-02 2014-12-02 Preparation method of mulberry extract and application of mulberry extract in cigarettes Pending CN104593150A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410712230.0A CN104593150A (en) 2014-12-02 2014-12-02 Preparation method of mulberry extract and application of mulberry extract in cigarettes

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410712230.0A CN104593150A (en) 2014-12-02 2014-12-02 Preparation method of mulberry extract and application of mulberry extract in cigarettes

Publications (1)

Publication Number Publication Date
CN104593150A true CN104593150A (en) 2015-05-06

Family

ID=53119210

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410712230.0A Pending CN104593150A (en) 2014-12-02 2014-12-02 Preparation method of mulberry extract and application of mulberry extract in cigarettes

Country Status (1)

Country Link
CN (1) CN104593150A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105419381A (en) * 2015-11-30 2016-03-23 浙江辰鸿纺织品科技有限公司 Purification method of natural dyestuff of mulberries
CN110982624A (en) * 2019-12-26 2020-04-10 贵州中烟工业有限责任公司 Mulberry fruit essence, production method of mulberry fruit essence and tobacco product
CN113698990A (en) * 2021-08-05 2021-11-26 广东中烟工业有限责任公司 Mulberry extract and preparation method and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102028757A (en) * 2010-10-27 2011-04-27 安徽济人药业有限公司 Processing method of mulberry compound extract
CN102676301A (en) * 2012-06-01 2012-09-19 云南烟草科学研究院 Macadamia nutshell extractive and application thereof
CN102952634A (en) * 2011-08-24 2013-03-06 湖北中烟工业有限责任公司 Preparation method for cigarette cherry extract and application of cigarette cherry extract in cigarettes

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102028757A (en) * 2010-10-27 2011-04-27 安徽济人药业有限公司 Processing method of mulberry compound extract
CN102952634A (en) * 2011-08-24 2013-03-06 湖北中烟工业有限责任公司 Preparation method for cigarette cherry extract and application of cigarette cherry extract in cigarettes
CN102676301A (en) * 2012-06-01 2012-09-19 云南烟草科学研究院 Macadamia nutshell extractive and application thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105419381A (en) * 2015-11-30 2016-03-23 浙江辰鸿纺织品科技有限公司 Purification method of natural dyestuff of mulberries
CN110982624A (en) * 2019-12-26 2020-04-10 贵州中烟工业有限责任公司 Mulberry fruit essence, production method of mulberry fruit essence and tobacco product
CN113698990A (en) * 2021-08-05 2021-11-26 广东中烟工业有限责任公司 Mulberry extract and preparation method and application thereof

Similar Documents

Publication Publication Date Title
CN104946390B (en) A kind of processing method of electronics natural perfume for cigarette
CN104839885B (en) A kind of electronic cigarette liquid and preparation method thereof of improvement
CN104403794A (en) Preparation method and application of Pu'er tea extract to cigarettes
CN1957777A (en) Method for preparing slices reconstituted from tea, and application in tobacco product
CN101565652A (en) Fruity type flue-cured tobacco essence and applications thereof
CN103783660B (en) The supercritical extraction method of flavor matter and application thereof in a kind of tobacco leaf fragment
CN108060014A (en) For the preparation method of the Flos Caryophylli extract of quick-fried pearl base oil
CN106136311A (en) A kind of non-tobacco new cigarette and preparation method thereof
CN105686065A (en) Tea tobacco and making method thereof
CN108926030A (en) A kind of tobacco style leaf composition for multiple heating mode cigarette, multiple heating mode cigarette and preparation method thereof
CN105011353B (en) Natural bio-chemical agent used for cigar fermentation and quality improvement and application thereof
CN109156895A (en) A kind of reduction cigarette smoking dry sensation and irritating filter stick additive, preparation method and the usage
CN104593150A (en) Preparation method of mulberry extract and application of mulberry extract in cigarettes
CN105747272B (en) A kind of cigarette shreds
CN104585864A (en) Electronic cigarette liquid containing polysaccharide
CN102920008B (en) Preparation method of burley tobacco shreds for cigarettes
CN108949347A (en) Increase the essence and its preparation method and application for heating the new cigarette flue gas moist feeling that do not burn
CN101919581A (en) Method for preparing lophatherum gracile reconstituted sheet and application of lophatherum gracile reconstituted sheet in tobacco product
CN101322582B (en) Pu'er raw tea alcohol-extracted extract and preparation and use thereof
CN105062672A (en) Charging essence for Chinese style cigar, and preparation method thereof
CN104489916B (en) The application of red currant extract in cigarette
CN101327041B (en) Pu'er cooked tea alcohol extract and preparation and use thereof
CN105029677B (en) Tobacco gel and preparation method thereof
CN103919281A (en) Electronic cigarette atomized liquid
CN101323817A (en) Cooked puerh tea essential oil, preparation and use thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20150506