CN101322581B - Mineral ether-extracted Pu'er cooked tea extract and preparation and use thereof - Google Patents
Mineral ether-extracted Pu'er cooked tea extract and preparation and use thereof Download PDFInfo
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- CN101322581B CN101322581B CN2008100587602A CN200810058760A CN101322581B CN 101322581 B CN101322581 B CN 101322581B CN 2008100587602 A CN2008100587602 A CN 2008100587602A CN 200810058760 A CN200810058760 A CN 200810058760A CN 101322581 B CN101322581 B CN 101322581B
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Abstract
The invention discloses a petroleum ether extracted cooked puerh tea extract, a preparation method thereof and the application. Cooked puerh tea and petroleum ether are evenly mixed, and the product is prepared by extraction, solid-liquid separation, distillation and concentration. The petroleum ether extracted cooked puerh tea extract is diluted to the concentration of 1 to 10 percent by using 95 percent of ethanol and then added in the cut tobacco according to 0.01 to 0.1 percent of the weight of the cut tobacco, thereby giving the special aroma to the tobacco. Free amino acids in the cooked puerh tea can well participate in the Maillard reaction during the tobacco alcoholization and the combustion processes to produce the fragrant substances and neutralize the alkaline substances in the tobacco to reduce the stimulus, enrich the smoke aroma, reduce the stimulus and the miscellaneous gas and improve the finish after the taste. The process of the invention is simple, the operation is simple, the existing production process does not need to be changed, and the product does not have the solvent pollution, thereby having great application prospect.
Description
Technical field
The invention belongs to the cigarette additive preparing technical field, be specifically related to a kind of mineral ether-extracted Pu'er cooked tea extract.Simultaneously, the invention still further relates to this extract making method and the application in cigarette thereof.
Background technology
Pu'er tea is the historical famous tea in Yunnan, is meant that generally with the big-leaf species in yunnan tea that meets Pu'er tea home environment condition be the solar dried green tea that raw material is made, and by the compressed tea and the loose tea of crude green tea all size of making after wet heap, compacting.Pu'er tea has its unique processing process, several procedures such as general needs pass through and complete, knead, drying, wet heap.The tealeaves that aquatic foods are adopted is through completing, knead, after the drying, becoming Pu'er gross tea.At this moment Pu'er tea, charm is dense high, sharp strong and owe Zhang Li.After gross tea is made, because of the difference of its subsequent handling is divided into " ripe tea " and " life tea ".By depositing what make its natural ageing all the year round is " give birth to tea ", and changes ripe through wet heap, just becomes " ripe tea ".The effect of Pu'er tea, on the books in Compendium of Material Medica, the traditional Chinese medical science thinks that Pu'er tea has heat-clearing simultaneously, relieves summer heat, detoxifies, helps digestion, goes rich, Li Shui, defaecation, eliminates the phlegm, expels pathogenic wind from the body surface, cough-relieving is promoted the production of body fluid, beneficial strength, effect such as promote longevity.And Pu'er cooked tea has sedimentation effects such as the therapeutic method to keep the adverse qi flowing downward, Li Shui, defaecation, and long-term drinking is useful to health.
The fragrance of Pu'er tea mainly is made up of terpenes and containing oxygen derivative thereof.Main fragrance component has instead-carypohyllene, p-cymene, 4-terpineol, cluck alkene, δ-elemene, α-humulene, linalool, dodecane, 4 (14), 11-folium eucalypti diene, isopropyl myristate, hexadecanoic acid, anethole, 3,5-octadiene-2-ketone, 3-(2,2-dimethyl propylidene) two ring [3.3.1] nonanes 1,4-diketone, geranyl acetone, 6,10,14-trimethyl-2-15 ketone etc., wherein based on instead-terpenes of carypohyllene is the abundantest.Instead-terpenes such as carypohyllene, α one humulene mostly belongs to woody type fragrance, terpene alcohol, terpene ketone, terpene ester etc. then have the sweet fragrance of a flower, sugar water fruital, the banksia rose, 1,2-dimethoxy-4 '-methylbenzene, 5-methyl isophthalic acid, 2,3-trimethoxy-benzene etc. then has old mould perfume (or spice), and these aroma substances have constituted the flavor characteristic of the sweet and pure and similar old camphor tree banksia rose of Pu'er cooked tea jointly.Pu'er cooked tea and extract thereof have the thick and heavy and strong smell of Chen Xiang of flavour glycol, after entering human body by respiratory tract, can bring into play special health-care effect.
Along with the problem of smoking with health more and more receives publicity, how to improve the security of sucking of cigarette, the harmful components in the reduction cigarette smoke, the comfort of aspirating that improves just become the focus of each tobacco productive corporation research and development.If the good characteristic that Pu'er cooked tea had can combine with cigarette, should be able to address the above problem well, but not see as yet in the prior art that relevant report is arranged.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, a kind of mineral ether-extracted Pu'er cooked tea extract is provided, use it for cigarette,, enrich cigarette cigarette perfume (or spice), improve the cigarette quality to reduce the harm of smoking to human body.
Another object of the present invention is to provide a kind of method for preparing described mineral ether-extracted Pu'er cooked tea extract.
The present invention also aims to provide the application of a kind of described mineral ether-extracted Pu'er cooked tea extract in cigarette.
Except as otherwise noted, percentage of the present invention is percetage by weight.
Purpose of the present invention is achieved by the following technical programs.
A kind of mineral ether-extracted Pu'er cooked tea extract is prepared by following method: Pu'er cooked tea and benzinum are mixed, obtain required Pu'er cooked tea extract through extraction, Separation of Solid and Liquid, distillation after concentrating.
The invention provides a kind of method for preparing mineral ether-extracted Pu'er cooked tea extract, this method comprises the step of following order:
(1) Pu'er cooked tea and benzinum are mixed, the mixed weight ratio is 1: 5～15;
(2) extract 10h～20h at ambient temperature;
(3) Separation of Solid and Liquid is collected supernatant liquid;
(4) decompression distillation 0.5～2.0h under vacuum 0.01～0.1MPa, 25 ℃～30 ℃ conditions of vapo(u)rizing temperature promptly obtains required medicinal extract except that after desolvating.
The preferred medical grade benzinum of described benzinum.
When described medical grade benzinum boiling point is 30 ℃～60 ℃, preferred 10h of extraction time.
When described medical grade benzinum boiling point is 60 ℃～90 ℃, preferred 20h of extraction time.
The invention provides the application of a kind of mineral ether-extracted Pu'er cooked tea extract in cigarette, be specially: it is 1～10% that mineral ether-extracted Pu'er cooked tea extract of the present invention is diluted to concentration with 95% ethanol, adds in the pipe tobacco by 0.01～0.1% of pipe tobacco weight then.
Preferably by pipe tobacco weight 0.05% with the dilution after mineral ether-extracted Pu'er cooked tea extract add in the pipe tobacco.
Preferably the mineral ether-extracted Pu'er cooked tea extract after diluting is added in the pipe tobacco with spray pattern.
The present invention has following beneficial effect:
1, Pu'er cooked tea also contains many identical with tobacco or similar fragrance components except that distinctive fragrance component own, adds in the pipe tobacco and can coordinate mutually with tobacco aroma, plays effect abundant, that coordinate cigarette perfume and give the tobacco characteristic perfume;
2, contain free amino acid in the Pu'er cooked tea, amino acid can be good at participating in mailland reaction and produces flavor matter in alcoholized tobacco, combustion process, thereby and can in and the alkaline matter in the tobacco reduce and stimulate, enrich cigarette perfume (or spice), reduce and stimulate and assorted gas, improve the mouthfeel pleasant impression;
3, extract and can carry out at ambient temperature with benzinum, do not need heating, extraction process is simple, and is easy and simple to handle, and room temperature condition extracts survivable to heat-labile Pu'er cooked tea flavor component down.Adopt the medical grade benzinum can guarantee that medicinal extract meets quality standard, and the Pu'er cooked tea extract that extracts can further extract the Pu'er cooked tea absolute oil;
4, technology is simple, and is easy and simple to handle, need not to change existing production technology, can significantly improve the cigarette quality.
The specific embodiment
The present invention is described in further detail below in conjunction with embodiment and Application Example, but they are not limitation of the invention.
Embodiment 1
With electronic balance weighing Pu'er cooked tea 500 grams, pack in the flask, adding 2500ml boiling point is 30～60 ℃ a medical grade benzinum, under 20 ℃ of conditions, soak 10h, carry out Separation of Solid and Liquid with Bush's funnel, collect supernatant liquid, the liquid that obtains is that 0.05MPa, vapo(u)rizing temperature are that distillation concentrates 2.0h under 28 ℃ of conditions in vacuum, and removing desolvates obtains medicinal extract 1.8 grams.
Embodiment 2
With electronic balance weighing Pu'er cooked tea 1000 grams, the conical flask of packing into, adding 10000ml boiling point is 60～90 ℃ a benzinum, under 30 ℃ of conditions, soak 20h, carry out Separation of Solid and Liquid with Bush's funnel, collect supernatant liquid, the liquid that obtains is that 0.1MPa, vapo(u)rizing temperature are that distillation concentrates 1.0h under 30 ℃ of conditions in vacuum, and removing desolvates obtains to such an extent that medicinal extract 10.13 restrains.
Embodiment 3
With electronic balance weighing Pu'er cooked tea 1000 grams, the conical flask of packing into, adding 15000ml boiling point is 30～60 ℃ a benzinum, under 15 ℃ of conditions, soak 10h, carry out Separation of Solid and Liquid with Bush's funnel, collect supernatant liquid, the liquid that obtains is that 0.01MPa, vapo(u)rizing temperature are that distillation concentrates 1.5h under 25 ℃ of conditions in vacuum, and removing desolvates obtains to such an extent that medicinal extract 10.20 restrains.
Application Example 1
Is standby after 1% concentration with embodiment 1 gained mineral ether-extracted Pu'er cooked tea extract with 95% ethanol dissolved dilution.Be sprayed onto Yunnan Flue-cured Tobacco X by 0.01%, 0.05% and 0.1% of pipe tobacco weight respectively
2Roll into cigarette in the F pipe tobacco, adopt the contrast method of smokeing panel test to smoke panel test, smoking result sees the following form:
| Sample | Smoking result |
| X 2The F pipe tobacco | Flue gas is rich slightly poor, and cigarette perfume (or spice) is lighter. |
| Apply the X of 0.01% Pu'er cooked tea extract 2The F pipe tobacco | Flue gas is than horn of plenty, and excitant decreases. |
| Apply 0.05% | Flue gas is than horn of plenty, and joyful sense is better, and Chen Xiang, banksia rose feature are better, sweet sense |
| The X of Pu'er cooked tea extract 2The F pipe tobacco | Increase to some extent, excitant decreases. |
| Apply the X of 0.1% Pu'er cooked tea extract 2The F pipe tobacco | Flue gas is than horn of plenty, and Chen Xiang, banksia rose feature are better, and stimulating to some extent increases. |
Application Example 2
Is standby after 5% concentration with embodiment 2 gained mineral ether-extracted Pu'er cooked tea extracts with 95% ethanol dissolved dilution.Be sprayed onto Yunnan Flue-cured Tobacco X by 0.01%, 0.05% and 0.1% of pipe tobacco weight respectively
3Roll into cigarette in the F pipe tobacco, adopt the contrast method of smokeing panel test to smoke panel test, smoking result sees the following form:
| Sample | Smoking result |
| X 3The F pipe tobacco | Flue gas is rich slightly poor, and cigarette perfume (or spice) is lighter. |
| Apply the X of 0.01% Pu'er cooked tea extract 3The F pipe tobacco | Fragrance is than horn of plenty, and fragrance matter promotes to some extent. |
| Sample | Smoking result |
| Apply the X of 0.05% Pu'er cooked tea extract 3The F pipe tobacco | Fragrance is than horn of plenty, coordination, and Chen Xiang, banksia rose feature are better, and the pure and mild property of fragrance promotes to some extent, and excitant decreases. |
| Apply the X of 0.1% Pu'er cooked tea extract 3The F pipe tobacco | Fragrance is than horn of plenty, and Chen Xiang, banksia rose feature are better, and stimulating to some extent increases. |
Application Example 3
Is standby after 10% concentration with embodiment 3 gained mineral ether-extracted Pu'er cooked tea extracts with 95% ethanol dissolved dilution.Be sprayed onto Yunnan Flue-cured Tobacco C by 0.01%, 0.05% and 0.1% of pipe tobacco weight respectively
3Roll into cigarette in the F pipe tobacco, adopt the contrast method of smokeing panel test to smoke panel test, smoking result sees the following form:
| Sample | Smoking result |
| C 3The F pipe tobacco | Flue gas is rich slightly poor, and cigarette perfume (or spice) is lighter. |
| Apply the C of 0.01% Pu'er cooked tea extract 3The F pipe tobacco | Fragrance is than horn of plenty, and fine and smooth sense better. |
| Apply the C of 0.05% Pu'er cooked tea extract 3The F pipe tobacco | Fragrance is than horn of plenty, coordination, and Chen Xiang, banksia rose feature are better, and the pure and mild property of fragrance promotes to some extent, and excitant decreases. |
| Apply the C of 0.1% Pu'er cooked tea extract 3The F pipe tobacco | Fragrance is than horn of plenty, and Chen Xiang, banksia rose feature are better, and stimulating to some extent increases. |
Claims (9)
1. a mineral ether-extracted Pu'er cooked tea extract is characterized in that: Pu'er cooked tea and benzinum are mixed, make product through extraction, Separation of Solid and Liquid, distillation after concentrating.
2. method for preparing the described mineral ether-extracted Pu'er cooked tea extract of claim 1, this method comprises the step of following order:
(1) Pu'er cooked tea and benzinum are mixed, the mixed weight ratio is 1: 5～15;
(2) extract 10h～20h at ambient temperature;
(3) Separation of Solid and Liquid is collected supernatant liquid;
(4) decompression distillation 0.5～2.0h under vacuum 0.01～0.1MPa, 25 ℃～30 ℃ conditions of vapo(u)rizing temperature promptly obtains required medicinal extract except that after desolvating.
3. method according to claim 2 is characterized in that: described benzinum is the medical grade benzinum.
4. method according to claim 3 is characterized in that: when described medical grade benzinum boiling point was 30 ℃～60 ℃, the extraction time was 10h.
5. method according to claim 3 is characterized in that: when described medical grade benzinum boiling point was 60 ℃～90 ℃, the extraction time was 20h.
6. the application of the described mineral ether-extracted Pu'er cooked tea extract of claim 1 in adding cigarette shreds.
7. the application of mineral ether-extracted Pu'er cooked tea extract according to claim 6 in adding cigarette shreds, it is characterized in that: it is 1～10% that described mineral ether-extracted Pu'er cooked tea extract is diluted to concentration with 95% ethanol, adds in the pipe tobacco by 0.01～0.1% of pipe tobacco weight then.
8. application according to claim 7 is characterized in that: by pipe tobacco weight 0.05% with the dilution after mineral ether-extracted Pu'er cooked tea extract add in the pipe tobacco.
9. application according to claim 7 is characterized in that: with spray pattern the mineral ether-extracted Pu'er cooked tea extract after diluting is added in the pipe tobacco.
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| CN2008100587602A CN101322581B (en) | 2008-07-29 | 2008-07-29 | Mineral ether-extracted Pu'er cooked tea extract and preparation and use thereof |
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| CN2008100587602A CN101322581B (en) | 2008-07-29 | 2008-07-29 | Mineral ether-extracted Pu'er cooked tea extract and preparation and use thereof |
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| CN101322581B true CN101322581B (en) | 2010-09-29 |
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| CN103999993B (en) * | 2014-05-04 | 2015-12-09 | 安徽中草香料有限公司 | A kind of preparation method of green tea extract |
| CN105779307B (en) * | 2016-04-18 | 2019-04-05 | 云南中烟工业有限责任公司 | A kind of trichoderma aureoviride bacterial strain and the method for preparing Pu'er tea tobacco aromaticss with it |
| CN105996115B (en) * | 2016-07-18 | 2018-08-17 | 福建中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke with extra-strong tea just object extract preparation processed |
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Owner name: HONGYUN HONGHE TOBACCO(GROUP )CO.LTD. Free format text: FORMER OWNER: HONGYUN TOBACCO (GROUP) CO.,LTD. Effective date: 20090703 |
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Effective date of registration: 20090703 Address after: Yunnan province Kunming City area village post encoding: 650202 Applicant after: Hongyun Honghe tobacco (Group) Co., Ltd. Address before: Yunnan province Kunming City area village post encoding: 650202 Applicant before: Hongyun Tobacco (Group) Co., Ltd. |
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