CN103409008B - Interior wall coating of a kind of high adhesive force and preparation method thereof - Google Patents
Interior wall coating of a kind of high adhesive force and preparation method thereof Download PDFInfo
- Publication number
- CN103409008B CN103409008B CN201310275747.3A CN201310275747A CN103409008B CN 103409008 B CN103409008 B CN 103409008B CN 201310275747 A CN201310275747 A CN 201310275747A CN 103409008 B CN103409008 B CN 103409008B
- Authority
- CN
- China
- Prior art keywords
- mentioned
- coating
- stirring
- rev
- interior wall
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a kind of interior wall coating of high adhesive force, it is made up of the raw material of following weight parts: benzene emulsion 40-50, modified adhesive 20-26, mica powder 20-25, nano-calcium carbonate 20-25, Natvosol 2-3, vinylcarbinol 2-3, ethylene glycol 3-4, tripoly phosphate sodium STPP 3-4, HMPA 1-2, alcohol ester 12 film coalescence aid 2-3, ethylenediamine tetramethylene fork Alendronate 3-4, calcium zinc stabilizer 0.2-0.3, γ-aminopropyl triethoxysilane 0.8-1, deionized water 20-40; Each recipe ingredient of the present invention has good consistency, dispersiveness and stability, the coating products coating produced is firm, smooth surface, strong adhesion, abrasion resistance, resistance to acids and bases, resistance to soiling are strong, safety and environmental protection, the modified adhesive added further enhancing the cohesiveness of coating, make coating more difficult drop-off, improve the performance of coating.
Description
Technical field
The present invention relates generally to a kind of coating, particularly relates to a kind of interior wall coating of high adhesive force.
Background technology
Interior wall coating is the important component part of building and ornament materials, mostly be made up of emulsion, deionized water, pigment and other auxiliary agents, the deficiency that but most of interior wall coating still exists, and coating is not firm, sticking power is not strong, coating easily comes off, abrasion resistance, resistance to acids and bases, resistance to soiling are not strong, nuisance substantially exceeds the aspects such as national limit standard, therefore, a kind of high-performance is produced and nontoxic construction coating for internal wall is real is expected by people.
Summary of the invention
The object of the invention is just to provide a kind of interior wall coating of high adhesive force.
The present invention is achieved by the following technical solutions:
An interior wall coating for high adhesive force, it is made up of the raw material of following weight parts:
Benzene emulsion 40-50, modified adhesive 20-26, mica powder 20-25, nano-calcium carbonate 20-25, Natvosol 2-3, vinylcarbinol 2-3, ethylene glycol 3-4, tripoly phosphate sodium STPP 3-4, HMPA 1-2, alcohol ester 12 film coalescence aid 2-3, ethylenediamine tetramethylene fork Alendronate 3-4, calcium zinc stabilizer 0.2-0.3, γ-aminopropyl triethoxysilane 0.8-1, deionized water 20-40;
Described modified adhesive is made up of the raw material of following weight parts:
Nano-bentonite 90-100, puffing glutinous rice powder 60-70, sodium laurylsulfate 2-4, vinyltriethoxysilane 1-2,1,2-two (triethoxy is silica-based) ethane 1-2, aluminium hydroxide 3-5, di-t-butyl peroxide 1-2, ethanol 6-8, polyvinyl alcohol 6-8, polypropylene glycerol aether 0.1-0.2, propylene glycol 2-4;
The preparation method of described modified adhesive comprises the following steps:
(1) nano-bentonite is put into 5-6 times of water gaging, then add above-mentioned sodium laurylsulfate, vinyltriethoxysilane, 1,2-two (triethoxy is silica-based) ethane, aluminium hydroxide, high speed 1200-1500 rev/min of stirring, obtains dispersion liquid;
(2) di-t-butyl peroxide of above-mentioned weight part is mixed with ethanol, stirring and dissolving, obtain lysate;
The polyvinyl alcohol of above-mentioned weight part is joined in 8-12 stirring at normal temperature water doubly, add hydrochloric acid, adjustment PH is 2-3, be 90-100 DEG C with being steam heated to temperature, Keep agitation, dissolve completely to polyvinyl alcohol, insulation 30-40 minute, adds above-mentioned polypropylene glycerol aether, propylene glycol, dispersed with stirring 15-20 minute, add sodium hydroxide, adjustment PH is 5-7, and then reducing vapor temperature is 65-75 DEG C, adds above-mentioned puffing glutinous rice powder and puffing glutinous rice grain weight amount 1-2 deionized water doubly, dispersed with stirring 30-40 minute, obtains mixed solution;
(3) by dispersion liquid obtained above, lysate, mixed solution mixing, low speed 200-300 rev/min of stirring 3-5 minute, adds hydrochloric acid or sodium hydroxide regulates PH for neutral, and ball-milling processing 2-3 hour, obtains described modified adhesive.
A preparation method for the interior wall coating of high adhesive force, comprises the following steps:
(1) 50-60% of above-mentioned Natvosol, vinylcarbinol, ethylene glycol, tripoly phosphate sodium STPP, HMPA, alcohol ester 12 film coalescence aid, deionized water weight is mixed to join in dispersion cylinder, 1000-1200 rev/min, high speed dispersion 3-5min;
(2) above-mentioned mica powder, nano-calcium carbonate is added, 1200-1600 rev/min, high speed dispersion 20-30min;
(3) add above-mentioned modified adhesive, 200-300 rev/min, low speed dispersion 4-6 minute, then add each raw material of residue, 400-600 rev/min, is uniformly dispersed, and obtains the interior wall coating of described high adhesive force.
Advantage of the present invention is:
Each recipe ingredient of the present invention has good consistency, dispersiveness and stability, the coating products coating produced is firm, smooth surface, strong adhesion, abrasion resistance, resistance to acids and bases, resistance to soiling are strong, safety and environmental protection, the modified adhesive added further enhancing the cohesiveness of coating, make coating more difficult drop-off, improve the performance of coating.
Embodiment
Embodiment 1
An interior wall coating for high adhesive force, it is made up of the raw material of following weight parts (kilogram):
Benzene emulsion 40-50, modified adhesive 20-26, mica powder 20-25, nano-calcium carbonate 20-25, Natvosol 2-3, vinylcarbinol 2-3, ethylene glycol 3-4, tripoly phosphate sodium STPP 3-4, HMPA 1-2, alcohol ester 12 film coalescence aid 2-3, ethylenediamine tetramethylene fork Alendronate 3-4, calcium zinc stabilizer 0.2-0.3, γ-aminopropyl triethoxysilane 0.8-1, deionized water 20-40;
Described modified adhesive is made up of the raw material of following weight parts:
Nano-bentonite 100, puffing glutinous rice powder 70, sodium laurylsulfate 4, vinyltriethoxysilane 2,1,2-two (triethoxy is silica-based) ethane 1-2, aluminium hydroxide 3, di-t-butyl peroxide 2, ethanol 8, polyvinyl alcohol 8, polypropylene glycerol aether 0.2, propylene glycol 4;
The preparation method of described modified adhesive comprises the following steps:
(1) nano-bentonite is put into 6 times of water gagings, then add above-mentioned sodium laurylsulfate, vinyltriethoxysilane, 1,2-two (triethoxy is silica-based) ethane, aluminium hydroxide, 1500 revs/min of stirrings at a high speed, obtain dispersion liquid;
(2) di-t-butyl peroxide of above-mentioned weight part is mixed with ethanol, stirring and dissolving, obtain lysate;
The polyvinyl alcohol of above-mentioned weight part is joined in the stirring at normal temperature water of 10 times, adds hydrochloric acid, regulate PH to be 2, be 100 DEG C with being steam heated to temperature, Keep agitation, dissolves completely to polyvinyl alcohol, be incubated 40 minutes, add above-mentioned polypropylene glycerol aether, propylene glycol, dispersed with stirring 15-20 minute, add sodium hydroxide, adjustment PH is 5-7, and then reducing vapor temperature is 75 DEG C, adds the deionized water of above-mentioned puffing glutinous rice powder and puffing glutinous rice grain weight amount 2 times, dispersed with stirring 40 minutes, obtains mixed solution;
(3) by dispersion liquid obtained above, lysate, mixed solution mixing, low speed 300 revs/min stirring 5 minutes, adds hydrochloric acid or sodium hydroxide regulates PH for neutral, and ball-milling processing 3 hours, obtains described modified adhesive.
A preparation method for the interior wall coating of high adhesive force, comprises the following steps:
(1) above-mentioned Natvosol, vinylcarbinol, ethylene glycol, tripoly phosphate sodium STPP, HMPA, alcohol ester 12 film coalescence aid, deionized water weight 50-60% are mixed to join in dispersion cylinder, 1200 revs/min, high speed dispersion 5min;
(2) above-mentioned mica powder, nano-calcium carbonate is added, 1600 revs/min, high speed dispersion 30min;
(3) add above-mentioned modified adhesive, 300 revs/min, low speed disperses 6 minutes, then adds each raw material of residue, 600 revs/min, is uniformly dispersed, obtains the interior wall coating of described high adhesive force.
Performance test:
Paint film appearance is smooth, good without lump, good hand touch, glossiness;
Abrasion resistance is tested: pass through for 1000 times, paint film is without breakage;
Artificial ageing resistance test: 2000 hours non-foaming, do not peel off, flawless;
Water tolerance: 140h paint film is without breakage;
Alkali resistance: 120h paint film is without breakage.
Claims (2)
1. an interior wall coating for high adhesive force, is characterized in that it is made up of the raw material of following weight parts: benzene emulsion 40-50, modified adhesive 20-26, mica powder 20-25, nano-calcium carbonate 20-25, Natvosol 2-3, vinylcarbinol 2-3, ethylene glycol 3-4, tripoly phosphate sodium STPP 3-4, HMPA 1-2, alcohol ester 12 film coalescence aid 2-3, ethylenediamine tetramethylene fork Alendronate 3-4, calcium zinc stabilizer 0.2-0.3, γ-aminopropyl triethoxysilane 0.8-1, deionized water 20-40;
Described modified adhesive comprises the raw material of following weight parts: nano-bentonite 90-100, puffing glutinous rice powder 60-70, sodium laurylsulfate 2-4, vinyltriethoxysilane 1-2,1,2-two (triethoxy is silica-based) ethane 1-2, aluminium hydroxide 3-5, di-t-butyl peroxide 1-2, ethanol 6-8, polyvinyl alcohol 6-8, polypropylene glycerol aether 0.1-0.2, propylene glycol 2-4;
The preparation method of described modified adhesive comprises the following steps:
(1) nano-bentonite is put into 5-6 times of water gaging, then add above-mentioned sodium laurylsulfate, vinyltriethoxysilane, 1,2-two (triethoxy is silica-based) ethane, aluminium hydroxide, high speed 1200-1500 rev/min of stirring, obtains dispersion liquid;
(2) di-t-butyl peroxide of above-mentioned weight part is mixed with ethanol, stirring and dissolving, obtain lysate; The polyvinyl alcohol of above-mentioned weight part is joined in 8-12 stirring at normal temperature water doubly, add hydrochloric acid, adjustment pH is 2-3, be 90-100 DEG C with being steam heated to temperature, Keep agitation, dissolve completely to polyvinyl alcohol, insulation 30-40 minute, adds above-mentioned polypropylene glycerol aether, propylene glycol, dispersed with stirring 15-20 minute, add sodium hydroxide, adjustment pH is 5-7, and then reducing vapor temperature is 65-75 DEG C, adds above-mentioned puffing glutinous rice powder and puffing glutinous rice grain weight amount 1-2 deionized water doubly, dispersed with stirring 30-40 minute, obtains mixed solution;
(3) by dispersion liquid obtained above, lysate, mixed solution mixing, low speed 200-300 rev/min of stirring 3-5 minute, adds hydrochloric acid or sodium hydroxide regulates pH for neutral, and ball-milling processing 2-3 hour, obtains described modified adhesive.
2. a preparation method for the interior wall coating of high adhesive force as claimed in claim 1, is characterized in that comprising the following steps:
(1) 50-60% of above-mentioned Natvosol, vinylcarbinol, ethylene glycol, tripoly phosphate sodium STPP, HMPA, alcohol ester 12 film coalescence aid, deionized water weight is mixed to join in dispersion cylinder, 1000-1200 rev/min, high speed dispersion 3-5min;
(2) above-mentioned mica powder, nano-calcium carbonate is added, 1200-1600 rev/min, high speed dispersion 20-30min;
(3) add above-mentioned modified adhesive, 200-300 rev/min, low speed dispersion 4-6 minute, then add each raw material of residue, 400-600 rev/min, is uniformly dispersed, and obtains the interior wall coating of described high adhesive force.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310275747.3A CN103409008B (en) | 2013-07-03 | 2013-07-03 | Interior wall coating of a kind of high adhesive force and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310275747.3A CN103409008B (en) | 2013-07-03 | 2013-07-03 | Interior wall coating of a kind of high adhesive force and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103409008A CN103409008A (en) | 2013-11-27 |
| CN103409008B true CN103409008B (en) | 2016-01-20 |
Family
ID=49602053
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310275747.3A Active CN103409008B (en) | 2013-07-03 | 2013-07-03 | Interior wall coating of a kind of high adhesive force and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103409008B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104177945A (en) * | 2014-08-21 | 2014-12-03 | 苏州靖羽新材料有限公司 | Polyvinyl alcohol bentonite interior wall paint |
| CN106118459A (en) * | 2016-07-04 | 2016-11-16 | 铜陵方正塑业科技有限公司 | A kind of casein modified film coating and preparation method thereof |
| US20200071535A1 (en) * | 2017-05-05 | 2020-03-05 | Basf Se | Fluidically applicable vapor retarder |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1048558A (en) * | 1989-07-03 | 1991-01-16 | 宋祥生 | Modified emulsion binder and preparation method thereof |
| CN102079916A (en) * | 2009-12-01 | 2011-06-01 | 邹敏 | Water-based waterproof paint |
| CN102618177A (en) * | 2012-04-11 | 2012-08-01 | 宣城晶瑞新材料有限公司 | Special nano modified bonding agent for ceramic and preparation method of bonding agent |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102004044662A1 (en) * | 2004-09-15 | 2006-03-30 | Ashland-Südchemie-Kernfest GmbH | Thixotropic coating compositions |
-
2013
- 2013-07-03 CN CN201310275747.3A patent/CN103409008B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1048558A (en) * | 1989-07-03 | 1991-01-16 | 宋祥生 | Modified emulsion binder and preparation method thereof |
| CN102079916A (en) * | 2009-12-01 | 2011-06-01 | 邹敏 | Water-based waterproof paint |
| CN102618177A (en) * | 2012-04-11 | 2012-08-01 | 宣城晶瑞新材料有限公司 | Special nano modified bonding agent for ceramic and preparation method of bonding agent |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103409008A (en) | 2013-11-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103409008B (en) | Interior wall coating of a kind of high adhesive force and preparation method thereof | |
| CN103788781B (en) | A kind of frie retardant coating adding modified nano zeolite powder | |
| CN103525211B (en) | A kind of exterior wall latex coating | |
| CN103409007B (en) | A kind of ageing-resistant interior wall coating and preparation method thereof | |
| CN106046905A (en) | Environment-friendly anti-crack material for wall decoration and preparation method thereof | |
| CN103173076B (en) | A kind of exterior coating and preparation method thereof | |
| CN101891411A (en) | Waterproofing gypsum agent preparation method | |
| CN103409009B (en) | A kind of high alkaline-resisting interior wall coating and preparation method thereof | |
| CN104326726A (en) | Light thermal-insulation exterior-wall coating | |
| CN104046144B (en) | A kind of clean taste emulsion paint | |
| CN103773170B (en) | A kind of frie retardant coating adding biotite powder | |
| CN101323704B (en) | Resin slicer for granite sand wall paint, preparation and use thereof | |
| CN109337608A (en) | A kind of starch-based adhesive and preparation method thereof having flame retarding function | |
| CN103409010A (en) | Anti-scrubbing interior wall coating material and preparation method thereof | |
| CN104790265A (en) | Mixed fiber wallpaper and making method thereof | |
| CN103409006A (en) | Environment-friendly internal wall paint and preparation method thereof | |
| CN104845488A (en) | Impact resistant fireproof coating and preparation method thereof | |
| CN105802319A (en) | Anti-microbial putty powder and preparation method thereof | |
| CN103614011B (en) | A kind of waterproof paint containing oyster shell powder | |
| CN104263121A (en) | Polyvinyl acetate latex paint | |
| CN103525206B (en) | A kind of Staining-resistant heat-insulationcoatiand | |
| CN105778603A (en) | Environment-friendly interior wall putty with indoor humidity adjustment function | |
| CN104231803A (en) | Heat insulation and heat preservation latex paint | |
| CN104355592B (en) | The building coating that cementability is good | |
| CN103980778A (en) | High solid content exterior wall coating |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |