CN103409007B - A kind of ageing-resistant interior wall coating and preparation method thereof - Google Patents
A kind of ageing-resistant interior wall coating and preparation method thereof Download PDFInfo
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- CN103409007B CN103409007B CN201310275746.9A CN201310275746A CN103409007B CN 103409007 B CN103409007 B CN 103409007B CN 201310275746 A CN201310275746 A CN 201310275746A CN 103409007 B CN103409007 B CN 103409007B
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Abstract
The invention discloses a kind of ageing-resistant interior wall coating, it is made up of the raw material of following weight parts: benzene emulsion 50-60, modified adhesive 30-34, nanometer sepiolite 30-35, nano zine oxide 10-15, methyl hydroxyethylcellulose 2-5, Sorbitol Powder 2-3, glycerol 2-3, Xylo-Mucine 2-4, ethylene glycol monobutyl ether 1-2, alcohol ester 12 film coalescence aid 2-3, ethylenediamine tetramethylene fork Alendronate 2-3, methyl-silicone oil 0.2-0.3, 1, two (triethoxy is silica-based) ethane 0.6-1 of 2-, dodecyl dimethyl benzyl ammonium bromide 1-2, deionized water 20-40, each recipe ingredient of the present invention has good consistency, dispersiveness and stability, the coating products coating produced is firm, smooth surface, strong adhesion, abrasion resistance, resistance to acids and bases, resistance to soiling are strong, safety and environmental protection, the modified adhesive added further enhancing the cohesiveness of coating, make coating more difficult drop-off, improve the performance of coating.
Description
Technical field
The present invention relates generally to a kind of coating, particularly relates to a kind of ageing-resistant interior wall coating.
Background technology
Interior wall coating is the important component part of building and ornament materials, mostly be made up of emulsion, deionized water, pigment and other auxiliary agents, the deficiency that but most of interior wall coating still exists, and coating is not firm, sticking power is not strong, coating easily comes off, abrasion resistance, resistance to acids and bases, resistance to soiling are not strong, nuisance substantially exceeds the aspects such as national limit standard, therefore, a kind of high-performance is produced and nontoxic construction coating for internal wall is real is expected by people.
Summary of the invention
The object of the invention is just to provide a kind of ageing-resistant interior wall coating.
The present invention is achieved by the following technical solutions:
An ageing-resistant interior wall coating, it is made up of the raw material of following weight parts:
Benzene emulsion 50-60, modified adhesive 30-34, nanometer sepiolite 30-35, nano zine oxide 10-15, methyl hydroxyethylcellulose 2-5, Sorbitol Powder 2-3, glycerol 2-3, Xylo-Mucine 2-4, ethylene glycol monobutyl ether 1-2, alcohol ester 12 film coalescence aid 2-3, ethylenediamine tetramethylene fork Alendronate 2-3, methyl-silicone oil 0.2-0.3,1,2-two (triethoxy is silica-based) ethane 0.6-1, dodecyl dimethyl benzyl ammonium bromide 1-2, deionized water 20-40;
Described modified adhesive is made up of the raw material of following weight parts:
Nano-bentonite 90-100, puffing glutinous rice powder 60-70, sodium laurylsulfate 2-4, vinyltriethoxysilane 1-2,1,2-two (triethoxy is silica-based) ethane 1-2, aluminium hydroxide 3-5, di-t-butyl peroxide 1-2, ethanol 6-8, polyvinyl alcohol 6-8, polypropylene glycerol aether 0.1-0.2, propylene glycol 2-4;
The preparation method of described modified adhesive comprises the following steps:
(1) nano-bentonite is put into 5-6 times of water gaging, then add above-mentioned sodium laurylsulfate, vinyltriethoxysilane, 1,2-two (triethoxy is silica-based) ethane, aluminium hydroxide, high speed 1200-1500 rev/min of stirring, obtains dispersion liquid;
(2) di-t-butyl peroxide of above-mentioned weight part is mixed with ethanol, stirring and dissolving, obtain lysate;
The polyvinyl alcohol of above-mentioned weight part is joined in 8-12 stirring at normal temperature water doubly, add hydrochloric acid, adjustment pH is 2-3, be 90-100 DEG C with being steam heated to temperature, Keep agitation, dissolve completely to polyvinyl alcohol, insulation 30-40 minute, adds above-mentioned polypropylene glycerol aether, propylene glycol, dispersed with stirring 15-20 minute, add sodium hydroxide, adjustment pH is 5-7, and then reducing vapor temperature is 65-75 DEG C, adds above-mentioned puffing glutinous rice powder and puffing glutinous rice grain weight amount 1-2 deionized water doubly, dispersed with stirring 30-40 minute, obtains mixed solution;
(3) by dispersion liquid obtained above, lysate, mixed solution mixing, low speed 200-300 rev/min of stirring 3-5 minute, adds hydrochloric acid or sodium hydroxide regulates pH for neutral, and ball-milling processing 2-3 hour, obtains described modified adhesive.
A preparation method for ageing-resistant interior wall coating, comprises the following steps:
(1) 60-70% of above-mentioned methyl hydroxyethylcellulose, Sorbitol Powder, glycerol, Xylo-Mucine, ethylene glycol monobutyl ether, alcohol ester 12 film coalescence aid, deionized water weight is mixed to join in dispersion cylinder, 1000-1200 rev/min, high speed dispersion 3-5min;
(2) above-mentioned nanometer sepiolite, nano zine oxide is added, 1200-1600 rev/min, high speed dispersion 20-30min;
(3) add above-mentioned modified adhesive, 200-300 rev/min, low speed dispersion 4-6 minute, then add each raw material of residue, 400-600 rev/min, is uniformly dispersed, and obtains described ageing-resistant interior wall coating.
Advantage of the present invention is:
Each recipe ingredient of the present invention has good consistency, dispersiveness and stability, the coating products coating produced is firm, smooth surface, strong adhesion, abrasion resistance, resistance to acids and bases, resistance to soiling are strong, safety and environmental protection, the modified adhesive added further enhancing the cohesiveness of coating, make coating more difficult drop-off, improve the performance of coating.
Embodiment
Embodiment 1
An ageing-resistant interior wall coating, it is made up of the raw material of following weight parts (kilogram):
Benzene emulsion 50-60, modified adhesive 30-34, nanometer sepiolite 30-35, nano zine oxide 10-15, methyl hydroxyethylcellulose 2-5, Sorbitol Powder 2-3, glycerol 2-3, Xylo-Mucine 2-4, ethylene glycol monobutyl ether 1-2, alcohol ester 12 film coalescence aid 2-3, ethylenediamine tetramethylene fork Alendronate 2-3, methyl-silicone oil 0.2-0.3,1,2-two (triethoxy is silica-based) ethane 0.6-1, dodecyl dimethyl benzyl ammonium bromide 1-2, deionized water 20-40;
Described modified adhesive is made up of the raw material of following weight parts:
Nano-bentonite 100, puffing glutinous rice powder 70, sodium laurylsulfate 4, vinyltriethoxysilane 2,1,2-two (triethoxy is silica-based) ethane 1-2, aluminium hydroxide 3, di-t-butyl peroxide 2, ethanol 8, polyvinyl alcohol 8, polypropylene glycerol aether 0.2, propylene glycol 4;
The preparation method of described modified adhesive comprises the following steps:
(1) nano-bentonite is put into 6 times of water gagings, then add above-mentioned sodium laurylsulfate, vinyltriethoxysilane, 1,2-two (triethoxy is silica-based) ethane, aluminium hydroxide, 1500 revs/min of stirrings at a high speed, obtain dispersion liquid;
(2) di-t-butyl peroxide of above-mentioned weight part is mixed with ethanol, stirring and dissolving, obtain lysate;
The polyvinyl alcohol of above-mentioned weight part is joined in the stirring at normal temperature water of 10 times, adds hydrochloric acid, regulate pH to be 2, be 100 DEG C with being steam heated to temperature, Keep agitation, dissolves completely to polyvinyl alcohol, be incubated 40 minutes, add above-mentioned polypropylene glycerol aether, propylene glycol, dispersed with stirring 15-20 minute, add sodium hydroxide, adjustment pH is 5-7, and then reducing vapor temperature is 75 DEG C, adds the deionized water of above-mentioned puffing glutinous rice powder and puffing glutinous rice grain weight amount 2 times, dispersed with stirring 40 minutes, obtains mixed solution;
(3) by dispersion liquid obtained above, lysate, mixed solution mixing, low speed 300 revs/min stirring 5 minutes, adds hydrochloric acid or sodium hydroxide regulates pH for neutral, and ball-milling processing 3 hours, obtains described modified adhesive.
A preparation method for ageing-resistant interior wall coating, comprises the following steps:
(1) by above-mentioned methyl hydroxyethylcellulose, Sorbitol Powder, glycerol, Xylo-Mucine, ethylene glycol monobutyl ether, alcohol ester 12 film coalescence aid, deionized water weight 70% be mixed to join in dispersion cylinder, 1200 revs/min, high speed dispersion 5min;
(2) above-mentioned nanometer sepiolite, nano zine oxide is added, 1600 revs/min, high speed dispersion 30min;
(3) add above-mentioned modified adhesive, 300 revs/min, low speed disperses 6 minutes, then adds each raw material of residue, 600 revs/min, is uniformly dispersed, obtains described ageing-resistant interior wall coating.
Performance test:
Paint film appearance is smooth, good without lump, good hand touch, glossiness;
Abrasion resistance is tested: pass through for 1000 times, paint film is without breakage;
Artificial ageing resistance test: 2000 hours non-foaming, do not peel off, flawless;
Water tolerance: 140h paint film is without breakage;
Alkali resistance: 120h paint film is without breakage.
Claims (2)
1. an ageing-resistant interior wall coating, it is characterized in that it is made up of the raw material of following weight parts: benzene emulsion 50-60, modified adhesive 30-34, nanometer sepiolite 30-35, nano zine oxide 10-15, methyl hydroxyethylcellulose 2-5, Sorbitol Powder 2-3, glycerol 2-3, Xylo-Mucine 2-4, ethylene glycol monobutyl ether 1-2, alcohol ester 12 film coalescence aid 2-3, ethylenediamine tetramethylene fork Alendronate 2-3, methyl-silicone oil 0.2-0.3, 1, two (triethoxy is silica-based) ethane 0.6-1 of 2-, dodecyl dimethyl benzyl ammonium bromide 1-2, deionized water 20-40,
Described modified adhesive is made up of the raw material of following weight parts: nano-bentonite 90-100, puffing glutinous rice powder 60-70, sodium laurylsulfate 2-4, vinyltriethoxysilane 1-2,1,2-two (triethoxy is silica-based) ethane 1-2, aluminium hydroxide 3-5, di-t-butyl peroxide 1-2, ethanol 6-8, polyvinyl alcohol 6-8, polypropylene glycerol aether 0.1-0.2, propylene glycol 2-4;
The preparation method of described modified adhesive comprises the following steps:
1) nano-bentonite is put into 5-6 times of water gaging, then add above-mentioned sodium laurylsulfate, vinyltriethoxysilane, 1,2-two (triethoxy is silica-based) ethane, aluminium hydroxide, high speed 1200-1500 rev/min of stirring, obtains dispersion liquid;
2) di-t-butyl peroxide of above-mentioned weight part is mixed with ethanol, stirring and dissolving, obtain lysate; The polyvinyl alcohol of above-mentioned weight part is joined in 8-12 stirring at normal temperature water doubly, add hydrochloric acid, adjustment pH is 2-3, be 90-100 DEG C with being steam heated to temperature, Keep agitation, dissolve completely to polyvinyl alcohol, insulation 30-40 minute, adds above-mentioned polypropylene glycerol aether, propylene glycol, dispersed with stirring 15-20 minute, add sodium hydroxide, adjustment pH is 5-7, and then reducing vapor temperature is 65-75 DEG C, adds above-mentioned puffing glutinous rice powder and puffing glutinous rice grain weight amount 1-2 deionized water doubly, dispersed with stirring 30-40 minute, obtains mixed solution;
3) by dispersion liquid obtained above, lysate, mixed solution mixing, low speed 200-300 rev/min of stirring 3-5 minute, adds hydrochloric acid or sodium hydroxide regulates pH for neutral, and ball-milling processing 2-3 hour, obtains described modified adhesive.
2. a preparation method for ageing-resistant interior wall coating as claimed in claim 1, is characterized in that comprising the following steps:
(1) 60-70% of above-mentioned methyl hydroxyethylcellulose, Sorbitol Powder, glycerol, Xylo-Mucine, ethylene glycol monobutyl ether, alcohol ester 12 film coalescence aid, deionized water weight is mixed to join in dispersion cylinder, 1000-1200 rev/min, high speed dispersion 3-5min;
(2) above-mentioned nanometer sepiolite, nano zine oxide is added, 1200-1600 rev/min, high speed dispersion 20-30min; (3) add above-mentioned modified adhesive, 200-300 rev/min, low speed dispersion 4-6 minute, then add each raw material of residue, 400-600 rev/min, is uniformly dispersed, and obtains described ageing-resistant interior wall coating.
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| CN201310275746.9A CN103409007B (en) | 2013-07-03 | 2013-07-03 | A kind of ageing-resistant interior wall coating and preparation method thereof |
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| CN201310275746.9A CN103409007B (en) | 2013-07-03 | 2013-07-03 | A kind of ageing-resistant interior wall coating and preparation method thereof |
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| CN103409007A CN103409007A (en) | 2013-11-27 |
| CN103409007B true CN103409007B (en) | 2016-04-06 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105504929A (en) * | 2015-12-31 | 2016-04-20 | 文登蓝岛建筑工程有限公司 | Moisture-proof paint and preparation method thereof |
| CN106366478A (en) * | 2016-08-30 | 2017-02-01 | 张德轩 | Environment-friendly water-based material for heat insulation and protection of wall and preparation method thereof |
| CN107118649A (en) * | 2017-07-07 | 2017-09-01 | 佛山领新信息科技有限公司 | A kind of antibacterial and ageing-resistant interior wall coating and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1431260A (en) * | 2003-01-20 | 2003-07-23 | 湖南大学 | Multi-functional environmental protection type interior wall nano coating material and its preparing method |
| CN1435458A (en) * | 2002-01-28 | 2003-08-13 | 天津城市建设学院 | Nanopaint |
| KR20040099010A (en) * | 2003-05-17 | 2004-11-26 | 조광페인트주식회사 | Making process of water paint for architecture |
| CN1637082A (en) * | 2004-12-09 | 2005-07-13 | 中山大学 | Nanometer inorganic powder modified water emulsion wall paint and its prepn |
| CN102533032A (en) * | 2010-12-10 | 2012-07-04 | 深圳市嘉达高科产业发展有限公司 | Automatic indoor humidity adjusting coating |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1435458A (en) * | 2002-01-28 | 2003-08-13 | 天津城市建设学院 | Nanopaint |
| CN1431260A (en) * | 2003-01-20 | 2003-07-23 | 湖南大学 | Multi-functional environmental protection type interior wall nano coating material and its preparing method |
| KR20040099010A (en) * | 2003-05-17 | 2004-11-26 | 조광페인트주식회사 | Making process of water paint for architecture |
| CN1637082A (en) * | 2004-12-09 | 2005-07-13 | 中山大学 | Nanometer inorganic powder modified water emulsion wall paint and its prepn |
| CN102533032A (en) * | 2010-12-10 | 2012-07-04 | 深圳市嘉达高科产业发展有限公司 | Automatic indoor humidity adjusting coating |
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Denomination of invention: A kind of anti-aging interior wall paint and preparation method thereof Effective date of registration: 20220801 Granted publication date: 20160406 Pledgee: Xinhe Sub-branch of Anhui Qingyang Rural Commercial Bank Co., Ltd. Pledgor: ANHUI ZHENXIN PAINT Co.,Ltd. Registration number: Y2022980011723 |