CN103360891B - 一种胶黏剂涂料的制备方法 - Google Patents
一种胶黏剂涂料的制备方法 Download PDFInfo
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- CN103360891B CN103360891B CN201310316441.8A CN201310316441A CN103360891B CN 103360891 B CN103360891 B CN 103360891B CN 201310316441 A CN201310316441 A CN 201310316441A CN 103360891 B CN103360891 B CN 103360891B
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- adhesive coating
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- 230000001070 adhesive effect Effects 0.000 title claims abstract description 41
- 239000000853 adhesive Substances 0.000 title claims abstract description 40
- 239000011248 coating agent Substances 0.000 title claims abstract description 36
- 238000000576 coating method Methods 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 39
- 239000004814 polyurethane Substances 0.000 claims abstract description 36
- 229920002635 polyurethane Polymers 0.000 claims abstract description 36
- 239000002253 acid Substances 0.000 claims abstract description 27
- 239000004014 plasticizer Substances 0.000 claims abstract description 9
- 239000004611 light stabiliser Substances 0.000 claims abstract description 8
- 239000013008 thixotropic agent Substances 0.000 claims abstract description 7
- -1 flexibilizer Substances 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims description 42
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 36
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 32
- 239000005058 Isophorone diisocyanate Substances 0.000 claims description 28
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 claims description 28
- 239000000178 monomer Substances 0.000 claims description 23
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 22
- 239000011259 mixed solution Substances 0.000 claims description 21
- 239000000376 reactant Substances 0.000 claims description 18
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 17
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 16
- 238000002425 crystallisation Methods 0.000 claims description 16
- 230000008025 crystallization Effects 0.000 claims description 16
- 230000018044 dehydration Effects 0.000 claims description 16
- 238000006297 dehydration reaction Methods 0.000 claims description 16
- 229910052799 carbon Inorganic materials 0.000 claims description 15
- HXTCWLNZDIPLCA-UHFFFAOYSA-N dodecanoic acid;2-methylprop-2-enoic acid Chemical compound CC(=C)C(O)=O.CCCCCCCCCCCC(O)=O HXTCWLNZDIPLCA-UHFFFAOYSA-N 0.000 claims description 14
- 239000012046 mixed solvent Substances 0.000 claims description 14
- 238000010792 warming Methods 0.000 claims description 13
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 12
- KQNPFQTWMSNSAP-UHFFFAOYSA-N alpha-isobutyric acid Natural products CC(C)C(O)=O KQNPFQTWMSNSAP-UHFFFAOYSA-N 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 11
- 235000013312 flour Nutrition 0.000 claims description 11
- 239000000377 silicon dioxide Substances 0.000 claims description 11
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 claims description 10
- 239000012965 benzophenone Substances 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 9
- 239000002904 solvent Substances 0.000 claims description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- 229920000459 Nitrile rubber Polymers 0.000 claims description 8
- 150000001298 alcohols Chemical class 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 238000012360 testing method Methods 0.000 claims description 8
- 230000015572 biosynthetic process Effects 0.000 claims description 7
- 238000003786 synthesis reaction Methods 0.000 claims description 7
- 230000002194 synthesizing effect Effects 0.000 claims description 7
- VOZRXNHHFUQHIL-UHFFFAOYSA-N glycidyl methacrylate Chemical compound CC(=C)C(=O)OCC1CO1 VOZRXNHHFUQHIL-UHFFFAOYSA-N 0.000 claims description 6
- OJURWUUOVGOHJZ-UHFFFAOYSA-N methyl 2-[(2-acetyloxyphenyl)methyl-[2-[(2-acetyloxyphenyl)methyl-(2-methoxy-2-oxoethyl)amino]ethyl]amino]acetate Chemical compound C=1C=CC=C(OC(C)=O)C=1CN(CC(=O)OC)CCN(CC(=O)OC)CC1=CC=CC=C1OC(C)=O OJURWUUOVGOHJZ-UHFFFAOYSA-N 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 4
- 229920005989 resin Polymers 0.000 claims description 4
- 239000011347 resin Substances 0.000 claims description 4
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 claims description 3
- 125000004494 ethyl ester group Chemical group 0.000 claims description 3
- 150000005605 isobutyric acids Chemical class 0.000 claims description 3
- 150000004702 methyl esters Chemical class 0.000 claims description 3
- 230000009974 thixotropic effect Effects 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 abstract description 7
- 239000004033 plastic Substances 0.000 abstract description 7
- 150000007513 acids Chemical class 0.000 abstract description 4
- 230000032683 aging Effects 0.000 abstract description 3
- 238000005520 cutting process Methods 0.000 abstract description 3
- 239000000945 filler Substances 0.000 abstract description 3
- 238000004383 yellowing Methods 0.000 abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 17
- 238000003756 stirring Methods 0.000 description 11
- 150000002576 ketones Chemical class 0.000 description 10
- 239000003054 catalyst Substances 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000004821 distillation Methods 0.000 description 5
- 230000001105 regulatory effect Effects 0.000 description 5
- 230000004044 response Effects 0.000 description 5
- RPQRDASANLAFCM-UHFFFAOYSA-N oxiran-2-ylmethyl prop-2-enoate Chemical compound C=CC(=O)OCC1CO1 RPQRDASANLAFCM-UHFFFAOYSA-N 0.000 description 4
- 229920001971 elastomer Polymers 0.000 description 3
- 125000002462 isocyano group Chemical group *[N+]#[C-] 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- XNGIFLGASWRNHJ-UHFFFAOYSA-L phthalate(2-) Chemical compound [O-]C(=O)C1=CC=CC=C1C([O-])=O XNGIFLGASWRNHJ-UHFFFAOYSA-L 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 241000219146 Gossypium Species 0.000 description 1
- 230000006750 UV protection Effects 0.000 description 1
- 125000000751 azo group Chemical group [*]N=N[*] 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 229920006332 epoxy adhesive Polymers 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Polyurethanes Or Polyureas (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
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CN201310316441.8A CN103360891B (zh) | 2013-07-25 | 2013-07-25 | 一种胶黏剂涂料的制备方法 |
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CN201310316441.8A CN103360891B (zh) | 2013-07-25 | 2013-07-25 | 一种胶黏剂涂料的制备方法 |
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CN103360891A CN103360891A (zh) | 2013-10-23 |
CN103360891B true CN103360891B (zh) | 2016-05-11 |
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103709975B (zh) * | 2013-11-29 | 2016-07-06 | 中国科学院长春应用化学研究所 | 用于复合氟塑料薄膜的聚氨酯胶粘剂及其制备方法 |
CN104327784B (zh) * | 2014-11-02 | 2016-08-24 | 吉林省电力科学研究院有限公司 | 多组份高弹性凝汽器密封胶 |
CN110172264A (zh) * | 2019-05-25 | 2019-08-27 | 北京点域科技有限公司 | 一种耐高温型油性涂料的制备方法 |
CN110964323A (zh) * | 2019-10-30 | 2020-04-07 | 安徽康宁油脂科技有限公司 | 一种高性能工业复合甘油及其制备方法 |
CN111978870A (zh) * | 2020-09-03 | 2020-11-24 | 宿州洛通木业有限公司 | 一种红木家具用蜡膏及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101280156A (zh) * | 2007-10-15 | 2008-10-08 | 浙江传化股份有限公司 | 抗紫外聚氨酯丙烯酸酯水性涂层胶及其制备方法 |
CN101429407A (zh) * | 2008-12-08 | 2009-05-13 | 广州市科霖水性材料有限公司 | 水性聚氨酯丙烯酸复合涂层剂及其制备方法 |
CN101824152A (zh) * | 2010-04-13 | 2010-09-08 | 深圳职业技术学院 | 一种含双固化基团树脂的制备方法及其应用 |
CN101914360A (zh) * | 2010-08-11 | 2010-12-15 | 江苏中金玛泰医药包装有限公司 | 一种低温热封胶及其制备方法 |
-
2013
- 2013-07-25 CN CN201310316441.8A patent/CN103360891B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101280156A (zh) * | 2007-10-15 | 2008-10-08 | 浙江传化股份有限公司 | 抗紫外聚氨酯丙烯酸酯水性涂层胶及其制备方法 |
CN101429407A (zh) * | 2008-12-08 | 2009-05-13 | 广州市科霖水性材料有限公司 | 水性聚氨酯丙烯酸复合涂层剂及其制备方法 |
CN101824152A (zh) * | 2010-04-13 | 2010-09-08 | 深圳职业技术学院 | 一种含双固化基团树脂的制备方法及其应用 |
CN101914360A (zh) * | 2010-08-11 | 2010-12-15 | 江苏中金玛泰医药包装有限公司 | 一种低温热封胶及其制备方法 |
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Address after: 518132 Guangdong province Shenzhen Guangming Tianliao community Juhui Industrial Park 1 Applicant after: SHENZHEN SHENDA AURORA TECHNOLOGY Co.,Ltd. Address before: 518132 Guangdong province Shenzhen Guangming Tianliao Avenue Juhui Industrial Park 1 Applicant before: Reflective Materials Manufactory Company SZU |
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COR | Change of bibliographic data | ||
CB03 | Change of inventor or designer information |
Inventor after: Wang Xiaobing Inventor after: Liang Houhui Inventor after: Wang Leilei Inventor after: Li Jianbing Inventor after: Huang Yanyan Inventor before: Wang Xiaobing Inventor before: Zhang Aifeng Inventor before: Wang Leilei Inventor before: Li Jianbing Inventor before: Zhang Haiming |
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Address after: 518132 Building 1 and Building 3, 1st Floor, Tianliao Avenue Juhui Mold Industrial Park, Tianliao Community, Yutang Street, Guangming New District, Shenzhen City, Guangdong Province Patentee after: Shenzhen Shenda Aurora Technology Co.,Ltd. Address before: 518132 Building 1, Juhui Industrial Park, Tianliao community, Guangming New District, Shenzhen City, Guangdong Province Patentee before: SHENZHEN SHENDA AURORA TECHNOLOGY Co.,Ltd. |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method for adhesive coatings Effective date of registration: 20230706 Granted publication date: 20160511 Pledgee: Shenzhen small and medium sized small loan Co.,Ltd. Pledgor: Shenzhen Shenda Aurora Technology Co.,Ltd. Registration number: Y2023980047584 |
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