CN101928202B - 一种高纯度3-氯-1,2-丙二醇的生产方法 - Google Patents
一种高纯度3-氯-1,2-丙二醇的生产方法 Download PDFInfo
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- CN101928202B CN101928202B CN201010011544XA CN201010011544A CN101928202B CN 101928202 B CN101928202 B CN 101928202B CN 201010011544X A CN201010011544X A CN 201010011544XA CN 201010011544 A CN201010011544 A CN 201010011544A CN 101928202 B CN101928202 B CN 101928202B
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Abstract
Description
序号 | 检测指标 | 分析方法 | 检测结果 |
1 | 外观 | 目测 | 无色透明液体 |
2 | 氯代甘油含量(GC)(%) | 企业标准Q/WZY009-2009 | 99.86 |
3 | 低沸物含量(GC)(%) | 企业标准Q/WZY009-2009 | 0.11 |
4 | 高沸物含量(GC)(%) | 企业标准Q/WZY009-2009 | 0.03 |
4 | 水分(wt%) | 卡尔·费休法 | 0.35 |
序号 | 检测指标 | 分析方法 | 检测结果 |
1 | 外观 | 目测 | 无色透明液体 |
2 | 氯代甘油含量(GC)(%) | 企业标准Q/WZY009-2009 | 99.82 |
3 | 低沸物含量(GC)(%) | 企业标准Q/WZY009-2009 | 0.17 |
4 | 高沸物含量(GC)(%) | 企业标准Q/WZY009-2009 | 0.01 |
4 | 水分(wt%) | 卡尔·费休法 | 0.41 |
序号 | 检测指标 | 分析方法 | 检测结果 |
1 | 外观 | 目测 | 无色透明液体 |
2 | 氯代甘油含量(GC)(%) | 企业标准Q/WZY009-2009 | 99.85 |
3 | 低沸物含量(GC)(%) | 企业标准Q/WZY009-2009 | 0.15 |
4 | 高沸物含量(GC)(%) | 企业标准Q/WZY009-2009 | 未检出 |
4 | 水分(wt%) | 卡尔·费休法 | 0.47 |
Claims (8)
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CN101928202A CN101928202A (zh) | 2010-12-29 |
CN101928202B true CN101928202B (zh) | 2012-11-14 |
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Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102229523B (zh) * | 2011-05-25 | 2013-07-31 | 郭学阳 | 一种3-氯-1,2-丙二醇的制备方法 |
CN102786561A (zh) * | 2012-08-02 | 2012-11-21 | 中国石油化工股份有限公司 | 一种钻井液用阳离子烷基糖苷的制备方法 |
CN104557848A (zh) * | 2015-01-09 | 2015-04-29 | 山东师范大学 | 氟代碳酸丙烯酯的制备方法 |
CN104892365B (zh) * | 2015-05-27 | 2017-06-27 | 泰山医学院 | 一种低压合成高纯度氯代甘油的方法 |
CN107176903B (zh) * | 2017-06-27 | 2020-12-11 | 江苏合泰新材料科技有限公司 | 一种合成3-氯-1,2-丙二醇的方法 |
CN109336735A (zh) * | 2018-11-29 | 2019-02-15 | 湖北阿泰克生物科技股份有限公司 | 一种采用微通道连续流反应器制备3-氯-1,2-丙二醇的方法 |
CN111170968B (zh) * | 2020-01-13 | 2020-10-27 | 北京笃敬科技有限公司 | 一种制备四氢呋喃的***及方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101219961A (zh) * | 2008-01-24 | 2008-07-16 | 浙江理工大学 | 一种(s)-托利洛尔的合成方法 |
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CN101219961A (zh) * | 2008-01-24 | 2008-07-16 | 浙江理工大学 | 一种(s)-托利洛尔的合成方法 |
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Owner name: QINGDAO ZHONGKE RONGDA NEW MATERIAL CO., LTD. Free format text: FORMER OWNER: ZHANG ZHONGFA Effective date: 20120920 |
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Inventor after: Guo Xiangrong Inventor after: Zhuang Qing Inventor after: Wang Cui Inventor after: Guo Yankai Inventor after: Li Cuandong Inventor after: Zhang Yunling Inventor after: Wang Xiaoli Inventor after: Guo Xueyang Inventor before: Zhang Zhongfa Inventor before: Guo Xueyang Inventor before: Ding Aimei Inventor before: Huang Hui Inventor before: Lv Cailing Inventor before: Zhang Qingguo Inventor before: Wei Lihua |
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Free format text: CORRECT: ADDRESS; FROM: 262737 WEIFANG, SHANDONG PROVINCE TO: 266600 QINGDAO, SHANDONG PROVINCE Free format text: CORRECT: INVENTOR; FROM: ZHANG ZHONGFA GUO XUEYANG DING AIMEI HUANG HUI LV CAILING ZHANG QINGGUO WEI LIHUA TO: GUO XIANGRONG ZHUANG QING WANG CUI GUO YANKAI LI XINDONG ZHANG YUNLING WANG XIAOLI GUO XUEYANG |
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