CN101283964A - No-ethanol essence aquose dispersion system - Google Patents
No-ethanol essence aquose dispersion system Download PDFInfo
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- CN101283964A CN101283964A CNA2008100619162A CN200810061916A CN101283964A CN 101283964 A CN101283964 A CN 101283964A CN A2008100619162 A CNA2008100619162 A CN A2008100619162A CN 200810061916 A CN200810061916 A CN 200810061916A CN 101283964 A CN101283964 A CN 101283964A
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Abstract
The invention relates to an ethanol-free essence waterborne dispersion system, particularly to perfume, body spraying agent, deodorant, waterborne cosmetic composition, domestic detergent and air freshener. The essence waterborne dispersion system comprises the following component of (wt%): aroma materials 0.1-0.6%, phase dispersant 1-60%, and water 10-95%, wherein the aroma materials, phase dispersant and water form a low molecular weight dispersion system or a colloidal dispersion system. The dispersion system uses water as basic medium, the properly added phase dispersant (with high boiling point and slow evaporation) takes both cosolvent and stabilizer effects, so that the products can keep scent for a longer time. In addition, the products are normally not greasy and sticky, and the phase dispersant may not influence the quality of aroma materials and is not sensitive to air oxidation, so as to keep the natural color of perfume.
Description
Technical field
The present invention relates to a kind of essence aquose dispersion system, relate in particular to perfume, the agent of spray health, remove body odor agent, aqueous cosmetic composition, household cleaners and air freshener.
Background technology
The method that tradition perfume is made is by being solvent with ethanol, and mixing various Oleum sesami essences becomes a kind of uniform and stable solution, i.e. perfume.Because at the initial stage that perfume is made, the chemical industry technology and unlike today so flourishing, so the perfume teachers have selected this chemical solvent that comparatively is easy to get of ethanol.The ethanol boiling point is low, high volatility (and current tendency is to reduce the use that volatile organic is learned product (VOC)), and can dissolve most of organic quintessence oil, can also play certain preservation, a kind of really good solvent, yet itself has acid ethanol, even after the expensive redistillation technology of experience, the taste of self still can be mixed in the fragrance of Oleum sesami essence, usually the quality to this life of perfume damages, and also is the difficult problem that the perfume teachers must face when allotment perfume.The ethanol easy firing also causes the danger to a certain degree of perfume production and this life of perfume in addition.In addition, contain pure cosmetics because a variety of causes such as cutaneous sensibility, baby safe and forbid it being unacceptable for the religion that some users' ethanol uses.
Up to now, ethanol-free aqueous perfume composition has certain release, comprise one or more aroma materials, solvent, aqueous medium and randomly, one or more surfactants as the open said composition of Chinese invention patent application (publication number is CN1964691A); Wherein the solvent in the microemulsion be the vicinal glycol as 1, the 2-hexanediol.But there is following shortcoming in they: or outward appearance is emulsion, influenced the traditional visual effect of perfume; Or need the surfactant of high concentration, because the viscosity essence of surfactant makes product viscosity increase, be not useful especially to health yet; Perhaps, influenced the olfactory sensation characteristic because the attack essence of the zest of solubilizing agent essence and surfactant stimulates product to a certain extent; Or replace ethanol as solvent or solubilizing agent with other alcohol compounds, obscured the original intention of alcohol-free perfume with the title of no ethanol perfume.
Summary of the invention
In order to solve the technical problem that above-mentioned spirituosity class perfume exists, the purpose of this invention is to provide a kind of essence aquose dispersion system, this dispersion need not to add under the situation of any surfactant, still can provide effectively, the characteristic of optically clear, non-greasy, non-sticky fragrance microemulsion.
In order to realize above-mentioned purpose, the present invention has adopted following technical scheme:
No-ethanol essence aquose dispersion system, this essence aquose dispersion system comprise following component by weight percentage: aroma materials 0.1～60%; Phase dispersant 1～60%; Water 10～95%; Above-mentioned aroma materials, phase dispersant, water form low molecular dispersion system or colloidal dispersion.
Low molecule of the present invention (or ion) disperse system (the linear size of its particle is below 1nm); Colloidal dispersion (the linear size of its particle is between 1-100nm).Phase dispersant of the present invention is the disappearance of practising physiognomy that can make water and organic facies, forms the blended system of homogeneous.The difference of phase dispersant and surfactant is, surfactant is not energy dissolve flavor material (being the material in the organic facies) but inserts organic facies with its hydrophobic group, and its hydrophilic radical covers outside it, formed from several microns (sometimes or even several millimeters) to the micelle group between the hundreds of nanometer, also can form transparent mixture from macroscopic view, but from microcosmic, this is the system under a kind of metastable condition.In addition, aroma materials is covered by a large amount of surfactants, can not really disperse uniformly, on the angle of technology, also is unfavorable for flavor molecule performance effect.And the phase dispersant itself that this patent adopts just can dissolve the aroma materials of fat-soluble compound, so the mixed system major part of formed final stable homogeneous is a solution, even the hydrosol that under the situation that the high concentration aroma materials exists, forms, it also is molecular colloid, there is not micelle, therefore can itself do not influence to some extent aroma materials (flavor molecule).
As preferably, above-mentioned essence aquose dispersion system comprises following component by weight percentage: aroma materials 1～30%; Phase dispersant 1～35%; Water 55～90%.
As preferably, above-mentioned phase dispersant is dimethyl sulfoxide, N-Methyl pyrrolidone or 1, the 4-diox.As most preferably, above-mentioned phase dispersant is a dimethyl sulfoxide.
Dimethyl sulfoxide is the organic solvent of using always, and it can dissolve most Organic substance, comprises carbohydrate, polymer, peptide and a lot of inorganic matter and gas.It can dissolve the solute (common solvent is only with dissolving 10-20%) that is equal to own 50-60% weight, so it is very important in sample management and high velocity medicament screening now, is employed widely and medical chemistry and biochemical field.Ao Legang university can deeply permeate with the discovery dimethyl sulfoxide of the medical college team headed by the Stanley Jacob but not destroy skin and other epithelium, and other material of portability gos deep in the biosystem.Pharmaceutically, main local analgesia agent, topical remedy's carrier, antibiotic medicine and the antioxidant of being used for of dimethyl sulfoxide.The toxicologic study of dimethyl sulfoxide indicates that (FDA) this organic compound is all harmless substantially to human body and most of animal, and human body is had certain pharmacological action.Under the application requirements of this patent, the side effect of the content of dimethyl sulfoxide in product is very also low than ethanol, be those ions or non-ionic surface active agent in the relevant patent, or various alcohols solubilizing agent is incomparable.Dimethyl sulfoxide relies on self powerful dissolving dispersibility, makes this perfuming waterborne compositions need not just to form homogeneous under the situation of any surfactant, the decentralized photo of stable (comprising Thermodynamically stable).In addition, because the high boiling point and the permeability of dimethyl sulfoxide, by the perfume fragrance of this patent explained hereafter fragrance unlike traditional ethanol perfume dense for the moment but die loose very fast, this perfume fragrance is deep and remote light and of long standing and well established, vitality is of a specified duration, allows the user better savour the charming effect of perfume, experiences the disperse state of nature fragrance matter, even perfume spray smear the place with water wash after, fragrance can not disappear rapidly yet.
Certainly for N-Methyl pyrrolidone or 1, the 4-diox relies on they self powerful dissolving dispersibility, and this perfuming waterborne compositions need not under the situation of any surfactant, just can form homogeneous, the decentralized photo of stable (comprising Thermodynamically stable).Its shortcoming is to be that skin is had slight stimulation.
The composition of above-mentioned phase dispersant decide on the character of concrete aroma materials and metering percentage ratio, is generally between 1%～60%, and is preferably about 1%～35%, more preferably between 5%～25%, is most preferably between 8%～15%.
Aroma materials of the present invention can adopt one or more in fat-soluble Oleum sesami essence, the water solublity Oleum sesami essence.For fat-soluble Oleum sesami essence, phase dispersant of the present invention can make fat-soluble Oleum sesami essence be dissolved in aqueous phase, and for water solublity Oleum sesami essence, phase dispersant of the present invention can make water-based system more stable, prevents separating out of Oleum sesami essence.Therefore, aroma materials is a kind of or fat-soluble Oleum sesami essence and the smart mixture of water solublity Oleum sesami that can adopt in fat-soluble Oleum sesami essence, the water solublity Oleum sesami essence.Aroma materials is between 0.1～60% by weight percentage, and is preferred about 1%～50%, more preferably between 1%～30%, is most preferably between 1%～20%.
Aroma materials of the present invention is selected natural flavor raw material (this patent definitely is applicable to the production of the perfume or the Related product of synthetic perfume certainly) for use, and interested especially is fat-soluble Oleum sesami essence, as orange oil, and Oleum menthae, eucalyptus oil, Fructus Citri Limoniae oil, Folium Caryophylli oil, Olibanum oil, cedarwood oil, bergmot oil, Pu Luowangsi Essential lavender oil, Flos Matricariae chamomillae oil, Jasmin oil, Oleum Rosae Rugosae, Oleum Anisi Stellati, thyme oil, Oleum Camphora, black (in vain) oil of pepper, chilli oil ， geranium wilfordii oil, Moschus, castoreum, zibet perfume (or spice), Ambergris or the like.
As preferably, no-ethanol essence aquose dispersion system of the present invention also comprises one or more optional members such as antioxidant (natural antioxidant, vitamin E, tea polyphenols, rosmarinic acid, synthetic antioxidant, four (β-(3, the 5-di-tert-butyl-hydroxy phenyl) propanoic acid) pentaerythritol ester, ditertbutylparacresol), intercalating agent (sodium citrate, edetate), UV filtering agent (benzophenone-4) and antiseptic (benzoic acid fat).Other composition such as thickening agent (hydroxypropyl emthylcellulose, methyl glucoside trioleate etc.), cosmetic active ingredient, humidizer, wetting agent, lubricant, opacifier, Margarita is like gloss shock resistance material, and coloring agent and defoamer also can be included in the dispersion system of the present invention.
The content of water of the present invention is generally between 10%～95%, and is preferred about 55%～90%, more preferably between 60%～85%.No-ethanol essence aquose dispersion system of the present invention can mix by manual or motor device and form.Aromatic, perfume, the body odor agent is gone in the agent of spray health, aqueous cosmetic composition, household cleaners and air freshener all can benefit from this patent.
The present invention is the basic medium of dispersion with water, replaces traditional ethanol, makes product really become green product, has removed alcoholic acid assorted flavor, and the taste of this life of reduction aroma materials makes new generation product more charming.Yet in order to overcome the intersolubility of water and aroma materials, add suitable phase dispersant, both played the effect of cosolvent, function of stabilizer (high boiling point, slow vaporization) had been arranged again, make the fragrant time of product tape more permanent, and product is non-greasy and non-sticky normally, and the phase dispersant does not cause the influence of quality to fragrance matter, also, can keep the natural colour of perfume not to the air oxidation sensitivity.Simultaneously, the present invention can also introduce more poor solubility in ethanol and can be dissolved in the novel substance of solvent of new generation, for choosing of Oleum sesami essence opened bigger gate greatly.
The specific embodiment
Embodiment 1
Oleum sesami essence: snow pinke needle oil Fichtennadel (place of production, Siberia)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
44.44% snow pinke needle oil (20 microlitre)
44.44% dimethyl sulfoxide (20 microlitre)
11.11% high purity water (5 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be the high concentration essence product.
Embodiment 2
Oleum sesami essence: snow pinke needle oil Fichtennadel (place of production, Siberia)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
5.71% snow pinke needle oil (20 microlitre)
51.43% dimethyl sulfoxide (180 microlitre)
42.86% high purity water (150 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be GULONG water (the Eau de Cologn) product of low essence concentration.
Embodiment 3
The smart: geranium wilfordii oil of Oleum sesami Geranium (place of production, China)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
25% geranium wilfordii oil (10 microlitre)
50% dimethyl sulfoxide (20 microlitre)
25% high purity water (10 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be perfume (Parfum) product of higher concentration.
Embodiment 4
The smart: geranium wilfordii oil of Oleum sesami Geranium (place of production, China)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
5.88% geranium wilfordii oil (10 microlitre)
35.29% dimethyl sulfoxide (60 microlitre)
58.52% high purity water (100 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be GULONG water (the Eau de Cologn) product of low essence concentration.
Embodiment 5
Oleum sesami essence: Oleum Camphora Camphor (place of production, China)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
18.18% Oleum Camphora (20 microlitre)
36.36% dimethyl sulfoxide (40 microlitre)
45.45% high purity water (50 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be popular on the market perfume (Eau de Parfum) product.
Embodiment 6
Oleum sesami essence: Oleum Camphora Camphor (place of production, China)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
8.54% Oleum Camphora (7 microlitre)
48.78% dimethyl sulfoxide (40 microlitre)
42.68% high purity water (35 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be the lower light perfume of essence concentration (Eau de Toilette) product.
Embodiment 7
Oleum sesami essence: Oleum Camphora Camphor (place of production, China)
Reddish orange oil Mandarine Rot (place of production, Spain)
Geranium wilfordii oil Geranium (place of production, China)
Snow pinke needle oil Fichtennadel (place of production, Siberia)
Illawarra mountain pine oil Fichtennadel (place of production, Balkan)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
5.26% reddish orange oil (10 microlitre)
2.63% Oleum Camphora (5 microlitre)
3.95% snow pinke needle oil (7.5 microlitre)
1.32% illawarra mountain pine oil (2.5 microlitre)
2.63% geranium wilfordii oil (5 microlitre)
68.4% dimethyl sulfoxide (130 microlitre)
15.8% high purity water (30 microlitre)
Gentle agitation or concussion at room temperature obtains the mixed solution of lemon yellow homogeneous, is the perfume (Eau de Parfum) of a east charm (oriental) type.
Embodiment 8
The smart: geranium wilfordii oil of Oleum sesami Geranium (place of production, China)
The phase dispersant: N-Methyl pyrrolidone NMP (99% is pure: Acros chemical drugs company)
Aqueous medium: high purity water, millipore water,
25% geranium wilfordii oil (10 microlitre)
50%N-methyl pyrrolidone (20 microlitre)
25% high purity water (10 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be perfume (Parfum) product of higher concentration.
Embodiment 9
Oleum sesami essence: Oleum Camphora Camphor (place of production, China)
The phase dispersant: N-Methyl pyrrolidone NMP (99% is pure: Acros chemical drugs company)
Aqueous medium: high purity water, millipore water,
19.05% Oleum Camphora (20 microlitre)
33.33%N-methyl pyrrolidone (35 microlitre)
47.62% high purity water (50 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be popular on the market perfume (Eau de Parfum) product.
Embodiment 10
Oleum sesami essence: snow pinke needle oil Fichtennadel (place of production, Siberia)
The phase dispersant: 1,4-diox, 1,4-Dioxane (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
11.11% snow pinke needle oil (5 microlitre)
44.44%1,4-diox (20 microlitre)
44.44% high purity water (20 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be the lower light perfume of essence concentration (Eau de Toilette) product.
Embodiment 11
The smart: geranium wilfordii oil of Oleum sesami Geranium (place of production, China)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
UV-filtering agent: benzophenone-4 (99% is pure, Aldrich chemical drugs company)
Antiseptic: benzoic acid isopropyl ester (99% is pure, Aldrich chemical drugs company)
25% geranium wilfordii oil (100 microlitre)
50% dimethyl sulfoxide (200 microlitre)
24.4% high purity water (97.6 microlitre)
0.5% benzophenone-4 (2 milligrams)
0.1% benzoic acid, third fat (0.4 milligram)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be perfume (Parfum) product of higher concentration.
Embodiment 12
The smart: geranium wilfordii oil of Oleum sesami Geranium (place of production, China)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
Antioxidant: vitamin E (99% is pure, Aldrich chemical drugs company)
Antiseptic: benzoic acid third fat (99% is pure, Aldrich chemical drugs company)
25% geranium wilfordii oil (100 microlitre)
50% dimethyl sulfoxide (200 microlitre)
24.8% high purity water (99.2 microlitre)
0.1% vitamin E (0.4 milligram)
0.1% benzoic acid isopropyl ester (0.4 milligram)
Gentle agitation or concussion at room temperature obtains the mixture of colourless homogeneous, and this product can be perfume (Parfum) product of higher concentration.
Embodiment 13
The smart: geranium wilfordii oil of Oleum sesami Geranium (place of production, China)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
Antioxidant: rosmarinic acid Ros A (99% is pure, Aldrich chemical drugs company)
Antiseptic: benzoic acid third fat (99% is pure, Aldrich chemical drugs company)
Intercalating agent: sodium citrate (99% is pure, Aldrich chemical drugs company)
25% geranium wilfordii oil (100 microlitre)
50% dimethyl sulfoxide (200 microlitre)
24.75% high purity water (99 microlitre)
0.1% rosmarinic acid (0.4 milligram)
0.1% benzoic acid, third fat (0.4 milligram)
0.05% sodium citrate (0.2 milligram)
Gentle agitation or concussion at room temperature obtains the mixture of utmost point lavender transparent and homogeneous, and this product can be perfume (Parfum) product of higher concentration.
Embodiment 14
Oleum sesami essence: the smart Lavender oil (place of production, Spain) of Garden lavender Oleum sesami
Coumarin Coumarin (99% is pure, Sigma biotechnology drug company)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
Other work efficiency compositions: glycerol (99.5% is pure, Aldrich chemical drugs company)
Formalin (37% is pure, Aldrich chemical drugs company)
1% Garden lavender Oleum sesami essence (1 microlitre)
1% coumarin (1 milligram)
35% dimethyl sulfoxide (35 microlitre)
55% high purity water (55 microlitre)
5% glycerol (5 microlitre)
3% formaldehyde (3 microlitre)
Gentle agitation or concussion at room temperature obtains the mixture of transparent and homogeneous, and this product can be alcohol-free deodorant used in shoes agent, does not injure leather and skin.
Embodiment 15
Oleum sesami essence: NINGMENGXIANG olein (place of production, China)
Phase dispersant: dimethyl sulfoxide DMSO (99% is pure, Aldrich chemical drugs company)
Aqueous medium: high purity water, millipore water,
Other functional components: Punica granatum L. shell water extract
The licorice water extract
0.1% NINGMENGXIANG olein (1 microlitre)
12% dimethyl sulfoxide (120 microlitre)
41.9% high purity water (420 microlitre)
40% Punica granatum L. shell water extract (400 milligrams)
6% licorice water extract (60 milligrams)
Gentle agitation or concussion at room temperature obtains the mixture of transparent and homogeneous, and this product can be antozostomatic, the making good use of of deodorization and antiinflammatory.
Claims (10)
1. no-ethanol essence aquose dispersion system, it is characterized in that: this essence aquose dispersion system comprises following component by weight percentage:
Aroma materials 0.1～60%;
Phase dispersant 1～60%;
Water 10～95%;
Above-mentioned aroma materials, phase dispersant, water form low molecular dispersion system or colloidal dispersion.
2. no-ethanol essence aquose dispersion system according to claim 1 is characterized in that: this essence aquose dispersion system comprises following component by weight percentage:
Aroma materials 1～30%;
Phase dispersant 1～35%;
Water 55～90%.
3. no-ethanol essence aquose dispersion system according to claim 1 and 2 is characterized in that: the phase dispersant is dimethyl sulfoxide, N-Methyl pyrrolidone or 1, the 4-diox.
4. no-ethanol essence aquose dispersion system according to claim 3 is characterized in that: the phase dispersant is a dimethyl sulfoxide.
5. no-ethanol essence aquose dispersion system according to claim 1 and 2 is characterized in that: the phase dispersant is 5%～25% by weight percentage.
6. no-ethanol essence aquose dispersion system according to claim 5 is characterized in that: the phase dispersant is 8%～15% by weight percentage.
7. no-ethanol essence aquose dispersion system according to claim 1 and 2 is characterized in that: water is 60%～85% by weight percentage.
8. no-ethanol essence aquose dispersion system according to claim 1 and 2 is characterized in that: aroma materials adopts one or more in fat-soluble Oleum sesami essence, the water solublity Oleum sesami essence.
9. no-ethanol essence aquose dispersion system according to claim 8 is characterized in that: aroma materials is selected in orange oil, Oleum menthae, eucalyptus oil, Fructus Citri Limoniae oil, Folium Caryophylli oil, Olibanum oil, cedarwood oil, bergmot oil, Pu Luowangsi Essential lavender oil, Flos Matricariae chamomillae oil, Jasmin oil, Oleum Rosae Rugosae, Oleum Anisi Stellati, thyme oil, Oleum Camphora, Fructus piperis nigrum oil, Radix orixae japonicae oil, chilli oil, Herba Erodii oil, Moschus, castoreum, zibet perfume (or spice) and the Ambergris one or more for use.
10. no-ethanol essence aquose dispersion system according to claim 1 and 2 is characterized in that: this flavor compositions also comprises one or more in antioxidant, intercalating agent, UV filtering agent, antiseptic, the thickening agent.
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| CNA2008100619162A CN101283964A (en) | 2008-05-27 | 2008-05-27 | No-ethanol essence aquose dispersion system |
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| CNA2008100619162A CN101283964A (en) | 2008-05-27 | 2008-05-27 | No-ethanol essence aquose dispersion system |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102178965A (en) * | 2011-05-04 | 2011-09-14 | 云南同方科技有限公司 | Plant essential oil air-purifying agent and preparation method thereof |
| CN102639155A (en) * | 2009-12-02 | 2012-08-15 | 弗门尼舍有限公司 | Self-adhesive fragranced gels |
| CN103565716A (en) * | 2013-10-28 | 2014-02-12 | 义乌市庆鹏化妆品有限公司 | Natural castoreum containing perfume |
| CN103565715A (en) * | 2013-10-28 | 2014-02-12 | 义乌市庆鹏化妆品有限公司 | Natural civet containing perfume |
| CN103565718A (en) * | 2013-10-28 | 2014-02-12 | 义乌市庆鹏化妆品有限公司 | Perfume |
| CN109223608A (en) * | 2018-11-29 | 2019-01-18 | 四川省中医药科学院 | A kind of high speed homogenization forces solubilization method and its application |
| CN115251451A (en) * | 2022-08-24 | 2022-11-01 | 深圳市恒云生物科技有限公司 | Electronic atomized liquid and preparation method thereof |
-
2008
- 2008-05-27 CN CNA2008100619162A patent/CN101283964A/en active Pending
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102639155A (en) * | 2009-12-02 | 2012-08-15 | 弗门尼舍有限公司 | Self-adhesive fragranced gels |
| CN102639155B (en) * | 2009-12-02 | 2014-12-17 | 弗门尼舍有限公司 | Self-adhesive fragranced gels |
| CN102178965A (en) * | 2011-05-04 | 2011-09-14 | 云南同方科技有限公司 | Plant essential oil air-purifying agent and preparation method thereof |
| CN103565716A (en) * | 2013-10-28 | 2014-02-12 | 义乌市庆鹏化妆品有限公司 | Natural castoreum containing perfume |
| CN103565715A (en) * | 2013-10-28 | 2014-02-12 | 义乌市庆鹏化妆品有限公司 | Natural civet containing perfume |
| CN103565718A (en) * | 2013-10-28 | 2014-02-12 | 义乌市庆鹏化妆品有限公司 | Perfume |
| CN103565718B (en) * | 2013-10-28 | 2015-06-10 | 义乌市庆鹏化妆品有限公司 | Perfume |
| CN103565715B (en) * | 2013-10-28 | 2015-11-18 | 义乌市庆鹏化妆品有限公司 | A kind of perfume containing natural civet |
| CN109223608A (en) * | 2018-11-29 | 2019-01-18 | 四川省中医药科学院 | A kind of high speed homogenization forces solubilization method and its application |
| CN109223608B (en) * | 2018-11-29 | 2022-02-01 | 四川省中医药科学院 | High-speed homogeneous forced solubilization method and application thereof |
| CN115251451A (en) * | 2022-08-24 | 2022-11-01 | 深圳市恒云生物科技有限公司 | Electronic atomized liquid and preparation method thereof |
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