CN103054756A - Ethanol-free perfume - Google Patents
Ethanol-free perfume Download PDFInfo
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- CN103054756A CN103054756A CN2012105872271A CN201210587227A CN103054756A CN 103054756 A CN103054756 A CN 103054756A CN 2012105872271 A CN2012105872271 A CN 2012105872271A CN 201210587227 A CN201210587227 A CN 201210587227A CN 103054756 A CN103054756 A CN 103054756A
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- perfume
- dipropylene glycol
- ethanol
- bht
- peg
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Abstract
The invention relates to an ethanol-free perfume. The perfume comprises the following components in percentage by weight: 55-75% of dipropylene glycol methyl ether, 3-10% of butyl ether, 5-15% of dipropylene glycol, 0.5-5% of PEG-7 olive oil ester, 0.01-0.09% of benzophenone-3, 0.1% of BHT and the balance of deionized water. As a combined solvent including a group of ether derivatives replaces the ethanol as a solvent, the ethanol-free perfume provided by the invention is suitable for people allergic to alcohol to use and has the advantages of higher safety, longer aroma reserving effect and better compatibility with essence; and the problem that partial perfume is insoluble in the alcohol or the solubility of the partial perfume in the alcohol is limited is solved.
Description
Technical field
The present invention relates to a kind of perfume.
Background technology
Needed to use ethanol as solvent since long-term in perfume industry, such contains pure cosmetics because a variety of causes such as cutaneous sensibility, baby safe and some religion users are forbidden ethanol.
Therefore the perfume industrial quarters attempts developing without the ethanol perfume composition to satisfy user's demand.
Up to now, ethanol-free aqueous perfume composition, its outward appearance can be for from the outward appearance of emulsus to clarification, and the outward appearance of transparency liquid generally includes following component: the insoluble mixture of natural and/or synthetic perfume raw material in water; Ionic surface active agent and/or non-ionic surface active agent; The both sexes solubilizing agent is such as Polyethylene Glycol; Aqueous dispersion (normally water); And antiseptic.
Surfactant in the above compositions exists with high dose usually, and wishes the mixture of emulsifying or coupling aroma materials according to their content.
Above known have following shortcoming usually without the ethanol perfume composition: compositions is always not transparent; Because the viscosity of surfactant essence and because the application of the surfactant of relatively large number amount, so that compositions is viscosity; Easily rotten by solubilizing agent by the fragrance that the aroma materials that exists in the compositions is emitted; Compositions since the aggressivity essence of the zest of solubilizing agent essence and surfactant and be to a certain extent stimulation with compositions in the aroma materials that exists easily deteriorated by air oxidation, it adversely affects stability and the olfactory sensation characteristic of compositions.
Summary of the invention
For reaching above-mentioned purpose, the invention provides a kind of without ethanol perfume, combination solvent instead of ethanol with one group of ether derivative is used as solvent, being fit to the irritated crowd of ethanol uses, security performance is higher, aroma retaining effect is more permanent, better with the intermiscibility of essence, has solved part spice insoluble or problem that dissolubility is limited in ethanol.
Concrete technical scheme of the present invention is:
A kind of without ethanol perfume, it is characterized in that this perfume is made of following component by weight percentage:
Dipropylene glycol methyl ether 55 ~ 75%
Butyl ether 3 ~ 10%
Dipropylene glycol 5 ~ 15%
PEG-7 Fructus Canarii albi grease 0.5 ~ 5%
BP-3 0.01 ~ 0.09%
BHT 0.1%
Surplus is deionized water.
A prioritization scheme of the present invention is:
This perfume is made of following component by weight percentage:
Dipropylene glycol methyl ether 59 ~ 66%
Butyl ether 3.9 ~ 5.9%
Dipropylene glycol 9 ~ 11%
PEG-7 Fructus Canarii albi grease 0.9 ~ 3.9%
BP-3 0.03 ~ 0.06%
BHT 0.1%
Surplus is deionized water.
A prioritization scheme of the present invention is:
This perfume is made of following component by weight percentage:
Dipropylene glycol methyl ether 65%
Butyl ether 5%
Dipropylene glycol 10%
PEG-7 Fructus Canarii albi grease 2%
BP-3 0.05%
BHT 0.1%
Surplus is deionized water.
Obtain under this scheme without ethanol perfume, be optimum combination of the present invention, the solvent that the present invention adopts the special ratios of dipropylene glycol methyl ether, butyl ether and dipropylene glycol to mix as essence uses, have good intermiscibility and safety, have moderate evaporation rate, the faster then fragrance of volatilization is denseer, fragrance remaining time is shorter.
PEG-7 Fructus Canarii albi grease can reduce the zest of all the other components, suppresses the too fast volatilization of essence.
A kind of preparation method without ethanol perfume is characterized in that this preparation method is comprised of following steps;
Step 1 adds perfume to dipropylene glycol methyl ether, butyl ether and dipropylene glycol and makes pot, adds essence and stirs more than 5 minutes, to the abundant mix homogeneously of each component;
Step 2, with a container PEG-7 Fructus Canarii albi grease, BP-3 and BHT are mixed to fully dissolving after, add perfume and make in the pot, stir;
Step 3 added deionized water and stirring 5 minutes;
Step 4, sealing ageing after 24 hours room temperature filter and namely to get without ethanol perfume.
Described step 2, with PEG-7 Fructus Canarii albi grease, BP-3 and BHT mix and blend, wherein its whipping process is not higher than 50 ℃ heating simultaneously with a container, until fully dissolving.
Traditional ethanol perfume is assurance clarification free from admixture in manufacturing process, need Chen Hua 10 days and need to be in zubzero temperature freezing to remove the impurity of indissoluble, ether derivative combination of the present invention is better with the essence intermiscibility, can omit above-mentioned two steps, has greatly saved fabrication cycle and energy consumption.
PEG-7 Fructus Canarii albi grease
INCI Name：Olive Oil PEG 7 Esters
CAS No.： 103819-46-1
The skin moistening of olive oil and lubrication property can be promoted abundant texture, are highly suitable in shampoo, lotion and the personal care articles.
Have good lyotropy, be highly suitable for disperseing in the lotion oils and fats, spice and fat-soluble active component.
BHT English name: butylated hydroxytoluene
Chinese name: antioxidant 264
Chemical name: 2,6-di-tert-butyl-4-methy phenol or dibenzylatiooluene
Empirical formula: C15H24O
Molecular weight: 220.36(was by international relative atomic mass in 2007)
CAS: 128-37-0
BHT has another name called antioxidant BHT, by Bayer A.G invention, is widely used in industrial use, and wherein the German foreign cherry group BHT major part of producing is used on edible oil product printing ink and the rubber plastic industry.It also is the stabilizing agent of cosmetics, medicine etc.The addition of antioxidant BHT: 0.01%-2%.
The specific embodiment
Embodiment one
This perfume is made of following component by weight percentage:
Dipropylene glycol methyl ether 65%
Butyl ether 5%
Dipropylene glycol 10%
PEG-7 Fructus Canarii albi grease 2%
BP-3 0.05%
BHT 0.1%
Surplus is deionized water.
Obtain under this scheme without ethanol perfume, be optimum combination of the present invention, the solvent that the present invention adopts the special ratios of dipropylene glycol methyl ether, butyl ether and dipropylene glycol to mix as essence uses, have good intermiscibility and safety, have moderate evaporation rate, the faster then fragrance of volatilization is denseer, fragrance remaining time is shorter.
PEG-7 Fructus Canarii albi grease can reduce the zest of all the other components, suppresses the too fast volatilization of essence.
A kind of preparation method without ethanol perfume is comprised of following steps;
Step 1 adds perfume to dipropylene glycol methyl ether, butyl ether and dipropylene glycol and makes pot, adds essence and stirs more than 5 minutes, to the abundant mix homogeneously of each component;
Step 2, with PEG-7 Fructus Canarii albi grease, BP-3 and BHT mix and blend, wherein its whipping process is not higher than 50 ℃ heating simultaneously with a container, until then fully dissolving adds perfume and make in the pot, stirs;
Step 3 added deionized water and stirring 5 minutes;
Step 4, sealing ageing after 24 hours room temperature filter and namely to get without ethanol perfume.
Embodiment two
Different from embodiment one is that the constituent content of the present embodiment is as follows:
Dipropylene glycol methyl ether 55 ~ 75%
Butyl ether 3 ~ 10%
Dipropylene glycol 5 ~ 15%
PEG-7 Fructus Canarii albi grease 0.5 ~ 5%
BP-3 0.01 ~ 0.09%
BHT 0.1%
Surplus is deionized water.
Embodiment three
Different from embodiment one is that the constituent content of the present embodiment is as follows:
Dipropylene glycol methyl ether 55%
Butyl ether 3%
Dipropylene glycol 5%
PEG-7 Fructus Canarii albi grease 0.5%
BP-3 0.01%
BHT 0.1%
Surplus is deionized water.
Embodiment four
Different from embodiment one is that the constituent content of the present embodiment is as follows:
Dipropylene glycol methyl ether 75%
Butyl ether 10%
Dipropylene glycol 5%
PEG-7 Fructus Canarii albi grease 5%
BP-3 0.09%
BHT 0.1%
Surplus is deionized water.
Embodiment five
Different from embodiment one is that the constituent content of the present embodiment is as follows:
Dipropylene glycol methyl ether 59 ~ 66%
Butyl ether 3.9 ~ 5.9%
Dipropylene glycol 9 ~ 11%
PEG-7 Fructus Canarii albi grease 0.9 ~ 3.9%
BP-3 0.03 ~ 0.06%
BHT 0.1%
Surplus is deionized water
Embodiment six
Different from embodiment one is that the constituent content of the present embodiment is as follows:
Dipropylene glycol methyl ether 59%
Butyl ether 3.9%
Dipropylene glycol 9%
PEG-7 Fructus Canarii albi grease 0.9%
BP-3 0.03%
BHT 0.1%
Surplus is deionized water.
Embodiment seven
Different from embodiment one is that the constituent content of the present embodiment is as follows:
Dipropylene glycol methyl ether 66%
Butyl ether 5.9%
Dipropylene glycol 11%
PEG-7 Fructus Canarii albi grease 3.9%
BP-3 0.06%
BHT 0.1%
Surplus is deionized water.
Embodiment eight
Dipropylene glycol methyl ether 59%
Butyl ether 5.9%
Dipropylene glycol 9.9%
PEG-7 Fructus Canarii albi grease 1.9%
BP-3 0.05%
BHT 0.1%
Surplus is deionized water.
Claims (5)
1. one kind without ethanol perfume, it is characterized in that this perfume is made of following component by weight percentage:
Dipropylene glycol methyl ether 55 ~ 75%,
Butyl ether 3 ~ 10%,
Dipropylene glycol 5 ~ 15%,
PEG-7 Fructus Canarii albi grease 0.5 ~ 5%,
BP-3 0.01 ~ 0.09%,
BHT 0.1%，
Surplus is deionized water.
2. according to claim 1 without ethanol perfume, it is characterized in that this perfume is made of following component by weight percentage:
Dipropylene glycol methyl ether 59 ~ 66%,
Butyl ether 3.9 ~ 5.9%,
Dipropylene glycol 9 ~ 11%,
PEG-7 Fructus Canarii albi grease 0.9 ~ 3.9%,
BP-3 0.03 ~ 0.06%,
BHT 0.1%，
Surplus is deionized water.
3. according to claim 1 without ethanol perfume, it is characterized in that this perfume is made of following component by weight percentage:
Dipropylene glycol methyl ether 65%,
Butyl ether 5%,
Dipropylene glycol 10%,
PEG-7 Fructus Canarii albi grease 2%,
BP-3 0.05%,
BHT 0.1%，
Surplus is deionized water.
4. the preparation method without ethanol perfume is characterized in that this preparation method is comprised of following steps;
Step 1 adds perfume to dipropylene glycol methyl ether, butyl ether and dipropylene glycol and makes pot, adds essence and stirs more than 5 minutes, to the abundant mix homogeneously of each component;
Step 2, with a container PEG-7 Fructus Canarii albi grease, BP-3 and BHT are mixed to fully dissolving after, add perfume and make in the pot, stir;
Step 3 added deionized water and stirring 5 minutes;
Step 4, sealing ageing after 24 hours room temperature filter and namely to get without ethanol perfume.
5. the preparation method without ethanol perfume according to claim 4, it is characterized in that described step 2, with PEG-7 Fructus Canarii albi grease, BP-3 and BHT mix and blend, wherein its whipping process is not higher than 50 ℃ heating simultaneously with a container, until fully dissolving.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012105872271A CN103054756A (en) | 2012-12-31 | 2012-12-31 | Ethanol-free perfume |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012105872271A CN103054756A (en) | 2012-12-31 | 2012-12-31 | Ethanol-free perfume |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103054756A true CN103054756A (en) | 2013-04-24 |
Family
ID=48097859
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012105872271A Pending CN103054756A (en) | 2012-12-31 | 2012-12-31 | Ethanol-free perfume |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103054756A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103330670A (en) * | 2013-06-08 | 2013-10-02 | 吴江市利达上光制品有限公司 | Ethanol-free perfume |
| CN111135134A (en) * | 2020-01-22 | 2020-05-12 | 华东理工大学 | Twenty-four solar terms perfume and preparation method thereof |
| CN111388338A (en) * | 2020-03-20 | 2020-07-10 | 广州乐宠宠物用品有限公司 | Pet perfume with lasting fragrance retaining effect and preparation method thereof |
| CN112791015A (en) * | 2021-01-25 | 2021-05-14 | 湖北煜韩环境科技有限公司 | Essence solubilizer and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1286123A (en) * | 1999-08-26 | 2001-03-07 | 国际香料和香精公司 | Monophasic waer surfactant-free non-toxic air refreshing agent composition and core type air refreshing device using same |
-
2012
- 2012-12-31 CN CN2012105872271A patent/CN103054756A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1286123A (en) * | 1999-08-26 | 2001-03-07 | 国际香料和香精公司 | Monophasic waer surfactant-free non-toxic air refreshing agent composition and core type air refreshing device using same |
Non-Patent Citations (1)
| Title |
|---|
| 王利兵等: "《食品安全化学》", 31 October 2012, article "二苯甲酮" * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103330670A (en) * | 2013-06-08 | 2013-10-02 | 吴江市利达上光制品有限公司 | Ethanol-free perfume |
| CN111135134A (en) * | 2020-01-22 | 2020-05-12 | 华东理工大学 | Twenty-four solar terms perfume and preparation method thereof |
| CN111388338A (en) * | 2020-03-20 | 2020-07-10 | 广州乐宠宠物用品有限公司 | Pet perfume with lasting fragrance retaining effect and preparation method thereof |
| CN112791015A (en) * | 2021-01-25 | 2021-05-14 | 湖北煜韩环境科技有限公司 | Essence solubilizer and preparation method thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
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| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20130424 |