CN101215201A - Method of producing humic acid silicon fertilizer - Google Patents

Abstract

The invention relates to a process for producing humic acid silicon fertilizer, which belongs to the field of fertilizers. The process comprises: analytically burning and differentiating quartz sand blocks, mixing and weathering coal and quartz sand with fine crushing block shape, matching azophoska and trace element, granulating, drying, and preparing liquid amino acid, colorizing and drying, preparing the humic acid silicon fertilizer from the eight steps. The humic acid silicon fertilizer prepared according to the method contains various nutritional components which are needed for crops growth, the humic acid silicon fertilizer is not only easy to be absorbed by the crops, but also leads to a well developed root system and abundant fruits, further, the invention has distinctive benefit for lodging resistance, diseases and insect pests resistance, antifreezing and salt and alkali resistance.

Description

A kind of production method of humic acid silicon fertilizer

1, technical field: the production method of humic acid silicon fertilizer of the present invention belongs to fertilizer field, and relating in particular to a kind of is the production method of the green non-pollution humic acid silicon fertilizer of major ingredient with quartz sand, weathered coal.

2, background technology: the fertilizer of selling on the market mostly is chemical fertilizer greatly now, and facility investment is big, complex process.It is poor to use back soil compaction ventilation property, and crop quality descends, and chemical residual has certain influence to human and livestock health.By retrieval, existing 18 siliceous fertilizer applications for a patent for invention, wherein application number is 02137924.6, denomination of invention is the application of " seed amino acid, humic acid silicon fertilizer and production method thereof ", disclose a kind of with liquid soluble glass as hydrolytic reagent, be raw material with discarded albumen, add depress hydrolysis 2-8 hour after, add weathered coal, through stirring, granulation, oven dry back generate the method for amino acid, humic acid silicon fertilizer.

3, summary of the invention: the present invention seeks to provide a kind of is the production method of the humic acid silicon fertilizer of major ingredient with quartz sand, weathered coal.

The object of the present invention is achieved like this: the technical process of production is:

1. burn and separate differentiation: it is to make it dilution among 90% the sulfuric acid 30kg that clear water 50kg is blended into concentration, and the acid solution with dilution evenly is sprayed on the quartzy sand lump 100kg of dioxide-containing silica 65-70% again, makes it to be fragmented into bulk in small, broken bits;

2. mix: the blout sand 40kg in small, broken bits that 1. weathered coal 40kg and the step of content of humic acid 40-45% made mixes;

3. join nitrogen phosphorus potassium and trace element: in adding ferrous sulfate 1kg, total zinc 〉=0.01% zinc sulfate 1kg of the vitriolate of tartar 10kg of the calcium superphosphate 4kg of the urea 4kg of total nitrogen 〉=46%, total phosphorus 〉=46%, total potassium 〉=46%, total iron 〉=0.01% 2., be ground into 180-200 order powder;

4. granulation: the powder that step makes in is 3. sent into granulation in the tablets press, particle diameter 2.5-3mm;

5. oven dry: the pellet that step makes in is 4. sent into dryer, keeps 45-60 ℃ of temperature, dry while rotating to the pellet moisture content be 20% o'clock, from the discharging of the dryer the other end;

6. prepare liquid amino acid: with animal blood, animal skeleton, the animal chopped cooked entrails of sheep, vegetable oil residue by weight 1: 1: 1: 1 carries out proportioning, rubs by mincer, is placed on caldron, adds water to and soaks punishment in advance, heats to 100 ℃, boils sterilization in 30 minutes again.Use 1 * 1mm spun yarn net filtration to fall bone, the chopped cooked entrails of sheep, residue etc. subsequently, filtrate is inserted encloses container, naturally cool to 15-30 ℃.18g brown sugar is dissolved in the 479g water, makes brown sugar water.Photosynthetic bacteria (AM01), actinomycetes (AM02), each 1g of milk-acid bacteria (AM04) are blended in the brown sugar water, brown sugar water is added in the 12.5kg filtrate again, the ratio that adds yeast (AM03) 2kg in every 100kg filtrate adds yeast (AM03), make filtrate keep 5-40 ℃ of temperature, spontaneous fermentation 5-7 days, be converted into liquid amino acid;

7. colouring: liquid amino acid and clear water that step is made in 6. exchange uniform dilution in 1: 1 ratio, diluent evenly are sprayed on the pellet that step dried in 5. every 50kg pellet sprinkling 1kg diluent again;

8. oven dry: will go up lustful pellet and send into dryer, keep 45-60 ℃ of temperature, dry while rotate, to the pellet moisture content be 20% o'clock, from the discharging of the dryer the other end, be humic acid silicon fertilizer.

This humic acid silicon fertilizer raw material is extensively inexpensive, can gather materials on the spot, and fertilizer efficiency is comprehensive, contains the required various nutritive ingredients of crop growth, is not only easily absorbed by crop, and makes well developed root system, and fruit is plentiful, can improve crop quality, output, and anti-storage.Can obviously strengthen crop disease-resistant insect pest ability, resistant to lodging in addition, freeze proof, anti-saline and alkaline unusual effect.

Through Xinjiang Turfan Prefecture quality and metering test according to GB/T 8572-2001 " mensuration of total nitrogen content in the composite fertilizer ", GB/T 8573-1999 " mensuration of available phosphorus content in the composite fertilizer ", GB/T 8574-2002 " determination of potassium content in the composite fertilizer ", NY/T 797-2004 " siliceous fertilizer ", GB/T 11957-2001 " humic acid productive rate measuring method in the coal ", GB/T 8576-2002 " free-water Determination on content in the composite fertilizer " standard, humic acid silicon fertilizer is carried out complete check, and the result is as follows:

The individual event of technical indicator assay is judged

Silicon-dioxide+nitrogen+Vanadium Pentoxide in FLAKES+potassium oxide 〉=36% 46 are qualified

Humic acid≤8% 10.3 is qualified

Moisture content≤15% 10.4 is qualified

5.5-8.0 6.0 is qualified for potential of hydrogen (in pH value)

Outward appearance brown granulated brown granulated is qualified

Use example:

2006,3 mu of Ya Er township, Turpan, Xinjiang peasant Ah certain plantation Chinese cabbages were used this siliceous fertilizer 120 kg, and the Chinese cabbage stature is big, and the bag heart is solid, and volume increase is more than 10%, and disease and pest obviously reduces, and sprays insecticide 2-3 time less, reduces pesticide dosage 30%.Than the obvious anti-storage of the Chinese cabbage of using chemical fertilizer, seldom rotten, the dish of making has peculiar flavour.

2007, Gu Lebage township, Shaya County, Xinjiang Bo Zi village Ni peasant plants 1000 mu of upland cotton, uses 60 tons of this siliceous fertilizers, grows fine, the sturdy non-lodging of cotton stalk, the knot peach is many, and cotton producing increases by 25%, and velveteen increases by 2%, whiteness increases, cotton boll vegetative point place does not have macula lutea, shifts to an earlier date precocious 3-5 days, and drought resisting and diseases and insect pests resistance obviously strengthen.Reduce number of times 1-2 time of watering.Spray insecticide 2-3 time less, reduce pesticide dosage 30%.

4, embodiment:

Embodiment: the technical process of production:

1. burn and separate differentiation: it is to make it dilution among 90% the sulfuric acid 30kg that clear water 50kg is blended into concentration, and the acid solution with dilution evenly is sprayed on the quartzy sand lump 100kg of dioxide-containing silica 65-70% again, makes it to be fragmented into bulk in small, broken bits.

2. mix: the blout sand 40kg in small, broken bits that 1. weathered coal 40kg and the step of content of humic acid 40-45% made mixes.

3. join nitrogen phosphorus potassium and trace element: in adding ferrous sulfate 1kg, total zinc 〉=0.01% zinc sulfate 1kg of the vitriolate of tartar 10kg of the calcium superphosphate 4kg of the urea 4kg of total nitrogen 〉=46%, total phosphorus 〉=46%, total potassium 〉=46%, total iron 〉=0.01% 2., be ground into 180-200 order powder.

4. granulation: the powder that step makes in is 3. sent into granulation in the tablets press, particle diameter 2.5-3mm.

5. oven dry: the pellet that step makes in is 4. sent into dryer, keeps 45-60 ℃ of temperature, dry while rotating to the pellet moisture content be 20% o'clock, from the discharging of the dryer the other end.

6. prepare liquid amino acid: with animal blood such as cattle and sheep, animal skeleton, the animal chopped cooked entrails of sheep, vegetable oil residue by weight 1: 1: 1: 1 carries out proportioning, rubs by mincer, is placed on caldron, add water to and soak punishment in advance, heat to 100 ℃, boil sterilization in 30 minutes again, its soup juice high protein liquid.Use 1 * 1mm spun yarn net filtration to fall bone, the chopped cooked entrails of sheep, residue etc. subsequently, filtrate is inserted encloses container, naturally cool to 15-30 ℃.18g brown sugar is dissolved in the 479g water, makes brown sugar water.Photosynthetic bacteria (AM01), actinomycetes (AM02), each 1g of milk-acid bacteria (AM04) are blended in the brown sugar water, brown sugar water is added in the 12.5kg filtrate again, the ratio that adds yeast (AM03) 2kg in every 100kg filtrate adds yeast (AM03), make filtrate keep 5-40 ℃ of temperature, spontaneous fermentation 5-7 days, be converted into liquid amino acid.

7. colouring: liquid amino acid and clear water that step is made in 6. exchange uniform dilution in 1: 1 ratio, diluent evenly are sprayed on the pellet that step dried in 5. every 50kg pellet sprinkling diluent 1kg again.

8. oven dry: will go up lustful pellet and send into dryer, keep 45-60 ℃ of temperature, dry while rotate, to the pellet moisture content be 20% o'clock, from the discharging of the dryer the other end, be humic acid silicon fertilizer.

Claims (1)

1. the production method of a humic acid silicon fertilizer, it is characterized in that: the technical process of production is:

1. burn and separate differentiation: it is to make it dilution among 90% the sulfuric acid 30kg that clear water 50kg is blended into concentration, and the acid solution with dilution evenly is sprayed on the quartzy sand lump 100kg of dioxide-containing silica 65-70% again, makes it to be fragmented into bulk in small, broken bits;

2. mix: the blout sand 40kg in small, broken bits that 1. weathered coal 40 kg and the step of content of humic acid 40-45% made mixes;

3. join nitrogen phosphorus potassium and trace element: in adding ferrous sulfate 1kg, total zinc 〉=0.01% zinc sulfate 1kg of the vitriolate of tartar 10kg of the calcium superphosphate 4kg of the urea 4kg of total nitrogen 〉=46%, total phosphorus 〉=46%, total potassium 〉=46%, total iron 〉=0.01% 2., be ground into 180-200 order powder;

4. granulation: the powder that step makes in is 3. sent into granulation in the tablets press, particle diameter 2.5-3mm;

5. oven dry: the pellet that step makes in is 4. sent into dryer, keeps 45-60 ℃ of temperature, dry while rotating to the pellet moisture content be 20% o'clock, from the discharging of the dryer the other end;

6. prepare liquid amino acid: with animal blood, animal skeleton, the animal chopped cooked entrails of sheep, vegetable oil residue was by weight 1: 1: 1: 1 carries out proportioning, rub by mincer, be placed on caldron, add water to and soak punishment in advance, heat to 100 ℃, boil sterilization in 30 minutes again, use 1 * 1mm spun yarn net filtration to fall bone subsequently, the chopped cooked entrails of sheep, residue etc., filtrate is inserted encloses container, naturally cool to 15-30 ℃, 18g brown sugar is dissolved in the 479g water, make brown sugar water, with photosynthetic bacteria (AM01), actinomycetes (AM02), each 1g of milk-acid bacteria (AM04) is blended in the brown sugar water, brown sugar water is added in the 12.5kg filtrate, the ratio that adds yeast (AM03) 2kg in every 100kg filtrate adds yeast (AM03) again, makes filtrate keep 5-40 ℃ of temperature, spontaneous fermentation 5-7 days, be converted into liquid amino acid;

7. colouring: liquid amino acid and clear water that step is made in 6. exchange uniform dilution in 1: 1 ratio, diluent evenly are sprayed on the pellet that step dried in 5. every 50kg pellet sprinkling 1kg diluent again;

8. oven dry: will go up lustful pellet and send into dryer, keep 45-60 ℃ of temperature, dry while rotate, to the pellet moisture content be 20% o'clock, from the discharging of the dryer the other end, be humic acid silicon fertilizer.