CN101035499A - 包括多种酸性化合物的自粘合组合物 - Google Patents
包括多种酸性化合物的自粘合组合物 Download PDFInfo
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- CN101035499A CN101035499A CNA2005800274617A CN200580027461A CN101035499A CN 101035499 A CN101035499 A CN 101035499A CN A2005800274617 A CNA2005800274617 A CN A2005800274617A CN 200580027461 A CN200580027461 A CN 200580027461A CN 101035499 A CN101035499 A CN 101035499A
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- self
- adhesive compositions
- orthodontic appliance
- compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K6/00—Preparations for dentistry
- A61K6/30—Compositions for temporarily or permanently fixing teeth or palates, e.g. primers for dental adhesives
- A61K6/35—Preparations for stabilising dentures in the mouth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K6/00—Preparations for dentistry
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- Health & Medical Sciences (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dental Preparations (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
Description
缩写 | 说明和材料来源 |
TEGDMA | 三乙二醇二甲基丙烯酸酯(Sartomer,Exton,PA) |
Procrylat | 2,2-双-4-(3-羟基-丙氧基-苯基)丙烷二甲基丙烯酸酯(CAS 27689-2-9) |
KayamerPM2 | 双(甲基丙烯酰氧基乙基)磷酸酯(Nippon Kayaku,Japan) |
GDMA-P | 甘油二甲基丙烯酸酯磷酸酯如在EP 0237 233(Oxman)中引述的J.Dent.Res.,35,8466(1956)制备(还参见国际公布WO 02/092021(Hecht等人)的实施例3) |
MH-P | 甲基丙烯酰氧己基磷酸酯(参见本文描述的起始材料制备) |
MO-P | 8-甲基丙烯酰氧辛基磷酸酯(参见本文描述的起始材料制备) |
MD-P | 10-甲基丙烯酰氧癸基磷酸酯(参见本文描述的起始材料制备) |
AEROSILOX-50 | 热解二氧化硅(Degussa,Germany) |
填料A | Compolute GP 0.3%溶胶,用GF 31硅酸酯化,如美国专利4,376,835(Schmitt等人)中所述 |
填料B | Sinfony GP 5%,用GF 31硅酸酯化,平均粒度小于0.7微米(SchottElectronics Packaging GmbH,Landshut,Germany) |
填料C | Si Nanocluster AFG 100 V50 4%sil(如美国公开2003/0181541(Wu等人)的实施例1A所述制备) |
填料D | 硅烷处理过的氧化锆-二氧化硅(Zr-Si)填料,如美国专利4,503,169(Randkkev)中所述制备 |
GF-31 | 三甲氧基-甲硅烷基-丙氧基-甲基丙烯酸酯(WackerChemie GmbH,Burghausen,Germany) |
丁基BAP | 丁基氧化膦引发剂(如欧洲专利0 184 095(Ellrich等人)中所述制备) |
BHT | 2,6-二-叔丁基-4-甲基苯酚(Sigma-Aldrich,St.Louis,MO) |
DDSS | .十二烷基硫酸钠盐(Sigma-Aldrich) |
表1:实施例1-5和比较例(CE)1-3中的组分(重量%) | ||||||||
组分 | 实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | CE1 | CE2 | CE3 |
填料A | 37.9 | 0 | 0 | 0 | 0 | 37.9 | 37.9 | 37.9 |
填料B | 29.9 | 0 | 0 | 0 | 0 | 28.9 | 28.9 | 28.9 |
填料C | 0 | 61.8 | 0 | 0 | 0 | 0 | 0 | 0 |
填料D | 0 | 0 | 68.0 | 68.0 | 68.0 | 0 | 0 | 0 |
TEGDMA | 8.8 | 10.2 | 5.2 | 5.2 | 5.2 | 8.8 | 4.5 | 8.8 |
Procrylat | 6.4 | 7.4 | 7.3 | 7.3 | 7.3 | 6.4 | 6.3 | 6.4 |
Kayamer PM2 | 6.3 | 7.3 | 11.5 | 11.5 | 11.5 | 12.5 | 0 | 0 |
GDMA-P | 0 | 0 | 3.8 | 3.8 | 3.8 | 0 | 16.4 | 0 |
MH-P | 6.3 | 7.3 | 3.8 | 0 | 0 | 0 | 0 | 12.5 |
MO-P | 0 | 0 | 0 | 3.8 | 0 | 0 | 0 | 0 |
MD-P | 0 | 0 | 0 | 0 | 3.8 | 0 | 0 | 0 |
AEROSIL OX-50 | 5.2 | 5.2 | 0 | 0 | 0 | 5.2 | 5.2 | 5.2 |
丁基BAP | 0.2 | 0.4 | 0.3 | 0.3 | 0.3 | 0.2 | 0.7 | 0.2 |
BHT | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 |
DDSS | 0 | 0.5 | 0 | 0 | 0 | 0 | 0 | 0 |
总计 | 100 | 100 | 100 | 100 | 100 | 100 | 100 | 100 |
表1(续)评定结果 | ||||||||
对牙质的粘合力(MPa) | 3.0 | 0.7 | 2.8 | 2.9 | 1.9 | 2.5 | 0 | 0 |
对牙釉质的粘合力(MPa) | 6.1 | 3.8 | 5.5 | 8.1 | 10.6 | 4.1 | 0 | 2.7 |
挠曲强度(MPa) | 116 | 105 | 115 | 92 | 108 | 79 | 138 | 76 |
耐压强度(MPa) | 251 | 307 | 351 | 329 | 331 | 264 | 301 | 204 |
Claims (43)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US60065804P | 2004-08-11 | 2004-08-11 | |
US60/600,658 | 2004-08-11 | ||
PCT/US2005/028536 WO2006020760A1 (en) | 2004-08-11 | 2005-08-09 | Self-adhesive compositions including a plurality of acidic compounds |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101035499A true CN101035499A (zh) | 2007-09-12 |
CN101035499B CN101035499B (zh) | 2012-09-05 |
Family
ID=35385680
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2005800274617A Expired - Fee Related CN101035499B (zh) | 2004-08-11 | 2005-08-09 | 包括多种酸性化合物的自粘合组合物 |
Country Status (9)
Country | Link |
---|---|
US (1) | US8722760B2 (zh) |
EP (1) | EP1784155B1 (zh) |
JP (1) | JP5037342B2 (zh) |
KR (1) | KR101260525B1 (zh) |
CN (1) | CN101035499B (zh) |
AT (1) | ATE526006T1 (zh) |
AU (1) | AU2005272808B8 (zh) |
CA (1) | CA2575976A1 (zh) |
WO (1) | WO2006020760A1 (zh) |
Cited By (1)
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CN110236959A (zh) * | 2019-07-30 | 2019-09-17 | 山东大学 | 一种具有抗菌性能的自修复自粘接树脂水门汀及其制备方法 |
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-
2005
- 2005-08-09 WO PCT/US2005/028536 patent/WO2006020760A1/en active Application Filing
- 2005-08-09 CN CN2005800274617A patent/CN101035499B/zh not_active Expired - Fee Related
- 2005-08-09 AU AU2005272808A patent/AU2005272808B8/en not_active Ceased
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- 2005-08-09 US US11/573,423 patent/US8722760B2/en active Active
- 2005-08-09 JP JP2007525785A patent/JP5037342B2/ja not_active Expired - Fee Related
- 2005-08-09 KR KR1020077005562A patent/KR101260525B1/ko not_active IP Right Cessation
- 2005-08-09 CA CA002575976A patent/CA2575976A1/en not_active Abandoned
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110236959A (zh) * | 2019-07-30 | 2019-09-17 | 山东大学 | 一种具有抗菌性能的自修复自粘接树脂水门汀及其制备方法 |
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WO2006020760A1 (en) | 2006-02-23 |
US20070248927A1 (en) | 2007-10-25 |
EP1784155A1 (en) | 2007-05-16 |
EP1784155B1 (en) | 2011-09-28 |
AU2005272808B8 (en) | 2011-11-03 |
JP2008510038A (ja) | 2008-04-03 |
CA2575976A1 (en) | 2006-02-23 |
KR20070057824A (ko) | 2007-06-07 |
KR101260525B1 (ko) | 2013-05-06 |
CN101035499B (zh) | 2012-09-05 |
US8722760B2 (en) | 2014-05-13 |
JP5037342B2 (ja) | 2012-09-26 |
AU2005272808B2 (en) | 2011-10-06 |
AU2005272808A1 (en) | 2006-02-23 |
ATE526006T1 (de) | 2011-10-15 |
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