CN100545254C - 粒状洗涤剂组合物及其生产方法 - Google Patents

粒状洗涤剂组合物及其生产方法 Download PDF

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Publication number: CN100545254C
Authority: CN; China
Prior art keywords: weight; particle; detergent granules; active agent; detergent
Prior art date: 2003-02-06
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Lifetime

Application number

CNB2004800036205A

Other languages

English (en)

Chinese (zh)

Other versions

CN1748023A (zh

Inventor

增井宏之

堀江弘道

福留信一

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Lion Corp

Original Assignee

Lion Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2003-02-06

Filing date

2004-02-04

Publication date

2009-09-30

2004-02-04 Application filed by Lion Corp filed Critical Lion Corp

2006-03-15 Publication of CN1748023A publication Critical patent/CN1748023A/zh

2009-09-30 Application granted granted Critical

2009-09-30 Publication of CN100545254C publication Critical patent/CN100545254C/zh

2024-02-04 Anticipated expiration legal-status Critical

Status Expired - Lifetime legal-status Critical Current

Links

239000003599 detergent Substances 0.000 title claims abstract description 198
239000000203 mixture Substances 0.000 title claims abstract description 110
238000004519 manufacturing process Methods 0.000 title claims abstract description 25
239000002245 particle Substances 0.000 claims abstract description 155
239000008187 granular material Substances 0.000 claims abstract description 137
239000013543 active substance Substances 0.000 claims abstract description 95
239000003945 anionic surfactant Substances 0.000 claims abstract description 71
238000005406 washing Methods 0.000 claims abstract description 53
239000004094 surface-active agent Substances 0.000 claims abstract description 26
-1 fatty acid salt Chemical class 0.000 claims description 69
238000005469 granulation Methods 0.000 claims description 62
230000003179 granulation Effects 0.000 claims description 62
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
229910052799 carbon Inorganic materials 0.000 claims description 25
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 21
239000007864 aqueous solution Substances 0.000 claims description 15
239000000194 fatty acid Substances 0.000 claims description 14
150000003839 salts Chemical class 0.000 claims description 13
239000011230 binding agent Substances 0.000 claims description 10
239000004615 ingredient Substances 0.000 claims description 10
235000014113 dietary fatty acids Nutrition 0.000 claims description 9
229930195729 fatty acid Natural products 0.000 claims description 9
229920000642 polymer Polymers 0.000 claims description 9
NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 8
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 7
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 5
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 5
229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 4
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 4
239000001768 carboxy methyl cellulose Substances 0.000 claims description 4
235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 4
239000008112 carboxymethyl-cellulose Substances 0.000 claims description 4
239000011976 maleic acid Substances 0.000 claims description 4
239000004372 Polyvinyl alcohol Substances 0.000 claims description 3
229920002125 Sokalan® Polymers 0.000 claims description 3
150000004702 methyl esters Chemical class 0.000 claims description 3
239000004584 polyacrylic acid Substances 0.000 claims description 3
229920002451 polyvinyl alcohol Polymers 0.000 claims description 3
229920002153 Hydroxypropyl cellulose Polymers 0.000 claims description 2
QOSMNYMQXIVWKY-UHFFFAOYSA-N Propyl levulinate Chemical compound CCCOC(=O)CCC(C)=O QOSMNYMQXIVWKY-UHFFFAOYSA-N 0.000 claims description 2
125000004494 ethyl ester group Chemical group 0.000 claims description 2
239000001863 hydroxypropyl cellulose Substances 0.000 claims description 2
235000010977 hydroxypropyl cellulose Nutrition 0.000 claims description 2
229920006395 saturated elastomer Polymers 0.000 claims description 2
239000002075 main ingredient Substances 0.000 abstract description 18
238000010521 absorption reaction Methods 0.000 abstract description 6
230000000181 anti-adherent effect Effects 0.000 abstract description 4
238000002156 mixing Methods 0.000 description 57
238000000034 method Methods 0.000 description 54
239000000843 powder Substances 0.000 description 47
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 39
239000003795 chemical substances by application Substances 0.000 description 37
239000000463 material Substances 0.000 description 32
239000003921 oil Substances 0.000 description 32
235000019198 oils Nutrition 0.000 description 32
238000004898 kneading Methods 0.000 description 29
238000002360 preparation method Methods 0.000 description 27
238000003756 stirring Methods 0.000 description 27
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 26
229910021536 Zeolite Inorganic materials 0.000 description 25
125000000217 alkyl group Chemical group 0.000 description 25
239000010457 zeolite Substances 0.000 description 25
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 21
235000013599 spices Nutrition 0.000 description 20
235000017550 sodium carbonate Nutrition 0.000 description 19
229910000029 sodium carbonate Inorganic materials 0.000 description 19
238000000227 grinding Methods 0.000 description 15
239000013042 solid detergent Substances 0.000 description 15
239000000049 pigment Substances 0.000 description 14
239000002253 acid Substances 0.000 description 13
239000007921 spray Substances 0.000 description 13
238000005507 spraying Methods 0.000 description 13
125000003342 alkenyl group Chemical group 0.000 description 12
239000007788 liquid Substances 0.000 description 12
239000011734 sodium Substances 0.000 description 12
125000004432 carbon atom Chemical group C* 0.000 description 11
239000002002 slurry Substances 0.000 description 11
229910052708 sodium Inorganic materials 0.000 description 11
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 10
235000010724 Wisteria floribunda Nutrition 0.000 description 10
238000001035 drying Methods 0.000 description 10
235000019353 potassium silicate Nutrition 0.000 description 10
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 10
108090000790 Enzymes Proteins 0.000 description 9
102000004190 Enzymes Human genes 0.000 description 9
241000282326 Felis catus Species 0.000 description 9
239000002734 clay mineral Substances 0.000 description 9
239000002304 perfume Substances 0.000 description 9
BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 9
235000015320 potassium carbonate Nutrition 0.000 description 9
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 9
235000019832 sodium triphosphate Nutrition 0.000 description 9
229920003171 Poly (ethylene oxide) Polymers 0.000 description 8
229910052783 alkali metal Inorganic materials 0.000 description 8
239000002994 raw material Substances 0.000 description 8
239000000243 solution Substances 0.000 description 8
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
239000002585 base Substances 0.000 description 7
238000001125 extrusion Methods 0.000 description 7
239000004744 fabric Substances 0.000 description 7
125000005702 oxyalkylene group Chemical group 0.000 description 7
239000006187 pill Substances 0.000 description 7
229910052700 potassium Inorganic materials 0.000 description 7
238000010298 pulverizing process Methods 0.000 description 7
239000000126 substance Substances 0.000 description 7
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 6
GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 6
239000000654 additive Substances 0.000 description 6
230000000996 additive effect Effects 0.000 description 6
229910052910 alkali metal silicate Inorganic materials 0.000 description 6
125000005843 halogen group Chemical group 0.000 description 6
239000011591 potassium Substances 0.000 description 6
239000002243 precursor Substances 0.000 description 6
235000007586 terpenes Nutrition 0.000 description 6
101710194948 Protein phosphatase PhpP Proteins 0.000 description 5
125000005907 alkyl ester group Chemical group 0.000 description 5
239000001055 blue pigment Substances 0.000 description 5
239000013078 crystal Substances 0.000 description 5
238000009826 distribution Methods 0.000 description 5
239000000428 dust Substances 0.000 description 5
239000000975 dye Substances 0.000 description 5
150000002148 esters Chemical class 0.000 description 5
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 5
238000011068 loading method Methods 0.000 description 5
238000012986 modification Methods 0.000 description 5
230000004048 modification Effects 0.000 description 5
239000000344 soap Substances 0.000 description 5
238000001694 spray drying Methods 0.000 description 5
WPYMKLBDIGXBTP-UHFFFAOYSA-N Benzoic acid Natural products OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 4
GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 4
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
125000001931 aliphatic group Chemical group 0.000 description 4
125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 4
KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 4
235000010338 boric acid Nutrition 0.000 description 4
229960002645 boric acid Drugs 0.000 description 4
150000001721 carbon Chemical group 0.000 description 4
239000003610 charcoal Substances 0.000 description 4
238000005660 chlorination reaction Methods 0.000 description 4
239000011248 coating agent Substances 0.000 description 4
150000001875 compounds Chemical class 0.000 description 4
238000009792 diffusion process Methods 0.000 description 4
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238000011156 evaluation Methods 0.000 description 4
235000019387 fatty acid methyl ester Nutrition 0.000 description 4
150000002191 fatty alcohols Chemical class 0.000 description 4
125000002768 hydroxyalkyl group Chemical group 0.000 description 4
238000005259 measurement Methods 0.000 description 4
238000006386 neutralization reaction Methods 0.000 description 4
HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 4
230000002829 reductive effect Effects 0.000 description 4
238000012216 screening Methods 0.000 description 4
229910052938 sodium sulfate Inorganic materials 0.000 description 4
235000011152 sodium sulphate Nutrition 0.000 description 4
239000004834 spray adhesive Substances 0.000 description 4
239000003760 tallow Substances 0.000 description 4
UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 4
RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 3
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 3
229910004298 SiO 2 Inorganic materials 0.000 description 3
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 3
229920002472 Starch Polymers 0.000 description 3
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical group C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 3
238000013019 agitation Methods 0.000 description 3
150000001340 alkali metals Chemical group 0.000 description 3
229910021417 amorphous silicon Inorganic materials 0.000 description 3
SMWDFEZZVXVKRB-UHFFFAOYSA-N anhydrous quinoline Natural products N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 3
150000001450 anions Chemical class 0.000 description 3
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239000001110 calcium chloride Substances 0.000 description 3
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238000000576 coating method Methods 0.000 description 3
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230000008014 freezing Effects 0.000 description 3
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FDQGNLOWMMVRQL-UHFFFAOYSA-N Allobarbital Chemical compound C=CCC1(CC=C)C(=O)NC(=O)NC1=O FDQGNLOWMMVRQL-UHFFFAOYSA-N 0.000 description 2
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 2
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206010013786 Dry skin Diseases 0.000 description 2
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VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
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FEWJPZIEWOKRBE-JCYAYHJZSA-L L-tartrate(2-) Chemical compound [O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O FEWJPZIEWOKRBE-JCYAYHJZSA-L 0.000 description 2
229910019142 PO4 Inorganic materials 0.000 description 2
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150000003973 alkyl amines Chemical class 0.000 description 2
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150000001408 amides Chemical class 0.000 description 2
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150000003934 aromatic aldehydes Chemical class 0.000 description 2
IRERQBUNZFJFGC-UHFFFAOYSA-L azure blue Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[S-]S[S-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] IRERQBUNZFJFGC-UHFFFAOYSA-L 0.000 description 2
229910052728 basic metal Inorganic materials 0.000 description 2
150000003818 basic metals Chemical class 0.000 description 2
SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 description 2
HTZCNXWZYVXIMZ-UHFFFAOYSA-M benzyl(triethyl)azanium;chloride Chemical compound [Cl-].CC[N+](CC)(CC)CC1=CC=CC=C1 HTZCNXWZYVXIMZ-UHFFFAOYSA-M 0.000 description 2
OCBHHZMJRVXXQK-UHFFFAOYSA-M benzyl-dimethyl-tetradecylazanium;chloride Chemical compound [Cl-].CCCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 OCBHHZMJRVXXQK-UHFFFAOYSA-M 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
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150000001768 cations Chemical class 0.000 description 2
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239000003153 chemical reaction reagent Substances 0.000 description 2
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125000001309 chloro group Chemical group Cl* 0.000 description 2
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NZNMSOFKMUBTKW-UHFFFAOYSA-N cyclohexanecarboxylic acid Chemical compound OC(=O)C1CCCCC1 NZNMSOFKMUBTKW-UHFFFAOYSA-N 0.000 description 2
KSMVZQYAVGTKIV-UHFFFAOYSA-N decanal Chemical compound CCCCCCCCCC=O KSMVZQYAVGTKIV-UHFFFAOYSA-N 0.000 description 2
FLKPEMZONWLCSK-UHFFFAOYSA-N diethyl phthalate Chemical compound CCOC(=O)C1=CC=CC=C1C(=O)OCC FLKPEMZONWLCSK-UHFFFAOYSA-N 0.000 description 2
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KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 2
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KVWWIYGFBYDJQC-UHFFFAOYSA-N methyl dihydrojasmonate Chemical compound CCCCCC1C(CC(=O)OC)CCC1=O KVWWIYGFBYDJQC-UHFFFAOYSA-N 0.000 description 2
108010020132 microbial serine proteinases Proteins 0.000 description 2
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238000004513 sizing Methods 0.000 description 2
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BOPPSUHPZARXTH-UHFFFAOYSA-N ocean propanal Chemical compound O=CC(C)CC1=CC=C2OCOC2=C1 BOPPSUHPZARXTH-UHFFFAOYSA-N 0.000 description 1
125000005646 oximino group Chemical group 0.000 description 1
VGTPKLINSHNZRD-UHFFFAOYSA-N oxoborinic acid Chemical compound OB=O VGTPKLINSHNZRD-UHFFFAOYSA-N 0.000 description 1
ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 description 1
238000012856 packing Methods 0.000 description 1
239000011236 particulate material Substances 0.000 description 1
239000001814 pectin Substances 0.000 description 1
235000010987 pectin Nutrition 0.000 description 1
229920001277 pectin Polymers 0.000 description 1
RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 1
ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
150000002989 phenols Chemical class 0.000 description 1
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
WTJKGGKOPKCXLL-RRHRGVEJSA-N phosphatidylcholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCCC=CCCCCCCCC WTJKGGKOPKCXLL-RRHRGVEJSA-N 0.000 description 1
150000003016 phosphoric acids Chemical class 0.000 description 1
235000002949 phytic acid Nutrition 0.000 description 1
SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 description 1
229920000058 polyacrylate Polymers 0.000 description 1
229920005646 polycarboxylate Polymers 0.000 description 1
229920000728 polyester Polymers 0.000 description 1
229920001223 polyethylene glycol Polymers 0.000 description 1
229920005862 polyol Polymers 0.000 description 1
150000003077 polyols Chemical class 0.000 description 1
229910052913 potassium silicate Inorganic materials 0.000 description 1
BHZRJJOHZFYXTO-UHFFFAOYSA-L potassium sulfite Chemical compound [K+].[K+].[O-]S([O-])=O BHZRJJOHZFYXTO-UHFFFAOYSA-L 0.000 description 1
235000019252 potassium sulphite Nutrition 0.000 description 1
238000004321 preservation Methods 0.000 description 1
238000003825 pressing Methods 0.000 description 1
150000003138 primary alcohols Chemical class 0.000 description 1
230000000750 progressive effect Effects 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
150000003233 pyrroles Chemical class 0.000 description 1
150000003242 quaternary ammonium salts Chemical class 0.000 description 1
238000011160 research Methods 0.000 description 1
239000011435 rock Substances 0.000 description 1
229910000275 saponite Inorganic materials 0.000 description 1
150000003333 secondary alcohols Chemical class 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000003352 sequestering agent Substances 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1
229910052814 silicon oxide Inorganic materials 0.000 description 1
229910052709 silver Inorganic materials 0.000 description 1
239000004332 silver Substances 0.000 description 1
235000017557 sodium bicarbonate Nutrition 0.000 description 1
229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
239000001488 sodium phosphate Substances 0.000 description 1
RPACBEVZENYWOL-XFULWGLBSA-M sodium;(2r)-2-[6-(4-chlorophenoxy)hexyl]oxirane-2-carboxylate Chemical compound [Na+].C=1C=C(Cl)C=CC=1OCCCCCC[C@]1(C(=O)[O-])CO1 RPACBEVZENYWOL-XFULWGLBSA-M 0.000 description 1
239000002689 soil Substances 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000000600 sorbitol Substances 0.000 description 1
229910052596 spinel Inorganic materials 0.000 description 1
239000011029 spinel Substances 0.000 description 1
230000003068 static effect Effects 0.000 description 1
239000010959 steel Substances 0.000 description 1
125000001424 substituent group Chemical group 0.000 description 1
KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 description 1
KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical class OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
238000006277 sulfonation reaction Methods 0.000 description 1
229910021653 sulphate ion Inorganic materials 0.000 description 1
239000000454 talc Substances 0.000 description 1
235000012222 talc Nutrition 0.000 description 1
229910052623 talc Inorganic materials 0.000 description 1
239000008399 tap water Substances 0.000 description 1
235000020679 tap water Nutrition 0.000 description 1
150000003512 tertiary amines Chemical class 0.000 description 1
150000003866 tertiary ammonium salts Chemical class 0.000 description 1
FRPJTGXMTIIFIT-UHFFFAOYSA-N tetraacetylethylenediamine Chemical compound CC(=O)C(N)(C(C)=O)C(N)(C(C)=O)C(C)=O FRPJTGXMTIIFIT-UHFFFAOYSA-N 0.000 description 1
DZLFLBLQUQXARW-UHFFFAOYSA-N tetrabutylammonium Chemical compound CCCC[N+](CCCC)(CCCC)CCCC DZLFLBLQUQXARW-UHFFFAOYSA-N 0.000 description 1
JRMUNVKIHCOMHV-UHFFFAOYSA-M tetrabutylammonium bromide Chemical compound [Br-].CCCC[N+](CCCC)(CCCC)CCCC JRMUNVKIHCOMHV-UHFFFAOYSA-M 0.000 description 1
YMBCJWGVCUEGHA-UHFFFAOYSA-M tetraethylammonium chloride Chemical compound [Cl-].CC[N+](CC)(CC)CC YMBCJWGVCUEGHA-UHFFFAOYSA-M 0.000 description 1
RLQWHDODQVOVKU-UHFFFAOYSA-N tetrapotassium;silicate Chemical compound [K+].[K+].[K+].[K+].[O-][Si]([O-])([O-])[O-] RLQWHDODQVOVKU-UHFFFAOYSA-N 0.000 description 1
POWFTOSLLWLEBN-UHFFFAOYSA-N tetrasodium;silicate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-][Si]([O-])([O-])[O-] POWFTOSLLWLEBN-UHFFFAOYSA-N 0.000 description 1
RBNWAMSGVWEHFP-UHFFFAOYSA-N trans-p-Menthane-1,8-diol Chemical compound CC(C)(O)C1CCC(C)(O)CC1 RBNWAMSGVWEHFP-UHFFFAOYSA-N 0.000 description 1
ZNEOHLHCKGUAEB-UHFFFAOYSA-N trimethylphenylammonium Chemical compound C[N+](C)(C)C1=CC=CC=C1 ZNEOHLHCKGUAEB-UHFFFAOYSA-N 0.000 description 1
RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
229910000406 trisodium phosphate Inorganic materials 0.000 description 1
235000019801 trisodium phosphate Nutrition 0.000 description 1
230000000007 visual effect Effects 0.000 description 1
238000004018 waxing Methods 0.000 description 1
239000004711 α-olefin Substances 0.000 description 1
229930007850 β-damascenone Natural products 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Detergent Compositions (AREA)

CNB2004800036205A 2003-02-06 2004-02-04 粒状洗涤剂组合物及其生产方法 Expired - Lifetime CN100545254C (zh)

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JP2003029821		2003-02-06
JP029821/2003		2003-02-06

Publications (2)

Publication Number	Publication Date
CN1748023A CN1748023A (zh)	2006-03-15
CN100545254C true CN100545254C (zh)	2009-09-30

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JP (1)	JP4591704B2 (ja)
KR (1)	KR101029298B1 (ja)
CN (1)	CN100545254C (ja)
WO (1)	WO2004069970A1 (ja)

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Publication number	Priority date	Publication date	Assignee	Title
KR101134997B1 (ko) *	2004-06-30	2012-04-09	라이온 가부시키가이샤	높은 벌크밀도의 입상 세제 조성물 및 그 제조 방법
JP5971753B2 (ja) *	2012-07-09	2016-08-17	花王株式会社	洗剤粒子の製造方法
CN107043941A (zh) *	2017-01-20	2017-08-15	昌邑市龙港无机硅有限公司	一种金属清洗剂

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US4869843A (en) *	1986-01-17	1989-09-26	Kao Corporation	High-density granular detergent composition
WO2000077159A1 (fr) *	1999-06-16	2000-12-21	Kao Corporation	Particules d'addition a un detergent
JP3265699B2 (ja) *	1993-04-15	2002-03-11	富士通株式会社	無線通信機器のテストモードにおけるモード切替え方法

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JPS62253699A (ja) *	1986-04-09	1987-11-05	花王株式会社	高密度粒状洗剤組成物
JP2787941B2 (ja) *	1986-09-12	1998-08-20	花王株式会社	酵素含有高密度粒状洗剤組成物
JP2802450B2 (ja) *	1990-03-16	1998-09-24	ライオン株式会社	高嵩密度粒状洗剤組成物
JPH06192697A (ja) *	1992-12-25	1994-07-12	Lion Corp	高嵩密度粒状洗剤組成物
JP2954487B2 (ja) *	1994-07-13	1999-09-27	花王株式会社	非イオン性粉末洗浄剤組成物

2004
- 2004-02-04 JP JP2005504857A patent/JP4591704B2/ja not_active Expired - Fee Related
- 2004-02-04 KR KR20057014436A patent/KR101029298B1/ko active IP Right Grant
- 2004-02-04 WO PCT/JP2004/001127 patent/WO2004069970A1/ja active Application Filing
- 2004-02-04 CN CNB2004800036205A patent/CN100545254C/zh not_active Expired - Lifetime

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US4869843A (en) *	1986-01-17	1989-09-26	Kao Corporation	High-density granular detergent composition
JP3265699B2 (ja) *	1993-04-15	2002-03-11	富士通株式会社	無線通信機器のテストモードにおけるモード切替え方法
WO2000077159A1 (fr) *	1999-06-16	2000-12-21	Kao Corporation	Particules d'addition a un detergent

Also Published As

Publication number	Publication date
CN1748023A (zh)	2006-03-15
WO2004069970A1 (ja)	2004-08-19
KR101029298B1 (ko)	2011-04-18
JPWO2004069970A1 (ja)	2006-05-25
JP4591704B2 (ja)	2010-12-01
KR20050099532A (ko)	2005-10-13

Legal Events

Date	Code	Title	Description
2006-03-15	C06	Publication
2006-03-15	PB01	Publication
2006-05-10	C10	Entry into substantive examination
2006-05-10	SE01	Entry into force of request for substantive examination
2009-09-30	C14	Grant of patent or utility model
2009-09-30	GR01	Patent grant
2024-02-27	CX01	Expiry of patent term	Granted publication date: 20090930
2024-02-27	CX01	Expiry of patent term

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US7115548B1 (en)	2006-10-03	High-density detergent composition
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JP5401036B2 (ja)	2014-01-29	粒状洗剤の製造方法
JPH0762160B2 (ja)	1995-07-05	粘土を含有する高嵩密度の洗剤粉末の製造方法
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JPH0436398A (ja)	1992-02-06	高嵩密度粒状洗剤組成物
ES2226865T3 (es)	2005-04-01	Procedimiento para fabricar una composicion detergente granular.
JP4480810B2 (ja)	2010-06-16	顆粒状洗剤組成物及びその製造方法
JP2909888B2 (ja)	1999-06-23	酵素含有造粒物、その製造法及びこれを含有する洗浄剤及び漂白剤組成物
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