BR112017003122A2 - materiais zeolíticos com acentuada macroposididade no monocristal e processo para a sua produção - Google Patents

materiais zeolíticos com acentuada macroposididade no monocristal e processo para a sua produção

Info

Publication number
BR112017003122A2
BR112017003122A2 BR112017003122A BR112017003122A BR112017003122A2 BR 112017003122 A2 BR112017003122 A2 BR 112017003122A2 BR 112017003122 A BR112017003122 A BR 112017003122A BR 112017003122 A BR112017003122 A BR 112017003122A BR 112017003122 A2 BR112017003122 A2 BR 112017003122A2
Authority
BR
Brazil
Prior art keywords
production
macroposidity
marked
single crystal
zeolitic materials
Prior art date
Application number
BR112017003122A
Other languages
English (en)
Other versions
BR112017003122B1 (pt
Inventor
Gonche Fortunatus Machoke Albert
Inayat Alexandra
Maria Beltrán Custodio Ana
Spiecker Erdmann
Kruse Nadine
Güttel Robert
Schwieger Wilhelm
Original Assignee
Univ Friedrich Alexander Er
Technische Univ Clausthal
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Friedrich Alexander Er, Technische Univ Clausthal filed Critical Univ Friedrich Alexander Er
Priority to BR122020007784-0A priority Critical patent/BR122020007784B1/pt
Publication of BR112017003122A2 publication Critical patent/BR112017003122A2/pt
Publication of BR112017003122B1 publication Critical patent/BR112017003122B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/02—Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/08—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the aluminium atoms being wholly replaced
    • C01B39/085—Group IVB- metallosilicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C01B39/38—Type ZSM-5
    • C01B39/40—Type ZSM-5 using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/54—Phosphates, e.g. APO or SAPO compounds
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/34—Silicates
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/10—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C01P2006/17—Pore diameter distribution

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Metallurgy (AREA)
  • Analytical Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

a presente invenção refere-se a um material zeolítico compreendendo monocristais zeolíticos, que apresentam em cada caso um sistema de poros, que compreende pelo menos um sistema de mi-croporos e pelo menos um sistema de macroporos, bem como um processo para a produção de um tal material zeolítico, no qual partículas porosas de óxidos são convertidas no material zeolítico na presença de um gabarito orgânico e vapor de água.
BR112017003122-1A 2014-08-22 2015-08-21 Método para a produção de um material zeolítico que compreende monocristais zeolíticos BR112017003122B1 (pt)

Priority Applications (1)

Application Number Priority Date Filing Date Title
BR122020007784-0A BR122020007784B1 (pt) 2014-08-22 2015-08-21 Material zeolítico compreendendo monocristais zeolíticos

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102014012681.1 2014-08-22
DE102014012681.1A DE102014012681A1 (de) 2014-08-22 2014-08-22 Zeolithische Materialien mit ausgeprägter Makroporosität im Einzelkristall und Verfahren zu deren Herstellung
PCT/EP2015/069254 WO2016026960A1 (de) 2014-08-22 2015-08-21 Zeolithische materialien mit ausgeprägter makroporosität im einzelkristall und verfahren zu deren herstellung

Publications (2)

Publication Number Publication Date
BR112017003122A2 true BR112017003122A2 (pt) 2017-11-28
BR112017003122B1 BR112017003122B1 (pt) 2022-03-29

Family

ID=54147135

Family Applications (2)

Application Number Title Priority Date Filing Date
BR122020007784-0A BR122020007784B1 (pt) 2014-08-22 2015-08-21 Material zeolítico compreendendo monocristais zeolíticos
BR112017003122-1A BR112017003122B1 (pt) 2014-08-22 2015-08-21 Método para a produção de um material zeolítico que compreende monocristais zeolíticos

Family Applications Before (1)

Application Number Title Priority Date Filing Date
BR122020007784-0A BR122020007784B1 (pt) 2014-08-22 2015-08-21 Material zeolítico compreendendo monocristais zeolíticos

Country Status (9)

Country Link
US (1) US10301184B2 (pt)
EP (1) EP3183213A1 (pt)
JP (2) JP6724007B2 (pt)
KR (1) KR102508183B1 (pt)
CN (2) CN107074565B (pt)
BR (2) BR122020007784B1 (pt)
DE (1) DE102014012681A1 (pt)
RU (1) RU2722028C2 (pt)
WO (1) WO2016026960A1 (pt)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102014012681A1 (de) * 2014-08-22 2016-02-25 Friedrich-Alexander-Universität Erlangen - Nürnberg Zeolithische Materialien mit ausgeprägter Makroporosität im Einzelkristall und Verfahren zu deren Herstellung
DE102015016908A1 (de) 2015-12-29 2017-06-29 Friedrich-Alexander-Universität Erlangen-Nürnberg Zeolithische Partikel mit Nanometerdimensionen und Verfahren zu deren Herstellung
US11179707B2 (en) 2017-03-31 2021-11-23 Johnson Matthey Catalysts (Germany) Gmbh Composite material
GB201900484D0 (en) 2019-01-14 2019-02-27 Johnson Matthey Catalysts Germany Gmbh Iron-loaded small pore aluminosilicate zeolites and method of making metal loaded small pore aluminosilicate zeolites
KR102459932B1 (ko) * 2020-09-29 2022-10-27 서강대학교산학협력단 매크로스케일 중공구조의 mww-타입 제올라이트

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU1450409C (ru) * 1986-02-24 1995-10-27 Индивидуальное частное предприятие "Голтар" Способ получения монокристаллов цеолита (na,li)f
US5019263A (en) * 1990-06-05 1991-05-28 Mobil Oil Corp. Membrane composed of a pure molecular sieve
JP3442348B2 (ja) * 1999-06-18 2003-09-02 株式会社日本触媒 バインダーレス結晶性アルミノシリケート成型体、その製造方法およびその用途
DE60327396D1 (de) 2002-08-30 2009-06-10 Satoshi Sato Kristallines inorganisches poröses Material
JP2004143035A (ja) * 2002-08-30 2004-05-20 Tokuyama Corp 結晶性無機多孔質材料およびその製造方法
JP2005219956A (ja) * 2004-02-04 2005-08-18 Tokuyama Corp 結晶性無機多孔質材料およびその製造方法
RU2362736C1 (ru) * 2007-11-22 2009-07-27 Юоп Ллк Способ получения слоистой композиции молекулярного сита
JP5495531B2 (ja) * 2008-10-09 2014-05-21 Ｊｘ日鉱日石エネルギー株式会社 パラキシレン製造用合成ゼオライト触媒の製造方法、並びに該方法で製造したパラキシレン製造用触媒を用いた高純度パラキシレンの製造方法
JP5479147B2 (ja) * 2010-02-19 2014-04-23 株式会社トクヤマデンタル 無機酸化物の製造方法
US20120093715A1 (en) * 2010-10-19 2012-04-19 Uop Llc Monolithic zeolite structures with and without hierarchical pore structures and methods for producing the same
US20130052126A1 (en) * 2010-10-19 2013-02-28 Uop Llc Monolithic zeolite structures with and without hierarchical pore structures and methods for producing the same
DE102014012681A1 (de) * 2014-08-22 2016-02-25 Friedrich-Alexander-Universität Erlangen - Nürnberg Zeolithische Materialien mit ausgeprägter Makroporosität im Einzelkristall und Verfahren zu deren Herstellung

Also Published As

Publication number Publication date
JP6724007B2 (ja) 2020-07-15
CN111717925A (zh) 2020-09-29
JP2020158389A (ja) 2020-10-01
KR20170046712A (ko) 2017-05-02
JP2017525653A (ja) 2017-09-07
CN107074565B (zh) 2020-07-28
RU2017109385A3 (pt) 2019-02-05
BR112017003122B1 (pt) 2022-03-29
BR122020007784B1 (pt) 2022-03-22
DE102014012681A1 (de) 2016-02-25
RU2722028C2 (ru) 2020-05-26
CN107074565A (zh) 2017-08-18
US20170267537A1 (en) 2017-09-21
RU2017109385A (ru) 2018-09-24
US10301184B2 (en) 2019-05-28
EP3183213A1 (de) 2017-06-28
WO2016026960A1 (de) 2016-02-25
KR102508183B1 (ko) 2023-03-09

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B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

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