WO2022172515A1 - 鋼帯のレーザー切断方法、レーザー切断設備、冷間圧延方法、及び冷延鋼帯の製造方法 - Google Patents
鋼帯のレーザー切断方法、レーザー切断設備、冷間圧延方法、及び冷延鋼帯の製造方法 Download PDFInfo
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- WO2022172515A1 WO2022172515A1 PCT/JP2021/039400 JP2021039400W WO2022172515A1 WO 2022172515 A1 WO2022172515 A1 WO 2022172515A1 JP 2021039400 W JP2021039400 W JP 2021039400W WO 2022172515 A1 WO2022172515 A1 WO 2022172515A1
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- WIPO (PCT)
- Prior art keywords
- steel strip
- laser cutting
- cold
- laser beam
- pulsed laser
- Prior art date
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- 229910000831 Steel Inorganic materials 0.000 title claims abstract description 98
- 239000010959 steel Substances 0.000 title claims abstract description 98
- 238000003698 laser cutting Methods 0.000 title claims abstract description 50
- 238000000034 method Methods 0.000 title claims abstract description 44
- 238000005097 cold rolling Methods 0.000 title claims description 23
- 239000010960 cold rolled steel Substances 0.000 title claims description 16
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 238000005520 cutting process Methods 0.000 claims description 4
- 239000000463 material Substances 0.000 description 27
- 238000005096 rolling process Methods 0.000 description 15
- 239000000956 alloy Substances 0.000 description 12
- 238000003466 welding Methods 0.000 description 10
- 239000007789 gas Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 229910000976 Electrical steel Inorganic materials 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 238000010008 shearing Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 229910001209 Low-carbon steel Inorganic materials 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 150000004767 nitrides Chemical class 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000004080 punching Methods 0.000 description 2
- 239000002436 steel type Substances 0.000 description 2
- 238000005482 strain hardening Methods 0.000 description 2
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 238000005275 alloying Methods 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
Images
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K26/00—Working by laser beam, e.g. welding, cutting or boring
- B23K26/36—Removing material
- B23K26/38—Removing material by boring or cutting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
- B21B1/22—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
- B21B1/22—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length
- B21B1/24—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length in a continuous or semi-continuous process
- B21B1/28—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length in a continuous or semi-continuous process by cold-rolling, e.g. Steckel cold mill
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B15/00—Arrangements for performing additional metal-working operations specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K26/00—Working by laser beam, e.g. welding, cutting or boring
- B23K26/02—Positioning or observing the workpiece, e.g. with respect to the point of impact; Aligning, aiming or focusing the laser beam
- B23K26/06—Shaping the laser beam, e.g. by masks or multi-focusing
- B23K26/062—Shaping the laser beam, e.g. by masks or multi-focusing by direct control of the laser beam
- B23K26/0622—Shaping the laser beam, e.g. by masks or multi-focusing by direct control of the laser beam by shaping pulses
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K26/00—Working by laser beam, e.g. welding, cutting or boring
- B23K26/14—Working by laser beam, e.g. welding, cutting or boring using a fluid stream, e.g. a jet of gas, in conjunction with the laser beam; Nozzles therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K26/00—Working by laser beam, e.g. welding, cutting or boring
- B23K26/36—Removing material
- B23K26/40—Removing material taking account of the properties of the material involved
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B15/00—Arrangements for performing additional metal-working operations specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
- B21B15/0007—Cutting or shearing the product
- B21B2015/0021—Cutting or shearing the product in the rolling direction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B15/00—Arrangements for performing additional metal-working operations specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
- B21B2015/0092—Welding in the rolling direction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K2101/00—Articles made by soldering, welding or cutting
- B23K2101/16—Bands or sheets of indefinite length
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K2103/00—Materials to be soldered, welded or cut
- B23K2103/02—Iron or ferrous alloys
- B23K2103/04—Steel or steel alloys
Definitions
- the present invention relates to a steel strip laser cutting method, laser cutting equipment, a cold rolling method, and a cold rolled steel strip manufacturing method.
- the rear end of the preceding material preceding steel strip
- the leading end of the following material following steel strip
- the steel strip can be rolled while tension is applied over the entire length, and the thickness and shape of the front end and rear end of the steel strip can be controlled with high accuracy.
- Patent Document 1 As a notching method, for example, as described in Patent Document 1, a method of mechanically shearing a semicircular notch having no corners is generally used. However, with a semi-circular notch, the curvature of the outer edge is uniform and the width of the strip is the smallest at the weld, resulting in the maximum stress in the weld. Therefore, Patent Document 2 describes a method of forming notches using laser cutting as a method for shortening the notching time. Further, Patent Document 3 describes a laser cutting method that generates a small amount of dross (melted material during laser cutting).
- the notching method described above is not sufficiently effective when cold-rolling brittle materials such as silicon steel sheets and high-strength steel sheets and high-alloy materials that contain a large amount of Si and Mn.
- the current situation is that the breakage of the steel strip at the welded portion cannot be sufficiently suppressed.
- the present invention has been made in view of the above problems, and an object of the present invention is to provide a steel strip laser cutting method and a laser cutting method capable of suppressing breakage of the steel strip at the weld even in the case of a brittle material or a high alloy material. to provide facilities. Another object of the present invention is to provide a steel strip cold rolling method capable of stably cold-rolling a steel strip by suppressing breakage of the steel strip at the weld even in the case of a brittle material or a high-alloy material.
- Another object of the present invention is to provide a method for producing a cold-rolled steel strip that can stably produce a cold-rolled steel strip by suppressing breakage of the steel strip at the weld zone even in the case of a brittle material or a high-alloy material. to provide.
- the inventors of the present invention have found that the dross generated in the cross-section of the steel strip after being cut by laser light extends into a sharp shape by cold rolling and serves as the starting point of cracks from the ends of the steel strip in the width direction. I realized that it could be. Therefore, as a result of examining laser cutting conditions that can further suppress the generation of dross, it was found that the length of dross generated relative to the laser cutting length can be shortened by setting the ratio (duty factor) between the pulse period time and the pulse time to less than a certain value. I found
- the cold-rolled steel strip in the vicinity of the welded portion is subjected to circular hole processing near the central portion in the width direction by a puncher during welding. This drilling is carried out for the purpose of tracking the position of the welding point on the cold tandem rolling mill, but since the puncher is a punching process, the puncher's fracture surface becomes a sheared surface. Therefore, when cold rolling is performed under a high load, stress concentration occurs from the puncher fracture surface, and the steel strip breaks near the welded portion.
- the present invention was made based on the above idea and has the following features.
- the steel strip laser cutting method uses a pulsed laser beam to cut the vicinity of the joint where the trailing end of the preceding steel strip and the leading end of the succeeding steel strip are joined.
- the output of the pulsed laser light is 0.5 kw or more per 1 ms
- the diameter of the processing point of the pulsed laser light is 0.1 mm or more and less than 0.6 mm
- the ratio of the pulse period time to the rest time is 0.5 mm. 3 or more and less than 0.8.
- the section cut by the pulsed laser beam preferably includes both widthwise end surfaces of the steel strip and one or more closed cross-sectional shapes.
- Compressed air of 0.5 MPa or more is preferably used as the gas used for the pulsed laser beam.
- the steel strip laser cutting equipment is a steel strip laser cutting equipment that uses a pulsed laser beam to cut the vicinity of the joint where the trailing end of the preceding steel strip and the leading end of the succeeding steel strip are joined.
- the output of the pulsed laser light is 0.5 kw or more per 1 ms
- the diameter of the processing point of the pulsed laser light is 0.1 mm or more and less than 0.6 mm
- the ratio of the pulse period time to the pulse time is 0.5 mm. 3 or more and less than 0.8.
- the section cut by the pulsed laser beam preferably includes both widthwise end surfaces of the steel strip and one or more closed cross-sectional shapes.
- Compressed air of 0.5 MPa or more is preferably used as the gas used for the pulsed laser beam.
- the steel strip cold rolling method according to the present invention cold-rolls the steel strip cut by the steel strip laser cutting method according to the present invention.
- the method for manufacturing a cold-rolled steel strip according to the present invention manufactures a cold-rolled steel strip through steps including the method for cold-rolling a steel strip according to the present invention.
- the steel strip laser cutting method and laser cutting equipment it is possible to suppress breakage of the steel strip at the weld even in the case of a brittle material or a high-alloy material. Moreover, according to the method for cold rolling a steel strip according to the present invention, even in the case of a brittle material or a high-alloy material, the steel strip can be stably cold-rolled by suppressing breakage of the steel strip at the weld zone.
- the method for manufacturing a cold-rolled steel strip according to the present invention it is possible to stably manufacture a cold-rolled steel strip by suppressing breakage of the steel strip at the weld even in the case of a brittle material or a high-alloy material. can.
- FIG. 1 is a schematic diagram for explaining a steel strip laser cutting method according to an embodiment of the present invention.
- FIG. 2 is a diagram showing a cross-sectional image and a surface image of the test material.
- FIG. 3 is a diagram for explaining the duty factor.
- a steel strip laser cutting method, laser cutting equipment, cold rolling method, and cold rolled steel strip manufacturing method according to an embodiment of the present invention will be described below with reference to the drawings.
- the embodiments shown below are examples of devices and methods for embodying the technical idea of the present invention. not something to do.
- the drawings are schematic. Therefore, it should be noted that the relationship, ratio, etc., between the thickness and the planar dimensions are different from the actual ones, and the drawings include portions where the relationship and ratio of the dimensions are different from each other.
- FIG. 1 is a schematic diagram for explaining a steel strip laser cutting method according to one embodiment of the present invention.
- the widthwise end of the welded portion 3 between the rear end portion of the preceding steel strip 1 and the leading end portion of the following steel strip 2 is An arc-shaped notch 11 is formed by cutting using a laser beam (laser cutting) in a predetermined range of the steel strip containing.
- the notch 11 can be formed without causing work hardening at the width direction end portion of the welded portion 3 .
- the preceding steel strip 1 and the following steel strip can be used without causing breakage at the weld zone 3.
- Strip 2 can be cold rolled continuously.
- the shape of the notch 11 and the trajectory of laser cutting are not limited to the present embodiment, and the shape of the notch 11 may be other shapes such as a semicircular shape and a substantially isosceles trapezoidal shape. No problem.
- punching near the central portion in the width direction of the steel strip which has conventionally been performed by a puncher, is performed by laser cutting into a closed cross-sectional shape.
- the leading steel strip 1 is formed with the hole 12 having a closed cross-sectional shape, but the trailing steel strip 2 may be formed with the hole 12 .
- the closed cross-sectional shape, the number of cut holes, and the cutting position coordinates are not particularly limited.
- holes need not be formed if the weld point tracking method is implemented by flux leakage or other imaging methods.
- the following laboratory-scale rolling experiment was conducted. That is, a 2 mm-thick silicon steel sheet containing 3.3% by mass of Si and having both ends in the width direction cut by laser was used as a test material. Then, the test material was cold-rolled at a total rolling reduction of 50% using a rolling mill with a work roll diameter of 500 mm without applying tension.
- FIG. 2(a) is a cross-sectional image of the test material when the rolling reduction is 0%
- FIG. 2(b) is a cross-sectional image of the test material when the rolling reduction is 50%
- FIG. 2(c) is a rolling reduction of 50%.
- the surface image of the test material at the time of is shown.
- FIGS. 2(a) to 2(c) when dross remains due to poor laser cutting conditions, the dross remains even after cold rolling, and the dross develops into a sharp shape. I understand. In this experiment, no tension was applied to the test material. It is presumed to lead to fracture.
- the laser cutting conditions are such that the laser output is 0.5 kw or more per 1 ms and the diameter of the laser processing point is 0.1 mm or more and 0.6 mm so as to minimize the dross adhesion area as described above.
- the ratio (duty factor) between the pulse period time and the pulse time shown in FIG. 3 is set to 0.3 or more and less than 0.8.
- the amount of heat input increases and dross is likely to be generated.
- the amount of heat input is reduced and the steel strip cannot be cut.
- the laser processing point diameter is more preferably 0.2 to 0.3 mm, and the duty factor is more preferably 0.5 to 0.75.
- the gas used for the pulsed laser is preferably compressed air of 0.5 MPa or higher. This is because at a gas pressure of less than 0.5 MPa, the generated dross tends to remain on the cut cross section without being blown off.
- cold tandem rolling mills may be dedicated mills for silicon steel sheets or high-strength steel sheets, but they may also be dual-purpose mills for rolling low-carbon steels. In that case, there is no problem in notching low-carbon steel by laser cutting.
- both a shearing machine and a laser cutting machine may be installed side by side and used separately depending on the type of steel.
- the incidence of weld fracture was 6.0 to 10.0%, whereas in the examples, the incidence of weld fracture was 2% or less. rice field. From the above, the effectiveness of the present invention was confirmed. That is, by applying the present invention and laser cutting the vicinity of the weld between the leading steel strip and the trailing steel strip, it is possible to reduce the amount of dross generated and eliminate work hardening in the vicinity of the weld. . As a result, it is possible to suppress the occurrence of breakage of the welded portion and to achieve improvements in productivity and yield.
- a steel strip laser cutting method and laser cutting equipment capable of suppressing breakage of the steel strip at the weld even in the case of a brittle material or a high alloy material.
- a steel strip cold rolling method capable of stably performing cold rolling while suppressing breakage of the steel strip at the weld even in the case of a brittle material or a high-alloy material. can do.
- a method for producing a cold-rolled steel strip that can stably produce a cold-rolled steel strip by suppressing breakage of the steel strip at the weld even in the case of a brittle material or a high-alloy material. be able to.
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- Optics & Photonics (AREA)
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- Plasma & Fusion (AREA)
- Metal Rolling (AREA)
- Laser Beam Processing (AREA)
Abstract
Description
2 後行鋼帯
11 ノッチ
12 孔部
Claims (8)
- パルス式レーザー光を用いて先行鋼帯の後端部と後行鋼帯の先端部とを接合した接合部近傍を切断する鋼帯のレーザー切断方法であって、
前記パルス式レーザー光の出力を1msあたり0.5kw以上、前記パルス式レーザー光の加工点径を0.1mm以上0.6mm未満、パルス周期時間と休止時間との比を0.3以上0.8未満とする、鋼帯のレーザー切断方法。 - 前記パルス式レーザー光による切断部は、鋼帯の幅方向両端面と一つ以上の閉断面形状を含むこと、請求項1に記載の鋼帯のレーザー切断方法。
- 前記パルス式レーザー光に用いるガスとして0.5MPa以上の圧縮空気を用いる、請求項1又は2に記載の鋼帯のレーザー切断方法。
- パルス式レーザー光を用いて先行鋼帯の後端部と後行鋼帯の先端部とを接合した接合部近傍を切断する鋼帯のレーザー切断設備であって、
前記パルス式レーザー光の出力を1msあたり0.5kw以上、前記パルス式レーザー光の加工点径を0.1mm以上0.6mm未満、パルス周期時間とパルス時間との比を0.3以上0.8未満とする、鋼帯のレーザー切断設備。 - 前記パルス式レーザー光による切断部は、鋼帯の幅方向両端面と一つ以上の閉断面形状を含む、請求項4に記載の鋼帯のレーザー切断設備。
- 前記パルス式レーザー光に用いるガスとして0.5MPa以上の圧縮空気を用いる、請求項4又は5に記載の鋼帯のレーザー切断設備。
- 請求項1~3のうち、いずれか1項に記載の鋼帯のレーザー切断方法によって切断された鋼帯に対して冷間圧延を行う、鋼帯の冷間圧延方法。
- 請求項7に記載の鋼帯の冷間圧延方法を含む工程によって冷延鋼帯を製造する、冷延鋼帯の製造方法。
Priority Applications (5)
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CN202180092600.3A CN116897093A (zh) | 2021-02-15 | 2021-10-26 | 钢带的激光切割方法、激光切割设备、冷轧方法和冷轧钢带的制造方法 |
US18/276,488 US20240123542A1 (en) | 2021-02-15 | 2021-10-26 | Laser cutting method, laser cutting facility, and cold rolling method for steel strip, and method of manufacturing cold rolled steel strip |
EP21925762.3A EP4265368A4 (en) | 2021-02-15 | 2021-10-26 | LASER CUTTING METHOD FOR STEEL STRIP, LASER CUTTING EQUIPMENT, COLD ROLLING METHOD, AND METHOD FOR MANUFACTURING COLD ROLLED STEEL STRIP |
KR1020237027108A KR20230130699A (ko) | 2021-02-15 | 2021-10-26 | 강대의 레이저 절단 방법, 레이저 절단 설비, 냉간압연 방법 및, 냉연 강대의 제조 방법 |
MX2023009516A MX2023009516A (es) | 2021-02-15 | 2021-10-26 | Metodo de corte por laser, instalacion de corte por laser y metodo de laminacion en frio para tira de acero, y metodo de fabricacion de tira de acero laminado en frio. |
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JP2021021846A JP7363832B2 (ja) | 2021-02-15 | 2021-02-15 | 鋼帯のレーザー切断方法、レーザー切断設備、冷間圧延方法、及び冷延鋼帯の製造方法 |
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EP (1) | EP4265368A4 (ja) |
JP (1) | JP7363832B2 (ja) |
KR (1) | KR20230130699A (ja) |
CN (1) | CN116897093A (ja) |
MX (1) | MX2023009516A (ja) |
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- 2021-10-26 EP EP21925762.3A patent/EP4265368A4/en active Pending
- 2021-10-26 US US18/276,488 patent/US20240123542A1/en active Pending
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- 2021-10-26 CN CN202180092600.3A patent/CN116897093A/zh active Pending
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Publication number | Publication date |
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EP4265368A1 (en) | 2023-10-25 |
CN116897093A (zh) | 2023-10-17 |
TWI789118B (zh) | 2023-01-01 |
US20240123542A1 (en) | 2024-04-18 |
JP7363832B2 (ja) | 2023-10-18 |
TW202233341A (zh) | 2022-09-01 |
KR20230130699A (ko) | 2023-09-12 |
MX2023009516A (es) | 2023-08-24 |
JP2022124212A (ja) | 2022-08-25 |
EP4265368A4 (en) | 2024-06-19 |
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