WO2021063256A1 - 电子烟烟弹用发烟基质及其制备方法 - Google Patents

电子烟烟弹用发烟基质及其制备方法 Download PDF

Info

Publication number
WO2021063256A1
WO2021063256A1 PCT/CN2020/117713 CN2020117713W WO2021063256A1 WO 2021063256 A1 WO2021063256 A1 WO 2021063256A1 CN 2020117713 W CN2020117713 W CN 2020117713W WO 2021063256 A1 WO2021063256 A1 WO 2021063256A1
Authority
WO
WIPO (PCT)
Prior art keywords
tea
smoking
electronic cigarette
parts
cartridges according
Prior art date
Application number
PCT/CN2020/117713
Other languages
English (en)
French (fr)
Inventor
佟欣洋
刘美洲
Original Assignee
深圳市舜宝科技有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 深圳市舜宝科技有限公司 filed Critical 深圳市舜宝科技有限公司
Priority to JP2022532593A priority Critical patent/JP7440123B2/ja
Publication of WO2021063256A1 publication Critical patent/WO2021063256A1/zh

Links

Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes

Definitions

  • This application relates to the field of electronic cigarettes, and more specifically, to a smoking substrate for electronic cigarette cartridges and a preparation method.
  • Heat-not-burn e-cigarettes are electronic products that imitate traditional cigarettes. They have a similar appearance, smoke and taste to traditional cigarettes. They abandon the burning method of traditional cigarettes and replace them with heat-not-burn methods to avoid excessive consumption of tar and carbon monoxide. harmful materials.
  • Cigarette cartridges are the main consumables of electronic cigarettes.
  • the smoking matrix in the cartridge mimics the smoke and taste of traditional cigarettes.
  • One is the smoke that produces vapor smoke by atomizing e-liquid.
  • the other is a cigarette-like cartridge that heats and wraps tobacco.
  • the smoking matrix still includes shredded tobacco.
  • the tobacco is processed by heat-not-burn method to produce smoke without reaching the ignition point, and the taste is completely real smoke.
  • Taste although avoiding more tar and carbon monoxide, there are still nicotine components, which not only endanger the health of smokers, but also pollute the environment, produce second-hand smoke and other social problems that endanger public health.
  • the purpose of this application is to overcome the above-mentioned shortcomings in the prior art, and provide a new type of smoking matrix that is environmentally friendly, does not harm the human body, and can effectively replace shredded tobacco, and a preparation method thereof.
  • a smoking base for electronic cigarette cartridges which is characterized in that it contains the following components by weight: 60 ⁇ 85 parts of tea particles, 3.5 ⁇ 15 parts of tea shreds, 3 ⁇ 5 parts of tea powder, 4 ⁇ 25 parts of smoker .
  • the particle size of the tea particles is larger than the particle size of the tea powder, and through the gradient setting of the particle size, the density of the entire smoking matrix can be effectively adjusted.
  • the tea thread has the smallest density, which not only increases the binding force during mixing, but also reduces the overall density of the smoking matrix; the particle size of the tea powder is the smallest, and the greater the filling amount of the tea powder, the greater the overall density of the smoking matrix ; The smaller the particle size of the tea powder, the larger the specific surface area, and the better the degree of binding and binding amount with the smoke generating agent. The higher the amount of smoke, the higher the heat required for the release of smoke, and the slower the release, The better the smoke persistence; the greater the overall density of the smoking matrix, the greater the suction resistance; therefore, by combining the tea particles, tea threads and tea powders of different particle sizes and shapes, the suction resistance of the smoking matrix can be comprehensively adjusted. Indicators such as smoke persistence and smoke release rate.
  • the various forms of tea raw materials used in the above technical solutions can be green tea, Pu'er tea, oolong tea, black tea, and the like.
  • the stabilizer is mainly used for fixing fragrance and slowly releasing smoke to improve the durability of smoke.
  • Flavoring agents are mainly used to adjust the astringency of tea materials and increase the flavor of smoke.
  • the tea particles contains the following components by weight: 71 to 80 parts of the tea particles, 5 to 10 parts of the tea silk, 4 to 5 parts of the tea powder, 5 to 6.5 parts of the smoker, and the fragrance 4 ⁇ 5 parts of the agent and 2 ⁇ 3.5 parts of the stabilizer.
  • the preparation method of the tea particles is as follows: wet-mixing powdered tea materials with any one or more combinations of flavoring agents, stabilizers and the smoking agents, and granulating to prepare the tea particles.
  • the method for preparing the powdered tea material is: the fresh tea leaves are quenched, dried, and ground to obtain the powdered tea material.
  • the particle size of the tea particles is 20-30 mesh.
  • the preparation method of the tea shreds is as follows: the fresh tea leaves are dried, shredded, and dried to prepare the tea shreds.
  • the tea silk has a length of 1 mm to 10 mm and a width of 0.2 mm to 1.5 mm.
  • the preparation method of the tea powder is as follows: the fresh tea leaves are quenched, dried, and ground to obtain the tea powder.
  • the particle size of the tea powder is 300-2000 mesh.
  • the temperature for curing is 110°C to 130°C, and the time for curing is 30 minutes to 50 minutes.
  • the curing process is optimized.
  • the curing temperature is 115 ⁇ 130°C, and the time is 30 min ⁇ 50min to reduce the moisture content of the product one to 5% ⁇ 15%.
  • the curing temperature in the tea-making process is about 300 degrees, drying for 3 minutes, rapid dehydration, and high-temperature rapid drying is used to avoid damage to chlorophyll and loss of tea color.
  • the curing temperature is higher than that of the tea-making process.
  • the purpose is to ensure the removal of enzyme activity (more than 80 °C can cause the loss of enzyme activity), to prevent too high temperature from scorching the tea stems, affecting the tea aroma of the smoking substrate, and the purpose is to ensure the removal of the enzyme activity.
  • the smoking agent comprises any one or more combinations of propylene glycol, glycerol, triacetin and 1,3-butanediol.
  • the stabilizer comprises one or more combinations of patchouli oil, vanillin or ethanol.
  • the fragrance includes one or more of essential oils, essence gels, and essence powders.
  • the flavors of each form may include fruit flavors, herbaceous woody flavors, nut and fruit flavors, etc. Flavors, such as lemon, sweet orange, cantaloupe, grapes and other flavors, herbal woody flavors, such as mint, wormwood, epimedium, ginseng, green tea, black tea, etc., nuts and fruit core flavors, such as coffee, nuts, etc.
  • the application also discloses a method for preparing the above-mentioned smoking substrate for electronic cigarette cartridges, which is characterized in that it includes the following processes:
  • the tea particles, the tea silk, the tea powder, the smoking agent, the stabilizer, and the fragrance are mixed uniformly according to the above weight parts by wet method to obtain product one;
  • the product one is made into granules to obtain product two.
  • the product two is filled into the electronic cigarette cartridge.
  • This application uses a mixture of tea particles, tea shreds and tea powder as the smoking matrix. Compared with shredded tobacco, the smoke produced by tea products after smoking releases tea polyphenols and theophylline, which has a refreshing effect. And it does not contain harmful substances such as tar and nicotine, which is very environmentally friendly and healthy.
  • the overall density of the smoking matrix can be adjusted, and the draw resistance during smoking can be adjusted.
  • the larger the particle size of the tea particles the more the The greater the length and width, the less the filling amount of tea powder, and the smaller the suction resistance.
  • Cementing Cement fresh tea leaves at a temperature of 130°C and a cementing time of 30 minutes to reduce the moisture content of the tea material to 15%;
  • Drying Dry the above-mentioned products at 100°C for 30 minutes to reduce the moisture content to less than 5%;
  • the above-mentioned dried product is sequentially passed through coarse powder and fine powder to obtain a powdered tea material with a particle size of 300-2000 mesh.
  • S6 Granulation: Weigh 70g of propylene glycol, 80g of glycerol, 25g of essential oil, and 25g of vanillin, and mix them evenly to obtain a mixed solution. Weigh 800g of powdered tea material, spray the mixed solution while stirring, and shake to obtain The tea particles are sieved to obtain the tea particles with a particle size of 20-50 mesh.
  • Cementing Cement fresh tea leaves at a temperature of 110°C and a cementing time of 50 minutes to reduce the moisture content of the tea material to 15%;
  • Shred Cut the finished product into shreds to obtain tea silk with a length of 1mm ⁇ 10mm and a width of 0.2mm ⁇ 1.5mm;
  • Drying Drying at 110°C for 30 minutes to obtain product two, the moisture content of which is reduced to less than 5%, to obtain dried tea silk.
  • Cementing Cement fresh tea leaves at a temperature of 130°C and a cementing time of 30 minutes to reduce the moisture content of the tea material to 15%;
  • Drying Dry the above-mentioned products at 100°C for 30 minutes to reduce the moisture content to less than 5%;
  • the above-mentioned dried product is sequentially passed through coarse powder and fine powder to obtain tea powder with a particle size of 300-2000 mesh.
  • tea particles particle size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder with a particle size of 300 ⁇ 1000 mesh
  • glycerol 40g essence curd 30g
  • vanillin 15g fully mix the raw materials uniformly to obtain product one; divide product one into 0.2g by the thousandth scale / Part of the particulates, the particulates are added to the cartridges in a filling manner to obtain the smoking matrix part of each cartridge.
  • tea particles particle size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder with a particle size of 300 ⁇ 1000 mesh
  • glycerol 50g glycerol 50g
  • essence curd 40g vanillin 20g
  • tea particles particle size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder particle size 300 ⁇ 1000 mesh
  • 50g, glycerol 60g, flavor curd 45g, vanillin 30g fully mix the raw materials uniformly to obtain product one; divide product one into 0.2g by the thousandth scale / Part of the particulates, the particulates are added to the cartridges in a filling manner to obtain the smoking matrix part of each cartridge.
  • tea granules particles size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder particle size 300 ⁇ 1000 mesh
  • glycerol 65g glycerol 65g
  • flavor curd 50g vanillin 35g.
  • tea granules particles size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder particle size 300 ⁇ 1000 mesh
  • glycerol 100g
  • essence curd 30g vanillin 15g
  • tea particles particle size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder with a particle size of 300 ⁇ 1000 mesh
  • 50g, glycerol 250g, essence curd 30g, vanillin 15g fully mix the raw materials uniformly to obtain product one; divide product one into 0.2g by the thousandth scale / Part of the particulates, the particulates are added to the cartridges in a filling manner to obtain the smoking matrix part of each cartridge.
  • the tea cartridges prepared by using the smoking substrates prepared in Examples 4-9 were scored and evaluated in accordance with the evaluation method of conventional tobacco cartridges.
  • the tasters were evaluated in terms of the amount of smoke, the durability of the smoke, the resistance to smoke, and the smoke.
  • the index of taste, smoke temperature, and refreshing effect is scored, and the comprehensive score is calculated according to the score of each index. The full score of each index is 5 points. The higher the score, the better the effect.
  • the scoring results are shown in Table 1, and the raw material ratios of Examples 4-9 are shown in Table 2.
  • the test method of smoke volume is: use a smoke machine to test the smoke volume under the same suction negative pressure and suction time, and observe the smoke concentration with the naked eye. The higher the concentration, the higher the score.
  • the test method for smoke persistence is: the number of puffs that can be sustained for the same amount of smoke, the more puffs, the higher the score.
  • the test method of draw resistance is: use a special cartridge draw resistance tester, the greater the draw resistance, the higher the score.
  • the test method for smoke and taste is as follows: a blind sample test is scored by a taster.
  • test method of the flue gas temperature is as follows: use an infrared thermal imager and a thermocouple to measure the temperature of the flue gas as it exits the filter and enters the oral cavity. The higher the temperature, the lower the score.
  • the test method of refreshing effect is as follows: a sample blind test is scored by a taster.
  • Examples 5 to 7 are preferred examples, the preferred range of tea particles is 71 ⁇ 80 parts by weight, the preferred range of tea silk is 5 ⁇ 10 parts by weight, and the preferred range of tea powder It is 4 to 5 parts by weight, and the preferred range of smoke-generating agent is 5 to 6.5 parts by weight; the preferred range of stabilizer is 2 to 3.5 parts by weight, and the preferred range of flavoring agent is 4 to 5 parts by weight.
  • Example 7 has the highest comprehensive score, which is close to full marks, and is the best example.
  • tea particles particle size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder 300 ⁇ 2000 mesh
  • glycerol 40g the raw materials are fully mixed uniformly, and the product 1 is obtained; the product 1 is equally divided into 0.2g/part particles by the thousandths, and the particles are divided into
  • the filling method is added to the cartridge to obtain the smoking matrix part of each cartridge.
  • the glycerin in Example 8 is replaced with other smoke agents in the same amount, and the other smoke agents are propylene glycol, glycerol, glyceryl triacetate and 1,3-butane Any one of alcohols, or multiple combinations of propylene glycol, glycerol, and triacetin.
  • tea particles particle size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder 300 ⁇ 1000 mesh
  • the raw materials are fully mixed uniformly, and the product 1 is obtained; the product 1 is divided into 0.2g/part of particulate matter by the thousandths of the day, and the particulate matter is divided into
  • the filling method is added to the cartridge to obtain the smoking matrix part of each cartridge.
  • the glycerin in Example 9 is replaced with other smoke agents in the same amount, and the other smoke agents are propylene glycol, glycerol, glycerol triacetate and 1,3-butane Any one of alcohols, or multiple combinations of propylene glycol, glycerol, and triacetin.
  • tea particles particle size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder with a particle size of 300 ⁇ 1000 mesh
  • the raw materials are thoroughly mixed to obtain product one; the product one is divided into 0.2g/part of particulate matter by thousandths of a day.
  • the particulate matter is added to the cartridge in a filling manner to obtain the smoking matrix part of each cartridge.
  • the glycerol in the tenth embodiment is replaced by other smoke agents in the same amount, and the other smoke agents are propylene glycol, glycerol, glyceryl triacetate and 1,3-butane. Any one of alcohols, or multiple combinations of propylene glycol, glycerol, and triacetin.
  • tea particles particle size 20-50 mesh
  • tea silk length 1mm-10mm, width 0.2mm-1.5mm
  • Tea powder particle size 300 ⁇ 1000 mesh
  • propylene glycol 220g, essential oil 30g the raw materials are thoroughly mixed uniformly to obtain product one; the product one is equally divided into 0.2g/part of particulate matter by thousandths of day.
  • the particles are added to the cartridges in a filling manner to obtain the smoking matrix part of each cartridge.
  • the propylene glycol in the eleventh embodiment is replaced by the equivalent amount of other smoke agents, and the other smoke agents are propylene glycol, glycerol, triacetin and 1,3-butanediol Any one of propylene glycol, glycerol, and triacetin.
  • the same amount of other fragrances are used to replace the essential oils in the eleventh embodiment, and the other fragrances are one or more combinations of essential oils, fragrance gels, and fragrance powders.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

一种电子烟烟弹用发烟基质及其制备方法，发烟基质包含以下重量份组份：茶颗粒60～85份、茶丝3.5～15份、茶粉3～5份、发烟剂4～25份。

Description

电子烟烟弹用发烟基质及其制备方法
本申请要求于2019年9月30日提交中国专利局、申请号为201910945134.3、申请名称为“电子烟烟弹用发烟基质及其制备方法”的中国专利申请的优先权，其全部内容通过引用结合在本申请中。
技术领域
本申请涉及电子烟领域，更具体地，涉及一种电子烟烟弹用发烟基质及制备方法。
 背景技术
加热不燃烧类电子烟是一种模仿传统卷烟的电子产品，与传统卷烟有着类似的外观、烟雾、口感，摒弃传统卷烟的燃烧方式，替换为加热不燃烧方式，避免吸食过多焦油和一氧化碳等有害物质。
烟弹是电子烟的主要耗材，烟弹内的发烟基质模仿传统卷烟的烟雾和口感，目前，市面上烟弹的种类主要有两类，一类是通过雾化烟油产生蒸汽烟雾的烟弹，另一种是加热包裹烟草的类似卷烟的烟弹。
 技术问题
对于第二种通过加热不燃烧方式吸食的烟弹，其发烟基质仍然包括烟丝，通过加热不燃烧的方式处理烟草，在不达到燃点的情况下产生烟雾，口感方面就是完完全全的真烟口感，虽然避免吸食较多的焦油和一氧化碳，但是，仍然存在尼古丁成分，不仅危害烟民的身体健康，还会污染环境，产生二手烟等危害公众健康的社会问题。
 技术解决方案
本申请的目的在于克服现有技术存在的上述缺陷，提供一种绿色环保、对人体无危害、可有效替代烟丝的新型发烟基质及其制备方法。
为实现上述目的，本申请的技术方案如下：
一种电子烟烟弹用发烟基质，其特征在于，包含以下重量份组份：茶颗粒60~85份、茶丝3.5~15份、茶粉3~5份、发烟剂4~25份。所述茶颗粒的粒度大于所述茶粉的粒度，通过粒度的梯度设置，可以有效调节发烟基质整体的密度。所述茶丝密度最小，不仅增加混合时的粘合力，而且减少发烟基质整体密度；所述茶粉的粒径最小，所述茶粉的填充量越大，发烟基质整体密度越大；所述茶粉粒径越小，比表面积越大，与所述发烟剂的结合度和结合量越好，发烟量越高，烟气的释放需要的热量越高，释放越缓慢，烟气持久性越好；发烟基质整体密度越大，吸阻越大；因此，通过配伍不同粒度和形态的所述茶颗粒、茶丝和茶粉，可以综合调节发烟基质的吸阻、烟气持久性、烟气释放率等指标。
上述技术方案中使用的各种形态的茶原料可以来自绿茶、普洱茶、乌龙茶、红茶等。
优选地，还包括1.5~3.5重量份的稳定剂和/或3~5重量份的香味剂，稳定剂主要用于定香，以及缓慢释放烟气，提高烟气的持久性。香味剂主要用于调节茶材料的涩感，以及增加烟气的香味等。
优选地，包含以下重量份组份：所述茶颗粒71~80份、所述茶丝5~10份、所述茶粉4~5份、所述发烟剂5~6.5份、所述香味剂4~5份以及所述稳定剂2~3.5份。
所述茶颗粒的制备方法为：用香味剂、稳定剂以及所述发烟剂中的任意一种或多种组合湿法混合粉状茶材料，经造粒制得所述茶颗粒。优选地，所述粉状茶材料的制备方法为：将新鲜茶叶经杀青、烘干、磨粉制得所述粉状茶材料。优选地，所述茶颗粒的粒度为20~30目。
所述茶丝的制备方法为：将新鲜茶叶经杀青、切丝、烘干制得所述茶丝。优选地，所述茶丝的长度为1mm~10mm，宽度为0.2mm~1.5mm。
所述茶粉的制备方法为：将新鲜茶叶经杀青、烘干、磨粉制得所述茶粉。优选地，所述茶粉的粒度为300~2000目。
优选地，所述杀青的温度为110℃~130℃，所述杀青的时间为30min~50min。
在杀青过程中，优化杀青工艺，优选地，所述杀青的温度为115~130℃，时间为30min ~ 50min，使所述产物一的水分率降至5%~15%。通常制茶工艺中的杀青温度为300度左右，烘3分钟，快速脱水，采用高温快速烘干的方式进行，目的是避免破坏叶绿素，损失茶色，在本申请中，杀青的温度比制茶工艺低，杀青时间更长，目的是在保证去除酶活性的前提下（超过80℃即可使酶活性丧失），防止过高温度使茶梗焦化，影响发烟基质的茶香味，另外，需最大化的保留茶中的茶多酚和茶碱物质，实验证明，茶多酚和茶碱在超过140°时，其损失率急剧下降，还有，温度过高也会使茶叶香气形成的主要成分可溶性糖和氨基酸被分解，延长杀青时间的目的在于使茶充分脱水干燥，因此，本申请的杀青工艺采用低温长时间烘干的方式进行。
优选地，所述发烟剂包含丙二醇、丙三醇、三醋酸甘油酯和1,3-丁二醇中的任意一种或多种组合。
优选地，所述稳定剂包含广藿香油、香兰素或者乙醇中的一种或多种组合。
优选地，所述香味剂包括香精油、香精凝脂、香精粉末中的一种或多种状态，每种形态的香精又可以包括水果味香精、草本木本香精、坚果果核类香精等，水果味香精，如柠檬、甜橙、哈密瓜、葡萄等口味，草本木本香精，如薄荷、艾草、淫羊藿、人参、绿茶、红茶等，坚果果核类香精，如咖啡，坚果等。
本申请还公开了上述的电子烟烟弹用发烟基质的制备方法，其特征在于，包括以下过程：
将所述茶颗粒、所述茶丝、所述茶粉、所述发烟剂、所述稳定剂、所述香味剂按上述的重量份数湿法混合均匀，得产物一；
将所述产物一制成颗粒状，得产物二，将产物二填充至所述电子烟烟弹，通过调节产物二的粒度大小，可以调整发烟基质的吸阻，粒度越大，填充密度越小，吸阻越小。
 有益效果
实施本申请实施例，将具有如下有益效果：
1、本申请通过采用茶颗粒、茶丝及茶粉的混合物作为发烟基质，相比于烟丝而言，茶叶制品发烟后产生的烟雾中，释放茶多酚和茶碱，有提神效果，并且不含焦油、尼古丁等有害物质，十分环保、健康。
2、茶叶成本低廉、来源广泛，可以降低生产成本。
3、采用茶颗粒、茶丝和茶粉的不同颗粒型态的混合物作为发烟基质，可以调节发烟基质整体的密度，调节吸烟时的吸阻，茶颗粒的粒径越大、茶丝的长宽越大、茶粉的填充量越少，吸阻越小。
4、由于茶颗粒、茶丝和茶粉的粒径不同，与发烟剂的结合度不同，颗粒越大，和发烟剂的结合度越低，发烟持久性越差，不同粒径的设置，可以梯度释放烟雾，增加烟雾的持久性。
 本发明的实施方式
下面对本申请实施例的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本申请一部分实施例，而不是全部的实施例。基于本申请中的实施例，本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例，都属于本申请保护的范围。
实施例一
茶颗粒的制备
杀青：对新鲜茶叶进行杀青，杀青温度为130℃，杀青时间30min，使茶材料含水率下降至15%；
烘干：将上述杀青产物于100℃下烘干30min，使含水率降至5%以内；
磨粉：将上述烘干产物依次经过粗粉、细粉得粒度为300-2000目的粉状茶材料。
S6：造粒：分别称取丙二醇70g、丙三醇80g、香精油25g、香兰素25g，混合均匀，得混合液，称取800g粉状茶材料，边搅拌边加喷混合液，震荡得到茶颗粒，过筛得粒度为20~50目的茶颗粒。
实施例二
茶丝的制备
杀青：对新鲜茶叶进行杀青，杀青温度为110℃，杀青时间50min，使茶材料含水率下降至15%；
切丝：将杀青后产品进行切丝，得到长度为1mm~10mm，宽度为0.2mm~1.5mm的茶丝；
烘干：于110℃下烘干30min，得产物二，其含水率降至5%以内，得烘干后的茶丝。
实施例三
茶粉的制备
杀青：对新鲜茶叶进行杀青，杀青温度为130℃，杀青时间30min，使茶材料含水率下降至15%；
烘干：将上述杀青产物于100℃下烘干30min，使含水率降至5%以内；
磨粉：将上述烘干产物依次经过粗粉、细粉得粒度为300-2000目的茶粉。
实施例四
称取实施例一制得的茶颗粒（粒度20~50目）850g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）35g，实施例三制得的茶粉（粒度为300~1000目）30g，丙三醇40g，香精凝脂30g，香兰素15g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
实施例五
称取实施例一制得的茶颗粒（粒度20~50目）800g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）50g，实施例三制得的茶粉（粒度为300~1000目）40g，丙三醇50g，香精凝脂40g，香兰素20g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
实施例六
称取实施例一制得的茶颗粒（粒度20~50目）750g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）65g，实施例三制得的茶粉（粒度为300~1000目）50g，丙三醇60g，香精凝脂45g，香兰素30g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
实施例七
称取实施例一制得的茶颗粒（粒度20~50目）710g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）100g，实施例三制得的茶粉（粒度为300~1000目）40g，丙三醇65g，香精凝脂50g，香兰素35g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
实施例八
称取实施例一制得的茶颗粒（粒度20~50目）655g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）150g，实施例三制得的茶粉（粒度为300~1000目）50g，丙三醇100g，香精凝脂30g，香兰素15g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
实施例九
称取实施例一制得的茶颗粒（粒度20~50目）600g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）55g，实施例三制得的茶粉（粒度为300~1000目）50g，丙三醇250g，香精凝脂30g，香兰素15g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
实验例
对采用实施例四~九所制得的发烟基质所制备的茶烟弹按照常规烟草烟弹的品评方式进行打分评价，品评员分别从烟量、烟气持久性、吸阻、烟气及口感、烟气温度、提神效果的指标进行评分，并根据各指标的评分计算综合得分，各项指标满分为5分，分数越高表示效果越好。打分结果如表1所示，实施例四~九的各原料配比如表2所示。
其中，烟量的测试方法为：采用抽烟机测试，同等抽吸负压和抽吸时间下的烟雾产生量,肉眼观察烟气浓度，浓度越高，评分分值越高。
烟气持久性的测试方法为：同等烟量能持续的抽吸口数，口数越多，评分分值越高。
吸阻的测试方法为：采用专用烟弹吸阻测试仪，吸阻越大，评分分值越高。
烟气及口感的测试方法为：由品评员抽样盲测打分。
烟气温度的测试方法为：采用红外热成像仪及热电偶测定烟气从过滤嘴出来进入口腔时的温度，温度值越高，评分分值越低。
提神效果的测试方法为：由品评员抽样盲测打分。
综合得分21分及以上为业界公认的优质烟弹。
Figure dest_path_image001
Figure 782391dest_path_image002
从表1和表2可以看到：实施例五~七为较佳实施例，茶颗粒的优选范围为71~80重量份，茶丝的优选范围为5~10重量份，茶粉的优选范围为4~5重量份，发烟剂的优选范围为5~6.5重量份数；稳定剂的优选范围为2~3.5重量份，香味剂的优选范围为4~5重量份。
实施例七的综合得分最高，接近满分，为最佳实施例。
实施例十
称取实施例一制得的茶颗粒（粒度20~50目）600g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）35g，实施例三制得的茶粉（粒度为300~2000目）30g，丙三醇40g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
在一个优选的具体实施例中，用等量的其它发烟剂代替实施例八中的丙三醇，该其它发烟剂为丙二醇、丙三醇、三醋酸甘油酯和1,3-丁二醇中的任意一种，或丙二醇、丙三醇以及三醋酸甘油酯中的多种组合。
实施例十一
称取实施例一制得的茶颗粒（粒度20~50目）800g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）150g，实施例三制得的茶粉（粒度为300~1000目）50g，丙三醇250g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
在一个优选的具体实施例中，用等量的其它发烟剂代替实施例九中的丙三醇，该其它发烟剂为丙二醇、丙三醇、三醋酸甘油酯和1,3-丁二醇中的任意一种，或丙二醇、丙三醇以及三醋酸甘油酯中的多种组合。
实施例十二
称取实施例一制得的茶颗粒（粒度20~50目）800g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）150g，实施例三制得的茶粉（粒度为300~1000目）50g，丙三醇220g，白酒30g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
在一个优选的具体实施例中，用等量的其它发烟剂代替实施例十中的丙三醇，该其它发烟剂为丙二醇、丙三醇、三醋酸甘油酯和1,3-丁二醇中的任意一种，或丙二醇、丙三醇以及三醋酸甘油酯中的多种组合。
实施例十三
称取实施例一制得的茶颗粒（粒度20~50目）800g，实施例二制得的茶丝（长度为1mm~10mm，宽度为0.2mm~1.5mm）150g，实施例三制得的茶粉（粒度为300~1000目）50g，丙二醇220g，香精油30g，将各原料充分混合均匀，得产物一；将产物一通过千分位天平等分为0.2g/份的颗粒物，将该颗粒物以填充的方式添加至烟弹中，得每个烟弹的发烟基质部分。
在一个优选的具体实施例中，用等量的其它发烟剂代替实施例十一中的丙二醇，该其它发烟剂为丙二醇、丙三醇、三醋酸甘油酯和1,3-丁二醇中的任意一种，或丙二醇、丙三醇以及三醋酸甘油酯中的多种组合。
在一个优选的具体实施例中，用等量的其它香味剂代替实施例十一中的香精油，该其它香味剂为香精油、香精凝脂、香精粉末中的一种或多种组合。
以上所揭露的仅为本申请较佳实施例而已，当然不能以此来限定本申请之权利范围，因此依本申请权利要求所作的等同变化，仍属本申请所涵盖的保护范围。

Claims (15)

  1. 一种电子烟烟弹用发烟基质，其特征在于，包含以下重量份组份：茶颗粒60~85份、茶丝3.5~15份、茶粉3~5份以及发烟剂4~25份。
  2. 根据权利要求1所述的电子烟烟弹用发烟基质，其特征在于，还包括以下重量份组份：稳定剂1.5~3.5份和/或香味剂3~5份。
  3. 根据权利要求2所述的电子烟烟弹用发烟基质，其特征在于，包含以下重量份组份：所述茶颗粒71~80份、所述茶丝5~10份、所述茶粉4~5份、所述发烟剂5~6.5份、所述香味剂4~5份以及所述稳定剂2~3.5份。
  4. 根据权利要求1或2或3所述的电子烟烟弹用发烟基质，其特征在于，所述发烟剂包含丙二醇、丙三醇、三醋酸甘油酯和1,3-丁二醇中的任意一种或多种组合。
  5. 根据权利要求2或3所述的电子烟烟弹用发烟基质，其特征在于，所述稳定剂包含广藿香油、香兰素或者乙醇中的一种或多种组合；所述香味剂包含香精油、香精凝脂、香精粉末中的一种或多种组合。
  6. 根据权利要求1所述的电子烟烟弹用发烟基质，其特征在于，所述茶颗粒的制备方法为：用香味剂、稳定剂以及所述发烟剂中的任意一种或多种组合湿法混合粉状茶材料，经造粒制得所述茶颗粒。
  7. 根据权利要求6所述的电子烟烟弹用发烟基质，其特征在于，所述粉状茶材料的制备方法为：将新鲜茶叶经杀青、烘干、磨粉制得所述粉状茶材料。
  8. 根据权利要求1或6所述的电子烟烟弹用发烟基质，其特征在于，所述茶颗粒的粒度为20~30目。
  9. 根据权利要求1所述的电子烟烟弹用发烟基质，其特征在于，所述茶丝的制备方法为：将新鲜茶叶经杀青、切丝、烘干制得所述茶丝。
  10. 根据权利要求1或9所述的电子烟烟弹用发烟基质，其特征在于，所述茶丝的长度为1mm~10mm，宽度为0.2mm~1.5mm。
  11. 根据权利要求1所述的电子烟烟弹用发烟基质，其特征在于，所述茶粉的制备方法为：将新鲜茶叶经杀青、烘干、磨粉制得所述茶粉。
  12. 根据权利要求1或11所述的电子烟烟弹用发烟基质，其特征在于，所述茶粉的粒度为300~2000目。
  13. 根据权利要求7或9或11所述的电子烟烟弹用发烟基质，其特征在于，所述杀青的温度为110℃~130℃，所述杀青的时间为30min~50min。
  14. 根据权利要求1或2或3所述的电子烟烟弹用发烟基质，其特征在于，所述茶颗粒的粒度为20~30目；所述茶丝的长度为1mm~10mm，宽度为0.2mm~1.5mm；所述茶粉的粒度为300~2000目。
  15. 权利要求1~14任意一项所述的电子烟烟弹用发烟基质的制备方法，其特征在于，
    将所述茶颗粒、所述茶丝、所述茶粉、所述发烟剂、所述稳定剂、所述香味剂按权利要求1~14任意一项所述的重量份数湿法混合均匀，得产物一；
    将所述产物一制成颗粒状，得产物二，所述产物二填充至所述电子烟烟弹。
PCT/CN2020/117713 2019-09-30 2020-09-25 电子烟烟弹用发烟基质及其制备方法 WO2021063256A1 (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2022532593A JP7440123B2 (ja) 2019-09-30 2020-09-25 電子タバコのタバコスティック用発煙基質及びその製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN201910945134.3 2019-09-30
CN201910945134.3A CN110537725A (zh) 2019-09-30 2019-09-30 电子烟烟弹用发烟基质及制备方法

Publications (1)

Publication Number Publication Date
WO2021063256A1 true WO2021063256A1 (zh) 2021-04-08

Family

ID=68715307

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/CN2020/117713 WO2021063256A1 (zh) 2019-09-30 2020-09-25 电子烟烟弹用发烟基质及其制备方法

Country Status (3)

Country Link
JP (1) JP7440123B2 (zh)
CN (1) CN110537725A (zh)
WO (1) WO2021063256A1 (zh)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110537725A (zh) * 2019-09-30 2019-12-06 深圳市舜宝科技有限公司 电子烟烟弹用发烟基质及制备方法
CN111165869B (zh) * 2020-01-17 2021-11-05 湖南中烟工业有限责任公司 一种经低危害增烟处理的卷烟
CN113349412A (zh) * 2020-03-03 2021-09-07 常州丰源生物科技有限公司 以膨化小米作为基体的气溶胶制品用载体及其制备方法
WO2022077219A1 (zh) * 2020-10-13 2022-04-21 深圳市舜宝科技有限公司 一种组合物、制备方法及一种茶烟弹
CN112273706B (zh) * 2020-10-19 2022-08-12 深圳波顿香料有限公司 加热不燃烧烟用颗粒及其制备方法与应用
CN113229522B (zh) * 2021-06-15 2023-09-15 河南中烟工业有限责任公司 一种适用于加热不燃烧烟具的固体烟弹及制备方法
CN113180283B (zh) * 2021-06-15 2022-12-23 河南中烟工业有限责任公司 一种固体烟弹的制备方法
CN113197370A (zh) * 2021-06-15 2021-08-03 河南中烟工业有限责任公司 一种固体烟弹及制备方法
CN113475757A (zh) * 2021-06-15 2021-10-08 河南中烟工业有限责任公司 一种加热不燃烧固体烟弹
CN113576020A (zh) * 2021-08-02 2021-11-02 云南中烟工业有限责任公司 一种抽吸制品用烟雾发生材料的制备方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109090685A (zh) * 2018-10-29 2018-12-28 云南巴菰生物科技有限公司 一种加热不燃烧卷烟烟丝与由其制备的加热不燃烧卷烟
TW201904450A (zh) * 2017-06-16 2019-02-01 日商東亞產業股份有限公司 採用非煙草植物的電子煙煙彈及其製造方法
CN109393541A (zh) * 2017-08-15 2019-03-01 东莞市香草生物工程有限公司 采用非烟草植物的电子烟烟弹用填充物、及其制造方法
CN109757761A (zh) * 2019-02-01 2019-05-17 福建绿色黄金生物科技有限公司 一种茶丝的制备方法及其在制备茶烟弹中的应用
CN109757763A (zh) * 2019-02-01 2019-05-17 福建绿色黄金生物科技有限公司 一种茶叶的压片方法及其在制备茶烟弹中的应用
CN110537725A (zh) * 2019-09-30 2019-12-06 深圳市舜宝科技有限公司 电子烟烟弹用发烟基质及制备方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT508244B1 (de) 2010-03-10 2010-12-15 Helmut Dr Buchberger Inhalatorkomponente
CN105357986A (zh) * 2013-05-02 2016-02-24 Jt国际公司 可汽化材料和胶囊
CN106805288A (zh) * 2015-11-27 2017-06-09 谭海韵 一种利用普洱茶丝作为烟丝的烟制品
GB201521626D0 (en) 2015-12-08 2016-01-20 British American Tobacco Co Tobacco composition
CN106858704A (zh) * 2017-02-28 2017-06-20 梧州市雅正农业科技有限公司 六堡茶茶烟及其制备方法
CN107307466B (zh) * 2017-05-27 2018-10-12 浙江中烟工业有限责任公司 一种颗粒状加热不燃烧的烟草基体及其制备方法
CN107319630A (zh) 2017-06-16 2017-11-07 宁淑敏 复方茶烟的制备方法
JP2019076077A (ja) * 2017-10-23 2019-05-23 株式会社 東亜産業 非タバコ植物を用いた電子タバコカートリッジ用充填物の製造方法
JP6280287B1 (ja) 2017-11-02 2018-02-14 株式会社 東亜産業 タバコ植物または非タバコ植物を用いた電子タバコカートリッジおよびその支持部材
JP6861998B2 (ja) 2018-01-09 2021-04-21 株式会社東亜産業 電子タバコカートリッジ及び電子タバコカートリッジ用充填物
US11019850B2 (en) 2018-02-26 2021-06-01 Rai Strategic Holdings, Inc. Heat conducting substrate for electrically heated aerosol delivery device
CN109363230A (zh) * 2018-10-31 2019-02-22 云南恒罡科技有限公司 一种加热不燃烧卷烟发烟颗粒材质及其制备方法
JP6526929B1 (ja) 2018-10-19 2019-06-05 株式会社 東亜産業 加熱式揮発物吸引カートリッジ用被加熱芳香発生体組成物、その組成物を用いた加熱式揮発物吸引カートリッジ用被加熱芳香発生体、その被加熱芳香発生体を用いた加熱式揮発物吸引カートリッジ、及び、その加熱式揮発物吸引カートリッジ用被加熱芳香発生体の製造方法
CN110179151B (zh) 2019-07-11 2021-10-22 中国烟草总公司郑州烟草研究院 一种烘烤中烟叶初始含水率的估算方法、鲜烟叶的烘烤方法、数学模型及其构建方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201904450A (zh) * 2017-06-16 2019-02-01 日商東亞產業股份有限公司 採用非煙草植物的電子煙煙彈及其製造方法
CN109393541A (zh) * 2017-08-15 2019-03-01 东莞市香草生物工程有限公司 采用非烟草植物的电子烟烟弹用填充物、及其制造方法
CN109090685A (zh) * 2018-10-29 2018-12-28 云南巴菰生物科技有限公司 一种加热不燃烧卷烟烟丝与由其制备的加热不燃烧卷烟
CN109757761A (zh) * 2019-02-01 2019-05-17 福建绿色黄金生物科技有限公司 一种茶丝的制备方法及其在制备茶烟弹中的应用
CN109757763A (zh) * 2019-02-01 2019-05-17 福建绿色黄金生物科技有限公司 一种茶叶的压片方法及其在制备茶烟弹中的应用
CN110537725A (zh) * 2019-09-30 2019-12-06 深圳市舜宝科技有限公司 电子烟烟弹用发烟基质及制备方法

Also Published As

Publication number Publication date
CN110537725A (zh) 2019-12-06
JP7440123B2 (ja) 2024-02-28
JP2023500735A (ja) 2023-01-10

Similar Documents

Publication Publication Date Title
WO2021063256A1 (zh) 电子烟烟弹用发烟基质及其制备方法
WO2019100545A1 (zh) 低温烟及其制备方法
WO2019071910A1 (zh) 一种发烟制品及其制备方法和用途
CN107536094B (zh) 一种自然赋香的异型卷烟的制备方法
CN108576931B (zh) 烤烟风味降温调香段的原料配方、其制备方法以及加热不燃烧卷烟基础棒
CN110250565A (zh) 一种植物颗粒香珠及其制备方法与应用
CN109730355B (zh) 一种用于卷烟滤棒的增香颗粒的制备方法
CN108576932B (zh) 混合型风味降温调香段的原料配方、其制备方法以及加热不燃烧卷烟基础棒
CN104026732B (zh) 一种烟叶糯米粉复合颗粒的制备方法及其在滤嘴中的增香应用
CN108783572A (zh) 应用于低温卷烟的具有药草香的高疏松度的烟草薄片及生产工艺
CN108968139A (zh) 应用于低温卷烟的具有花香的高疏松度的烟草薄片及生产工艺
WO2020168476A1 (zh) 一种异形烟草颗粒及其制备方法、烟草制品及其制备方法
CN114762534A (zh) 一种低温缓释微晶颗粒及其制备方法和应用
CN103704883A (zh) 一种具有增香作用的天然产物粉复合颗粒的制备及在卷烟滤嘴中的应用
CN108576912A (zh) 一种应用于低温卷烟的含金属粉末的烟草薄片及其生产工艺
CN110693070A (zh) 茶梗发烟基质的制备方法
CN108652073A (zh) 一种具有多层疏松一体烟草段的低温卷烟及其制备方法
TW202033108A (zh) 吸煙替代品耗材
CN108523242A (zh) 具有药草香的疏松一体烟草段的低温卷烟及其制备方法
CN114133983A (zh) 一种增香香料、缓释型载香颗粒及其制备方法和应用
CN108741206A (zh) 具有高导热性能的疏松一体烟草段的低温卷烟及制备方法
CN108713789A (zh) 一种应用于低温卷烟的具有枣香的高疏松度的烟草薄片及其生产工艺
CN108542000B (zh) 斗烟丝风味降温调香段的原料配方、其制备方法以及加热不燃烧卷烟基础棒
CN109512015B (zh) 一种卷烟用的加热不燃烧固体香精及其制备方法
CN107663808B (zh) 一种功能性植物颗粒烟用涂层成形纸及其制备方法

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 20871239

Country of ref document: EP

Kind code of ref document: A1

NENP Non-entry into the national phase

Ref country code: DE

ENP Entry into the national phase

Ref document number: 2022532593

Country of ref document: JP

Kind code of ref document: A

122 Ep: pct application non-entry in european phase

Ref document number: 20871239

Country of ref document: EP

Kind code of ref document: A1

32PN Ep: public notification in the ep bulletin as address of the adressee cannot be established

Free format text: NOTING OF LOSS OF RIGHTS PURSUANT TO RULE 112(1) EPC DATED 18.10.2022 (EPO FORM 1205A)