WO2010128650A3 - 炭素材料及びその製造方法 - Google Patents

炭素材料及びその製造方法 Download PDF

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Publication number
WO2010128650A3
WO2010128650A3 PCT/JP2010/057725 JP2010057725W WO2010128650A3 WO 2010128650 A3 WO2010128650 A3 WO 2010128650A3 JP 2010057725 W JP2010057725 W JP 2010057725W WO 2010128650 A3 WO2010128650 A3 WO 2010128650A3
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Prior art keywords
carbon material
graphite
porous
porous carbon
graphene
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PCT/JP2010/057725
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English (en)
French (fr)
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WO2010128650A2 (ja
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一生 村松
豊田　昌宏
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株式会社インキュベーション・アライアンス
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Priority to EP10772169.8A priority Critical patent/EP2431326B1/en
Priority to JP2011512349A priority patent/JP5613662B2/ja
Priority to ES10772169.8T priority patent/ES2606284T3/es
Priority to CN201080019171.9A priority patent/CN102414125B/zh
Priority to US13/266,295 priority patent/US8883112B2/en
Priority to KR1020117026928A priority patent/KR101446638B1/ko
Publication of WO2010128650A2 publication Critical patent/WO2010128650A2/ja
Publication of WO2010128650A3 publication Critical patent/WO2010128650A3/ja
Priority to US14/504,033 priority patent/US9379385B2/en

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/20—Graphite
    • C01B32/205—Preparation
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/52—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/52—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
    • C04B35/522—Graphite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/52—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
    • C04B35/524—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite obtained from polymer precursors, e.g. glass-like carbon material
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/62645—Thermal treatment of powders or mixtures thereof other than sintering
    • C04B35/6267—Pyrolysis, carbonisation or auto-combustion reactions
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64—Burning or sintering processes
    • C04B35/645—Pressure sintering
    • C04B35/6455—Hot isostatic pressing
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/0022—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof obtained by a chemical conversion or reaction other than those relating to the setting or hardening of cement-like material or to the formation of a sol or a gel, e.g. by carbonising or pyrolysing preformed cellular materials based on polymers, organo-metallic or organo-silicon precursors
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/583—Carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • H01M4/587—Carbonaceous material, e.g. graphite-intercalation compounds or CFx for inserting or intercalating light metals
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00853—Uses not provided for elsewhere in C04B2111/00 in electrochemical cells or batteries, e.g. fuel cells
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6562—Heating rate
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/76—Crystal structural characteristics, e.g. symmetry
    • C04B2235/767—Hexagonal symmetry, e.g. beta-Si3N4, beta-Sialon, alpha-SiC or hexa-ferrites
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/77—Density
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

Abstract

【課題】　黒鉛結晶性に優れ、良好なキャリア移動度を持ち適度な空間を有する多孔質炭素材料、炭素六角網面の端部が粒子及び構造体の外表面に位置する多孔質炭素材料、グラフェン類似の剥片状黒鉛を製造する。 【解決手段】　材料中の閉気孔率、残留水素量を適切な範囲に設定した炭素材料を、熱間静水圧加圧処理することにより炭素材料中から発生する水素、炭化水素による、閉気孔を核とした黒鉛の気相成長反応を生じさせ、目的の多孔質炭素材料を安価に大量に製造する。得られた多孔質炭素材料を物理的な衝撃印加や、多孔質炭素材料をホストとする黒鉛層間化合物を生成させ引き続き急速加熱することによりグラフェン類似の黒鉛薄片を製造する。
PCT/JP2010/057725 2009-05-06 2010-05-01 炭素材料及びその製造方法 WO2010128650A2 (ja)

Priority Applications (7)

Application Number Priority Date Filing Date Title
EP10772169.8A EP2431326B1 (en) 2009-05-06 2010-05-01 Manufacturing method of a carbon material
JP2011512349A JP5613662B2 (ja) 2009-05-06 2010-05-01 炭素材料及びその製造方法
ES10772169.8T ES2606284T3 (es) 2009-05-06 2010-05-01 Método de fabricación de un material de carbono
CN201080019171.9A CN102414125B (zh) 2009-05-06 2010-05-01 碳材料及其制造方法
US13/266,295 US8883112B2 (en) 2009-05-06 2010-05-01 Carbon material and method for producing same
KR1020117026928A KR101446638B1 (ko) 2009-05-06 2010-05-01 탄소 재료 및 그 제조 방법
US14/504,033 US9379385B2 (en) 2009-05-06 2014-10-01 Carbon material and method for producing same

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2009-112404 2009-05-06
JP2009112404 2009-05-06

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US13/266,295 A-371-Of-International US8883112B2 (en) 2009-05-06 2010-05-01 Carbon material and method for producing same
US14/504,033 Continuation US9379385B2 (en) 2009-05-06 2014-10-01 Carbon material and method for producing same

Publications (2)

Publication Number Publication Date
WO2010128650A2 WO2010128650A2 (ja) 2010-11-11
WO2010128650A3 true WO2010128650A3 (ja) 2011-01-06

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US (2) US8883112B2 (ja)
EP (1) EP2431326B1 (ja)
JP (1) JP5613662B2 (ja)
KR (1) KR101446638B1 (ja)
CN (2) CN104071766B (ja)
ES (1) ES2606284T3 (ja)
HK (1) HK1197816A1 (ja)
WO (1) WO2010128650A2 (ja)

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TWI517774B (zh) * 2011-02-09 2016-01-11 創業發展聯盟技術有限公司 製造多層石墨烯被覆基板之方法
CN104246031B (zh) * 2013-04-19 2016-05-25 创业发展联盟技术有限公司 碳纤维及其制造方法
US9546294B2 (en) 2013-04-19 2017-01-17 Incubation Alliance, Inc. Carbon fiber and method for producing same
US9969618B2 (en) 2013-11-15 2018-05-15 National University Of Singapore Hot press induced formation of an ordered graphene and few layered graphene sheets
KR20150065041A (ko) * 2013-12-04 2015-06-12 (주)포스코켐텍 리튬 이차 전지용 음극 활물질, 이의 제조 방법 및 이를 포함하는 리튬 이차 전지
SG10201505268UA (en) 2014-07-03 2016-02-26 Univ Singapore Highly Dense Nano-Carbon Foam With Controlled Porosity Synthesized From Hollow Carbon Nanoparticles
CN104401984B (zh) * 2014-11-20 2017-01-18 东南大学 毫米尺度的石墨烯球及其大规模制备方法
CN105883778B (zh) * 2014-12-31 2018-07-20 国家电网公司 一种石墨烯的制备方法
CN104752703A (zh) * 2015-04-01 2015-07-01 广东烛光新能源科技有限公司 一种多孔类石墨烯及其制备方法
US9862602B1 (en) * 2017-03-27 2018-01-09 Lyten, Inc. Cracking of a process gas
RU2663165C1 (ru) * 2017-06-16 2018-08-01 федеральное государственное автономное образовательное учреждение высшего образования "Южно-Уральский государственный университет (национальный исследовательский университет)" Способ получения углеродных материалов с высоким содержанием азота
KR101835385B1 (ko) * 2017-09-29 2018-03-09 인동전자(주) 인조 흑연 분말을 이용한 열전도성 박막의 제조방법
CN108947533B (zh) * 2018-08-31 2022-02-15 万华化学集团股份有限公司 一种多孔炭材料的制备方法及得到的多孔炭材料的用途
CN109850886B (zh) * 2019-01-18 2022-07-26 华南理工大学 一种多孔状石墨材料及其制备方法与应用
JP2021004150A (ja) * 2019-06-26 2021-01-14 イビデン株式会社 炭素系複合材料
US11476463B2 (en) * 2020-08-07 2022-10-18 GM Global Technology Operations LLC Flash carbon coating on active surfaces, methods of manufacture thereof and articles comprising the same
CN112816392A (zh) * 2021-03-11 2021-05-18 厦门厦钨新能源材料股份有限公司 晶态物质的闭孔孔隙率的分析测试方法
CN115925420A (zh) * 2021-09-30 2023-04-07 燕山大学 高弹性、高密封性的多孔碳块体材料及其制备方法

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JPS63218583A (ja) * 1987-03-06 1988-09-12 東海カ−ボン株式会社 炭素質成形体の製造方法
JPH0251412A (ja) * 1988-08-15 1990-02-21 Kobe Steel Ltd 高配向性黒鉛結晶の製造方法
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JPH06212517A (ja) * 1991-07-05 1994-08-02 Nikkiso Co Ltd 黒鉛繊維およびその製造方法

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US9379385B2 (en) 2016-06-28
CN104071766A (zh) 2014-10-01
JP5613662B2 (ja) 2014-10-29
EP2431326A4 (en) 2012-12-26
US20120045384A1 (en) 2012-02-23
EP2431326A2 (en) 2012-03-21
US20150024208A1 (en) 2015-01-22
CN102414125B (zh) 2014-10-22
US8883112B2 (en) 2014-11-11
CN102414125A (zh) 2012-04-11
JPWO2010128650A1 (ja) 2012-11-01
WO2010128650A2 (ja) 2010-11-11
EP2431326B1 (en) 2016-11-02
HK1197816A1 (zh) 2015-02-18
ES2606284T3 (es) 2017-03-23
KR20120025470A (ko) 2012-03-15
CN104071766B (zh) 2016-04-13
KR101446638B1 (ko) 2014-10-02

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