WO2001053022A1 - Herstellungsverfahren für ein kantiges, rostfreies strahlmittel auf basis einer fe-cr-c-legierung - Google Patents
Herstellungsverfahren für ein kantiges, rostfreies strahlmittel auf basis einer fe-cr-c-legierung Download PDFInfo
- Publication number
- WO2001053022A1 WO2001053022A1 PCT/EP2001/000252 EP0100252W WO0153022A1 WO 2001053022 A1 WO2001053022 A1 WO 2001053022A1 EP 0100252 W EP0100252 W EP 0100252W WO 0153022 A1 WO0153022 A1 WO 0153022A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- alloy
- granulate
- blasting
- gas mixture
- chromium
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/36—Ferrous alloys, e.g. steel alloys containing chromium with more than 1.7% by weight of carbon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/14—Treatment of metallic powder
- B22F1/142—Thermal or thermo-mechanical treatment
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/0068—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for particular articles not mentioned below
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C33/00—Making ferrous alloys
- C22C33/02—Making ferrous alloys by powder metallurgy
- C22C33/0257—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements
- C22C33/0278—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements with at least one alloying element having a minimum content above 5%
- C22C33/0285—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements with at least one alloying element having a minimum content above 5% with Cr, Co, or Ni having a minimum content higher than 5%
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
- B22F2998/10—Processes characterised by the sequence of their steps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/74—Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
- C21D1/76—Adjusting the composition of the atmosphere
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D6/00—Heat treatment of ferrous alloys
- C21D6/002—Heat treatment of ferrous alloys containing Cr
Definitions
- the invention relates to a method for producing abrasive grains from rustproof stainless steel casting, in which a granulate is first produced from the melt of a hardenable iron-chromium-carbon alloy, which then undergoes a heat treatment for hardening and is subsequently broken down into sharp-edged grains.
- rusting blasting media such as steel shot or steel gravel
- rusting blasting media such as steel shot or steel gravel
- iron-containing residues on the workpiece surface. Due to the oxidation of the adhering iron residues, rust spots appear undesirably within a very short time.
- mineral abrasives such as. B. electrical corundum, silicon carbide or glass
- rust-free metallic abrasives are known. Mention should be made of cast stainless steel shot from rust-resistant steel alloys. This material has a number of advantages over mineral abrasives.
- a granulate consisting of essentially round grains is first produced from a melt of a hardenable chromium cast iron alloy. This is hardened by being quenched in water after a heat treatment at 1000 ° C to 1100 ° C. Then the grains are broken so that a sharp-edged material is formed.
- a disadvantage of this method is that the undesired oxidation of the material is promoted by quenching the steel, which is hotter than 1000 ° C., in water. Furthermore, the achievable cooling rate is severely limited when using water (vapor phase). However, effective quenching is absolutely necessary in order to obtain a material that is as brittle as possible. This is the prerequisite that the grains can later be broken so that the desired sharp-edged granules are produced.
- the object of the present invention is to provide a process for the production of rustproof abrasive in which oxidation of the granules is excluded during the hardening and breaking process steps and in which the brittleness of the material achieved by the hardening is so high that breaking of the blasting grain to sharp-edged granules is possible with simple means.
- this object is achieved in that the heat treatment at> 900 ° Celsius in reducing atmosphere follows and that a reducing gas or gas mixture is also used for the subsequent cooling.
- the reducing atmosphere is expediently a gas mixture which contains hydrogen and nitrogen.
- a gas mixture which contains 60% to 80% hydrogen and 20% to 40% nitrogen is particularly suitable for the process according to the invention. The best results were achieved with 70% hydrogen and 30% nitrogen.
- a vibrating tube mill is particularly well suited to producing the desired sharp-edged granulate from the hardened starting material.
- the blasting agent For use in the surface treatment of metallic workpieces, it is advisable for the blasting agent to be classified according to the grain size.
- a further process step for grain fractionation with which the setting of the desired grain mixture is achieved, can follow the production process according to the invention. The method according to the invention is explained in more detail below with reference to the drawing.
- the drawing shows a flow diagram of the production process, the upper part comprising the process steps for producing the starting granulate, while the lower part shows hardening, breaking and classifying.
- the starting material for the abrasive is steel scrap, which is fed to the manufacturing process from a scrap store 1.
- carbon in the form of graphite 2 and chromium 3 is added to it from suitable storage containers.
- the raw material mixture is then melted into an alloy in a melting furnace 4. This contains 2.0% carbon and 30% to 32% chromium.
- the melt passes through a atomizing device 5 at a temperature of more than 1420 ° Celsius, whereby granules with a wide range of grain diameters are formed.
- the atomized droplets of the molten metal are quenched in a water bath, so that solid granulate collects on the bottom of a granulation basin 6.
- the granulate is removed from the basin from a fume cupboard 7 and goes through the process steps of draining 8 and drying 9. After passing through cooling 10, the starting material for the rust-resistant chrome cast alloy is available.
- the starting granulate is now fed to a furnace 11, in which it is annealed at more than 900 ° Celsius in an atmosphere of hydrogen and nitrogen 13 at low pressure, after which it is conveyed into a storage container 12.
- a furnace 11 By annealing the granulate at> 900 ° C, secondary carbides are separated from the alloy-rich matrix, which changes the composition of the matrix.
- a martensite conversion is only possible through the elimination of the secondary carbides, which then leads to an increase in hardness to> 60 HRC when the granules cool down from temperatures> 900 ° C.
- the granulate is fed from the container 12 to the crusher 15 by means of a bucket elevator 14.
- the crusher 15 is preferably designed as a vibrating tube mill and comminutes the hardened, brittle granulate into sharp-edged fragments. By using such pulse mills, it is particularly easy to break down the material under strong internal stresses into sharp-edged fragments.
- the grain mixture formed during crushing has a wide size distribution.
- a screening assembly 16 is now run through for classification. Oversize 17 that is too coarse is fed back to the crusher. The undersize 18, which is too fine, is removed from the process at this point and melted in the melting furnace 4.
- Gutkorn 19 with a diameter between 0.1 and 0.8 mm is either stored in a silo 20 or added to the fine classification of a further screening plant 21. Blasting media with different grain sizes are stored in silos 22, 23 and 24 until they are removed for dispatch to the end user.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Powder Metallurgy (AREA)
- Polishing Bodies And Polishing Tools (AREA)
- Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)
- Heat Treatment Of Articles (AREA)
- Golf Clubs (AREA)
- Eyeglasses (AREA)
- Conductive Materials (AREA)
- Heat Treatment Of Steel (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
Description
Claims
Priority Applications (13)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP01942587A EP1250205B1 (de) | 2000-01-22 | 2001-01-11 | Herstellungsverfahren für ein kantiges, rostfreies strahlmittel auf basis einer fe-cr-c-legierung |
DE50100333T DE50100333D1 (de) | 2000-01-22 | 2001-01-11 | Herstellungsverfahren für ein kantiges, rostfreies strahlmittel auf basis einer fe-cr-c-legierung |
SI200120012A SI20913A (sl) | 2000-01-22 | 2001-01-11 | Postopek za pripravo ostrorobnega nerjavečega peskalnega sredstva na osnovi zlitine Fe-Cr-C |
US10/181,825 US6764557B2 (en) | 2000-01-22 | 2001-01-11 | Method for producing angular, stainless shot-blasting abrasives based on an fe-cr-c alloy |
BR0107685-0A BR0107685A (pt) | 2000-01-22 | 2001-01-11 | Processo de fabricação para um abrasivo de jato inoxidável, de arestas vivas, à base de uma liga de fe-cr-c |
DK01942587T DK1250205T3 (da) | 2000-01-22 | 2001-01-11 | Fremgangsmåde til fremstilling af kantet, rustfrit sandblæsningsmiddel på basis af en Fe-Cr-C-legering |
NZ520233A NZ520233A (en) | 2000-01-22 | 2001-01-11 | Method for producing angular, stainless shot-blasting abrasives based on an FE-CR-C alloy |
JP2001553059A JP5085826B2 (ja) | 2000-01-22 | 2001-01-11 | Fe−Cr−C合金をベースとする角をもつ錆びのないショットブラスチング研磨剤の製造方法 |
AT01942587T ATE243594T1 (de) | 2000-01-22 | 2001-01-11 | Herstellungsverfahren für ein kantiges, rostfreies strahlmittel auf basis einer fe-cr-c- legierung |
CA002397953A CA2397953C (en) | 2000-01-22 | 2001-01-11 | Method for producing angular, stainless shot-blasting abrasives based on fe-cr-c alloy |
EA200200784A EA003956B1 (ru) | 2000-01-22 | 2001-01-11 | СПОСОБ ИЗГОТОВЛЕНИЯ РЕБРИСТОГО, НЕРЖАВЕЮЩЕГО МАТЕРИАЛА ДЛЯ СТРУЙНОЙ ОБРАБОТКИ НА ОСНОВЕ Fe-Cr-C-СПЛАВА |
AU28463/01A AU769520B2 (en) | 2000-01-22 | 2001-01-11 | Method for producing angular, stainless shot-blasting abrasives based on an FE-CR-C alloy |
UA2002076045A UA73545C2 (en) | 2000-01-22 | 2001-11-01 | METHOD FOR PRODUCING RUST-TRESISTANT GRANULES WITH SHARP FACES BASED ON Fe-Cr-C ALLOY FOR SHOT-BLASTING |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10002738.5 | 2000-01-22 | ||
DE10002738A DE10002738A1 (de) | 2000-01-22 | 2000-01-22 | Herstellungsverfahren für ein kantiges, rostfreies Strahlmittel auf Basis einer Fe-Cr-C-Legierung |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2001053022A1 true WO2001053022A1 (de) | 2001-07-26 |
Family
ID=7628430
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2001/000252 WO2001053022A1 (de) | 2000-01-22 | 2001-01-11 | Herstellungsverfahren für ein kantiges, rostfreies strahlmittel auf basis einer fe-cr-c-legierung |
Country Status (20)
Country | Link |
---|---|
US (1) | US6764557B2 (de) |
EP (1) | EP1250205B1 (de) |
JP (1) | JP5085826B2 (de) |
KR (1) | KR100790097B1 (de) |
CN (1) | CN1245269C (de) |
AT (1) | ATE243594T1 (de) |
AU (1) | AU769520B2 (de) |
BR (1) | BR0107685A (de) |
CA (1) | CA2397953C (de) |
CZ (1) | CZ296109B6 (de) |
DE (2) | DE10002738A1 (de) |
DK (1) | DK1250205T3 (de) |
EA (1) | EA003956B1 (de) |
ES (1) | ES2202290T3 (de) |
NZ (1) | NZ520233A (de) |
PT (1) | PT1250205E (de) |
SI (1) | SI20913A (de) |
UA (1) | UA73545C2 (de) |
WO (1) | WO2001053022A1 (de) |
ZA (1) | ZA200205764B (de) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1314523A2 (de) * | 2001-11-27 | 2003-05-28 | Pometon S.p.a. | Verfahren zur Herstellung eines Abrasivgemisches, insbesondere für das Sägen von Marmor, und dadurch erhaltenes Produkt |
AT13691U1 (de) * | 2013-09-02 | 2014-06-15 | Plansee Se | Chrommetallpulver |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6797080B2 (en) * | 2001-07-09 | 2004-09-28 | Showa Denko Kabushiki Kaisha | Method for producing spraying material |
US20060285989A1 (en) * | 2005-06-20 | 2006-12-21 | Hoeganaes Corporation | Corrosion resistant metallurgical powder compositions, methods, and compacted articles |
CN102390044A (zh) * | 2011-10-25 | 2012-03-28 | 张铮 | 一种钢砂的制作方法 |
FR3035607B1 (fr) * | 2015-04-30 | 2017-04-28 | Saint-Gobain Centre De Rech Et D'Etudes Europeen | Procede de modification de l'aspect d'une surface |
DE112019000541T5 (de) * | 2018-01-25 | 2020-10-08 | Sintokogio, Ltd. | Schleudermaterial und Strahlverfahren |
DE102019133017A1 (de) * | 2019-12-04 | 2021-06-10 | Vulkan Inox Gmbh | Abrasiv zum Strahlschneiden |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61257775A (ja) * | 1985-05-08 | 1986-11-15 | Mitsubishi Heavy Ind Ltd | 研掃材 |
WO1992013664A1 (en) * | 1991-02-01 | 1992-08-20 | Kaufman Sydney M | Method of recycling scrap metal |
DE19815087A1 (de) * | 1998-04-06 | 1999-10-07 | Vulkan Strahltechnik Gmbh | Nichtrostendes Strahlmittel |
Family Cites Families (11)
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---|---|---|---|---|
DE2443978C3 (de) * | 1974-09-12 | 1982-04-15 | Mannesmann AG, 4000 Düsseldorf | Verfahren zum Herstellen von Eispulver |
DE2813018A1 (de) * | 1978-03-23 | 1979-10-11 | Powdrex Ltd | Verfahren zur herstellung von metallartikeln aus metallpulver |
GB2114605B (en) * | 1982-01-21 | 1985-08-07 | Davy Loewy Ltd | Annealing steel powder |
US4448746A (en) * | 1982-11-05 | 1984-05-15 | Sumitomo Metal Industries, Ltd. | Process for producing alloy steel powder |
JPS6299080A (ja) * | 1985-10-24 | 1987-05-08 | Nippon Yakin Kogyo Co Ltd | 研掃用金属粒子 |
JPH01234504A (ja) * | 1988-03-12 | 1989-09-19 | Yoshikawa Kogyo Co Ltd | 焼結用微細鉄粉の製造法 |
JPH0645801B2 (ja) * | 1989-04-17 | 1994-06-15 | 川崎製鉄株式会社 | Cr系合金鋼粉の仕上熱処理方法 |
DE4030054C2 (de) * | 1990-09-20 | 1995-11-02 | Mannesmann Ag | Verfahren und Anlage zum Reduktionsglühen von Eisenpulver |
JPH08174034A (ja) * | 1994-12-21 | 1996-07-09 | Nippon Steel Corp | Cr系ステンレス鋼板の製造方法 |
JPH09213664A (ja) * | 1996-02-07 | 1997-08-15 | Furontetsuku:Kk | 基体の処理方法及び処理装置 |
US6358298B1 (en) * | 1999-07-30 | 2002-03-19 | Quebec Metal Powders Limited | Iron-graphite composite powders and sintered articles produced therefrom |
-
2000
- 2000-01-22 DE DE10002738A patent/DE10002738A1/de not_active Withdrawn
-
2001
- 2001-01-11 JP JP2001553059A patent/JP5085826B2/ja not_active Expired - Fee Related
- 2001-01-11 DK DK01942587T patent/DK1250205T3/da active
- 2001-01-11 KR KR1020027009342A patent/KR100790097B1/ko active IP Right Grant
- 2001-01-11 WO PCT/EP2001/000252 patent/WO2001053022A1/de active IP Right Grant
- 2001-01-11 CA CA002397953A patent/CA2397953C/en not_active Expired - Lifetime
- 2001-01-11 EA EA200200784A patent/EA003956B1/ru not_active IP Right Cessation
- 2001-01-11 US US10/181,825 patent/US6764557B2/en not_active Expired - Lifetime
- 2001-01-11 AU AU28463/01A patent/AU769520B2/en not_active Expired
- 2001-01-11 PT PT01942587T patent/PT1250205E/pt unknown
- 2001-01-11 AT AT01942587T patent/ATE243594T1/de active
- 2001-01-11 CZ CZ20022532A patent/CZ296109B6/cs not_active IP Right Cessation
- 2001-01-11 DE DE50100333T patent/DE50100333D1/de not_active Expired - Lifetime
- 2001-01-11 SI SI200120012A patent/SI20913A/sl active Search and Examination
- 2001-01-11 EP EP01942587A patent/EP1250205B1/de not_active Expired - Lifetime
- 2001-01-11 BR BR0107685-0A patent/BR0107685A/pt not_active IP Right Cessation
- 2001-01-11 ES ES01942587T patent/ES2202290T3/es not_active Expired - Lifetime
- 2001-01-11 CN CNB018039774A patent/CN1245269C/zh not_active Expired - Lifetime
- 2001-01-11 NZ NZ520233A patent/NZ520233A/xx not_active IP Right Cessation
- 2001-11-01 UA UA2002076045A patent/UA73545C2/uk unknown
-
2002
- 2002-07-18 ZA ZA200205764A patent/ZA200205764B/en unknown
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61257775A (ja) * | 1985-05-08 | 1986-11-15 | Mitsubishi Heavy Ind Ltd | 研掃材 |
WO1992013664A1 (en) * | 1991-02-01 | 1992-08-20 | Kaufman Sydney M | Method of recycling scrap metal |
DE19815087A1 (de) * | 1998-04-06 | 1999-10-07 | Vulkan Strahltechnik Gmbh | Nichtrostendes Strahlmittel |
Non-Patent Citations (2)
Title |
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DATABASE WPI Derwent World Patents Index; AN 1986-343332, XP002166442 * |
PATENT ABSTRACTS OF JAPAN vol. 011, no. 114 (M - 579) 10 April 1987 (1987-04-10) * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1314523A2 (de) * | 2001-11-27 | 2003-05-28 | Pometon S.p.a. | Verfahren zur Herstellung eines Abrasivgemisches, insbesondere für das Sägen von Marmor, und dadurch erhaltenes Produkt |
EP1314523A3 (de) * | 2001-11-27 | 2004-05-06 | Pometon S.p.a. | Verfahren zur Herstellung eines Abrasivgemisches, insbesondere für das Sägen von Marmor, und dadurch erhaltenes Produkt |
AT13691U1 (de) * | 2013-09-02 | 2014-06-15 | Plansee Se | Chrommetallpulver |
US11117188B2 (en) | 2013-09-02 | 2021-09-14 | Plansee Se | Chromium metal powder |
Also Published As
Publication number | Publication date |
---|---|
ZA200205764B (en) | 2003-11-04 |
AU2846301A (en) | 2001-07-31 |
ES2202290T3 (es) | 2004-04-01 |
DE10002738A1 (de) | 2001-07-26 |
US6764557B2 (en) | 2004-07-20 |
AU769520B2 (en) | 2004-01-29 |
JP5085826B2 (ja) | 2012-11-28 |
UA73545C2 (en) | 2005-08-15 |
BR0107685A (pt) | 2002-11-19 |
US20030136224A1 (en) | 2003-07-24 |
PT1250205E (pt) | 2003-11-28 |
DE50100333D1 (de) | 2003-07-31 |
CN1245269C (zh) | 2006-03-15 |
EP1250205A1 (de) | 2002-10-23 |
CN1422194A (zh) | 2003-06-04 |
CA2397953C (en) | 2009-11-10 |
ATE243594T1 (de) | 2003-07-15 |
EA200200784A1 (ru) | 2003-02-27 |
NZ520233A (en) | 2004-12-24 |
CZ296109B6 (cs) | 2006-01-11 |
EP1250205B1 (de) | 2003-06-25 |
CA2397953A1 (en) | 2001-07-26 |
SI20913A (sl) | 2002-12-31 |
KR100790097B1 (ko) | 2007-12-31 |
EA003956B1 (ru) | 2003-10-30 |
JP2003524690A (ja) | 2003-08-19 |
DK1250205T3 (da) | 2003-09-29 |
CZ20022532A3 (cs) | 2003-01-15 |
KR20020080380A (ko) | 2002-10-23 |
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