UA106915C2 - Спосіб розділення, виділення та очистки дикарбонових кислот - Google Patents

Спосіб розділення, виділення та очистки дикарбонових кислот

Info

Publication number
UA106915C2
UA106915C2 UAA201213967A UAA201213967A UA106915C2 UA 106915 C2 UA106915 C2 UA 106915C2 UA A201213967 A UAA201213967 A UA A201213967A UA A201213967 A UAA201213967 A UA A201213967A UA 106915 C2 UA106915 C2 UA 106915C2
Authority
UA
Ukraine
Prior art keywords
dicarboxylic acid
isolating
biomass
purifying
removal
Prior art date
Application number
UAA201213967A
Other languages
English (en)
Russian (ru)
Inventor
Вольфґанґ Тетз
Йоакім Шульз
Original Assignee
Тіссенкрупп Уде Ґмбг
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Тіссенкрупп Уде Ґмбг filed Critical Тіссенкрупп Уде Ґмбг
Publication of UA106915C2 publication Critical patent/UA106915C2/uk

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C55/00—Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
    • C07C55/02—Dicarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C55/00—Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
    • C07C55/02—Dicarboxylic acids
    • C07C55/10—Succinic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C55/00—Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
    • C07C55/02—Dicarboxylic acids
    • C07C55/14—Adipic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/13—Dicarboxylic acids
    • C07C57/145—Maleic acid
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/44—Polycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/44—Polycarboxylic acids
    • C12P7/46—Dicarboxylic acids having four or less carbon atoms, e.g. fumaric acid, maleic acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Biotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

Спосіб розділення, виділення та очистки дикарбонової кислоти з ферментаційного середовища, що включає наступні стадії: a) відокремлення біомаси та будь-яких твердих речовин, які присутні в ферментаційному середовищі, в два послідовних етапи; b) виділення розчину дикарбонової кислоти з ферментаційного середовища вільного від біомаси за допомогою хроматографії з псевдорухомим шаром; c) глибоке очищення розчину дикарбонової кислоти; d) багатоступінчате випаровування та кристалізацію; e) відокремлення та сушіння кристалів.
UAA201213967A 2010-06-25 2011-05-31 Спосіб розділення, виділення та очистки дикарбонових кислот UA106915C2 (uk)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102010025167A DE102010025167A1 (de) 2010-06-25 2010-06-25 Verfahren zur Abtrennung, Gewinnung und Reinigung von Bernsteinsäure
PCT/EP2011/002686 WO2011160760A1 (de) 2010-06-25 2011-05-31 Verfahren zur abtrennung, gewinnung und reinigung von dicarbonsäuren

Publications (1)

Publication Number Publication Date
UA106915C2 true UA106915C2 (uk) 2014-10-27

Family

ID=44511834

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA201213967A UA106915C2 (uk) 2010-06-25 2011-05-31 Спосіб розділення, виділення та очистки дикарбонових кислот

Country Status (15)

Country Link
US (1) US8957249B2 (uk)
EP (1) EP2585429B1 (uk)
JP (1) JP5862978B2 (uk)
KR (1) KR101828634B1 (uk)
CN (1) CN102958893B (uk)
AU (1) AU2011269353B2 (uk)
CA (1) CA2802951C (uk)
CO (1) CO6650355A2 (uk)
DE (1) DE102010025167A1 (uk)
ES (1) ES2646439T3 (uk)
MX (1) MX343617B (uk)
MY (1) MY161384A (uk)
UA (1) UA106915C2 (uk)
WO (1) WO2011160760A1 (uk)
ZA (1) ZA201300606B (uk)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
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MX358585B (es) 2012-05-07 2018-08-27 Archer Daniels Midland Co Purificación del ácido succínico.
DE102013000027A1 (de) 2013-01-03 2014-07-03 Thyssenkrupp Industrial Solutions Ag Verfahren zur Aufreinigung von Carbonsäuren aus Fermentationsbrühen
CN103497100A (zh) * 2013-09-23 2014-01-08 中国石油化工股份有限公司 长链二元酸水相双阶段提纯方法
CN103508877B (zh) * 2013-10-15 2016-09-14 济南华明生物科技有限公司 衣康酸节能型四效浓缩结晶的方法及装置
TW201610164A (zh) * 2013-12-06 2016-03-16 麥瑞安公司 製備琥珀酸及琥珀酸酯之方法
TW201538477A (zh) 2013-12-06 2015-10-16 Myriant Corp 製備丁二酸酯之方法
DE102014213637A1 (de) 2014-07-14 2016-01-14 Thyssenkrupp Ag Verfahren und Vorrichtung zur Aufkonzentration und Kristallisation von fermentierbaren Carbonsäuren
CN107207398A (zh) * 2014-09-02 2017-09-26 英威达技术有限责任公司 长链二酸的提纯
US9452968B1 (en) 2015-04-22 2016-09-27 Orochem Technologies, Inc. Separation of adipic acid and dodecanedioic acid from corresponding monoacid and hydroxy acid
EP3098880B1 (en) 2015-05-27 2019-02-27 Samsung Electronics Co., Ltd. Separator including microbial cellulose, method of producing the separator, and use of the separator
DE102015216815A1 (de) 2015-09-02 2017-03-02 Thyssenkrupp Ag Verfahren und Anlage zur Gewinnung einer in einem Fermentationsprozess hergestellten Carbonsäure
DE102016119938A1 (de) * 2016-10-19 2018-04-19 Thyssenkrupp Ag Reinigung und Konzentrierung von Carbonsäuren aus Fermentationsprozessen
DE102016220662A1 (de) 2016-10-21 2018-04-26 Thyssenkrupp Ag Verfahren zur Herstellung wenigstens einer hydrierten Verbindung aus einem Carbonsäurederivat
US11453636B2 (en) * 2017-06-22 2022-09-27 Archer Daniels Midland Company Process for separation and purification of a dicarboxylic acid containing mixture
CN107382706B (zh) * 2017-07-27 2019-09-03 江南大学 一种从发酵液中提取己二酸的方法
CN111592454B (zh) * 2019-02-21 2023-08-08 上海凯赛生物技术股份有限公司 二元酸胺盐的制备方法、二元酸胺盐溶液、二元酸胺盐和聚合物
US11999689B2 (en) 2019-12-19 2024-06-04 Cathay Biotech Inc. Method and system for extracting long chain dicarboxylic acid
CN111138272A (zh) 2019-12-19 2020-05-12 上海凯赛生物技术股份有限公司 一种长链二元酸的提取方法及***
US11806670B2 (en) 2019-12-19 2023-11-07 Cathay Biotech Inc. Method and system for extracting long chain dicarboxylic acid
CN111138273A (zh) * 2019-12-24 2020-05-12 上海凯赛生物技术股份有限公司 一种长链二元酸的精制工艺及***
US12017182B2 (en) 2019-12-24 2024-06-25 Cathay Biotech Inc. Method and system for refining long chain dicarboxylic acid

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US5168055A (en) 1986-06-11 1992-12-01 Rathin Datta Fermentation and purification process for succinic acid
US5143834A (en) 1986-06-11 1992-09-01 Glassner David A Process for the production and purification of succinic acid
JP2535962B2 (ja) * 1987-10-15 1996-09-18 住友化学工業株式会社 有機酸の回収方法
US5177008A (en) * 1987-12-22 1993-01-05 Kampen Willem H Process for manufacturing ethanol and for recovering glycerol, succinic acid, lactic acid, betaine, potassium sulfate, and free flowing distiller's dry grain and solubles or a solid fertilizer therefrom
US5034105A (en) 1989-07-27 1991-07-23 Michigan Biotechnology Institute Carboxylic acid purification and crystallization process
JPH0779927B2 (ja) * 1992-05-22 1995-08-30 川崎重工業株式会社 擬似移動床式液体クロマトオリゴ糖分離装置
JPH08176133A (ja) * 1994-12-26 1996-07-09 Takeda Chem Ind Ltd Ｌ−アスコルビン酸の精製法
FI962204A0 (fi) * 1996-05-24 1996-05-24 Cultor Oy Foerfarande foer fraktionering av en loesning
US5958744A (en) 1997-08-18 1999-09-28 Applied Carbochemicals Succinic acid production and purification
EP1059975A4 (en) * 1998-03-02 2003-04-23 Michigan Biotech Inst PURIFICATION OF ORGANIC ACIDS WITH ANIONIC REPLACEMENT CHROMATOGRAPHY
US6291708B1 (en) 1999-04-28 2001-09-18 A.E. Staley Manufacturing Co. Process for production of organic acids and esters thereof
DE19939630C2 (de) 1999-08-20 2001-07-12 Mg Technologies Ag Verfahren zum Feinreinigen einer wässrigen Lösung, die eine fermentativ hergestellte organische Säure enthält
JP4631706B2 (ja) * 2003-09-30 2011-02-16 味の素株式会社 発酵液からのコハク酸の精製方法
DE102004026152A1 (de) 2004-05-28 2005-12-15 Basf Ag Fermentative Herstellung von Feinchemikalien
JP2006328380A (ja) * 2005-04-26 2006-12-07 Mitsubishi Chemicals Corp ポリエステルの製造方法
CN101186571A (zh) * 2007-11-30 2008-05-28 江南大学 一种从衣康酸发酵液或衣康酸产品母液中提纯衣康酸的方法
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WO2011082378A2 (en) * 2009-12-31 2011-07-07 Myriant Technologies Llc Purification of succinic acid from the fermentation broth containing ammonium succinate

Also Published As

Publication number Publication date
ES2646439T3 (es) 2017-12-13
WO2011160760A1 (de) 2011-12-29
CO6650355A2 (es) 2013-04-15
CA2802951C (en) 2018-08-28
EP2585429B1 (de) 2017-08-09
CN102958893B (zh) 2015-07-15
MX343617B (es) 2016-11-14
AU2011269353B2 (en) 2015-04-02
CN102958893A (zh) 2013-03-06
AU2011269353A1 (en) 2013-01-10
DE102010025167A1 (de) 2011-12-29
US20130096343A1 (en) 2013-04-18
MY161384A (en) 2017-04-14
EP2585429A1 (de) 2013-05-01
US8957249B2 (en) 2015-02-17
CA2802951A1 (en) 2011-12-29
KR20130137119A (ko) 2013-12-16
ZA201300606B (en) 2014-03-26
KR101828634B1 (ko) 2018-02-12
JP5862978B2 (ja) 2016-02-16
MX2012015248A (es) 2013-10-01
JP2013529603A (ja) 2013-07-22

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