MX9302923A - Proceso para fabricar gel inorganica y producto obtenido mediante el mismo. - Google Patents

Proceso para fabricar gel inorganica y producto obtenido mediante el mismo.

Info

Publication number
MX9302923A
MX9302923A MX9302923A MX9302923A MX9302923A MX 9302923 A MX9302923 A MX 9302923A MX 9302923 A MX9302923 A MX 9302923A MX 9302923 A MX9302923 A MX 9302923A MX 9302923 A MX9302923 A MX 9302923A
Authority
MX
Mexico
Prior art keywords
same
product obtained
pore size
inorganic gel
gels
Prior art date
Application number
MX9302923A
Other languages
English (en)
Inventor
Kenneth George Sharp
Original Assignee
E I Du Pont De Neumours And Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by E I Du Pont De Neumours And Co filed Critical E I Du Pont De Neumours And Co
Publication of MX9302923A publication Critical patent/MX9302923A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/16—Preparation of silica xerogels
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
    • C03C1/006—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels to produce glass through wet route
    • C03C1/008—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels to produce glass through wet route for the production of films or coatings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/32—Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of elements or compounds in the liquid or solid state or in non-aqueous solution, e.g. sol-gel process
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/16—Preparation of silica xerogels
    • C01B33/163—Preparation of silica xerogels by hydrolysis of organosilicon compounds, e.g. ethyl orthosilicate
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C01P2006/17—Pore diameter distribution

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Silicon Compounds (AREA)
  • Silicon Polymers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Se describe un proceso para fabricar geles inorgánicos mediante la reacción de tetraalcoxiortosilicatos, tetraalcoxititanatos y tetraalcoxizirconatos con ácidos carboxílicos fuertes. Inicialmente no necesita estar presente el agua como reactivo. Por lo tanto se producen geles inorgánicos ópticamente claros, de tamaño de poro muy pequeño, de distribución de tamaño de poro estrecha, y con un área superficial específica elevada útiles para revestimientos resistentes a la abrasión, aplicaciones ópticas, soportes para catalizadores o enzimas, separación de gases o empaques cromatográficos.
MX9302923A 1992-05-20 1993-05-19 Proceso para fabricar gel inorganica y producto obtenido mediante el mismo. MX9302923A (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US88579392A 1992-05-20 1992-05-20

Publications (1)

Publication Number Publication Date
MX9302923A true MX9302923A (es) 1994-02-28

Family

ID=25387714

Family Applications (1)

Application Number Title Priority Date Filing Date
MX9302923A MX9302923A (es) 1992-05-20 1993-05-19 Proceso para fabricar gel inorganica y producto obtenido mediante el mismo.

Country Status (8)

Country Link
US (2) US5441718A (es)
EP (1) EP0641290B1 (es)
JP (1) JP3314935B2 (es)
KR (1) KR100229829B1 (es)
CA (1) CA2135875A1 (es)
DE (1) DE69304695T2 (es)
MX (1) MX9302923A (es)
WO (1) WO1993023333A1 (es)

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KR100229829B1 (ko) * 1992-05-20 1999-11-15 미리암디. 메코너헤이 무기질 겔의 제조방법
US5378790A (en) * 1992-09-16 1995-01-03 E. I. Du Pont De Nemours & Co. Single component inorganic/organic network materials and precursors thereof
US5372796A (en) * 1993-04-13 1994-12-13 Southwest Research Institute Metal oxide-polymer composites
DE4429533A1 (de) * 1994-08-19 1996-02-22 Cerdec Ag Wasser- und hydroxylgruppenfreie Gele und Xerogele, Verfahren zu deren Herstellung und deren Verwendung
ES2119473T3 (es) * 1994-09-22 1998-10-01 Hoffmann La Roche Catalizadores heterogeneos.
US5876686A (en) * 1995-06-28 1999-03-02 E. I. Du Pont De Nemours And Company Process for making inorganic oxide gels in fluorocarbon solvents
DE19619638A1 (de) * 1996-05-15 1997-11-20 Basf Ag Verfahren zur Herstellung von pulverförmigem Zirkondioxid
US6071486A (en) * 1997-04-09 2000-06-06 Cabot Corporation Process for producing metal oxide and organo-metal oxide compositions
US6172120B1 (en) 1997-04-09 2001-01-09 Cabot Corporation Process for producing low density gel compositions
US6315971B1 (en) 1997-04-09 2001-11-13 Cabot Corporation Process for producing low density gel compositions
US6090965A (en) * 1998-04-02 2000-07-18 Osi Specialties, Inc. Removal of dissolved silicates from alcohol-silicon direct synthesis solvents
US6514454B1 (en) 1998-10-07 2003-02-04 Yazaki Corporation Sol-gel process using porous mold
US6258864B1 (en) 1999-01-20 2001-07-10 Cabot Corporation Polymer foam containing chemically modified carbonaceous filler
US6586501B1 (en) 1999-01-20 2003-07-01 Cabot Corporation Aggregates having attached polymer groups and polymer foams
US6686035B2 (en) 1999-02-05 2004-02-03 Waters Investments Limited Porous inorganic/organic hybrid particles for chromatographic separations and process for their preparation
US6166237A (en) * 1999-08-13 2000-12-26 Crompton Corporation Removal of dissolved silicates from alcohol-silicon direct synthesis solvents
US6376590B2 (en) * 1999-10-28 2002-04-23 3M Innovative Properties Company Zirconia sol, process of making and composite material
US6730156B1 (en) 1999-10-28 2004-05-04 3M Innovative Properties Company Clustered particle dental fillers
US6572693B1 (en) 1999-10-28 2003-06-03 3M Innovative Properties Company Aesthetic dental materials
US6387981B1 (en) 1999-10-28 2002-05-14 3M Innovative Properties Company Radiopaque dental materials with nano-sized particles
FR2813393B1 (fr) * 2000-08-22 2002-10-18 Commissariat Energie Atomique Fabrication d'un capteur chimique a fibre optique comprenant un indicateur colore, utilisable notamment pour la mesure de l'acidite nitrique
US6528167B2 (en) * 2001-01-31 2003-03-04 Waters Investments Limited Porous hybrid particles with organic groups removed from the surface
WO2003014450A1 (en) * 2001-08-09 2003-02-20 Waters Investments Limited Porous inorganic/organic hybrid monolith materials for chromatographic separations and process for their preparation
US6965006B2 (en) * 2002-04-10 2005-11-15 Rpo Pty Ltd. Metal alkoxide polymers
US6998102B2 (en) * 2002-09-23 2006-02-14 The Regents Of The University Of California Rapid process for producing transparent, monolithic porous glass
AU2003285121A1 (en) * 2002-10-30 2004-06-07 Waters Investments Limited Porous inorganic/organic hybrid materials and preparation thereof
US20040215139A1 (en) * 2002-12-20 2004-10-28 Todd Cohen Apparatus and method for implanting left ventricular pacing leads within the coronary sinus
GR1004545B (el) * 2003-04-21 2004-04-30 Ηλιακη φωτοηλεκτροχημικη κυψελιδα παρασκευαζομενη απο συνθετα οργανικα/ανοργανα νανοδομημενα υλικα
DE112005000269T5 (de) * 2004-02-17 2007-01-25 Waters Investments Ltd., New Castle Poröse Hybridmonolithmaterialien mit von der Oberfläche entfernten organischen Gruppen
JP4513952B2 (ja) * 2004-04-21 2010-07-28 株式会社豊田中央研究所 多孔体の製造方法
DE112005001838B4 (de) 2004-07-30 2018-11-29 Waters Technologies Corp. (N.D.Ges.D. Staates Delaware) Poröse anorganische/organische Hybridmaterialien mit geordneten Domänen für chromatographische Auftrennungen, Verfahren für deren Herstellung sowie Auftrennvorrichtung und chromatographische Säule
US10773186B2 (en) 2004-07-30 2020-09-15 Waters Technologies Corporation Porous inorganic/organic hybrid materials with ordered domains for chromatographic separations and processes for their preparation
CN101610749B (zh) 2006-12-28 2013-01-02 3M创新有限公司 牙科填料及方法
US8697765B2 (en) 2007-01-12 2014-04-15 Waters Technologies Corporation Porous carbon-heteroatom-silicon hybrid inorganic/organic materials for chromatographic separations and process for the preparation thereof
US11439977B2 (en) 2009-06-01 2022-09-13 Waters Technologies Corporation Hybrid material for chromatographic separations comprising a superficially porous core and a surrounding material
WO2010141426A1 (en) 2009-06-01 2010-12-09 Waters Technologies Corporation Hybrid material for chromatographic separations
US8197782B2 (en) 2010-02-08 2012-06-12 Momentive Performance Materials Method for making high purity metal oxide particles and materials made thereof
US9249028B2 (en) 2010-02-08 2016-02-02 Momentive Performance Materials Inc. Method for making high purity metal oxide particles and materials made thereof
WO2012018598A1 (en) 2010-07-26 2012-02-09 Waters Technologies Corporation Superficially porous materials comprising a substantially nonporous core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations
JP5908800B2 (ja) * 2012-06-12 2016-04-26 国立大学法人岐阜大学 ムライト前駆体ゾル及びムライトの製造方法
EP3426388A1 (en) 2016-03-06 2019-01-16 Waters Technologies Corporation Superficially porous materials comprising a coated core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations

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SU865791A1 (ru) * 1978-08-11 1981-09-23 Ордена Ленина Институт Общей И Неорганический Химии Им. Н.С.Курнакова Ан Ссср Способ получени сферического силикагел
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Also Published As

Publication number Publication date
KR950701600A (ko) 1995-04-28
US5558849A (en) 1996-09-24
KR100229829B1 (ko) 1999-11-15
WO1993023333A1 (en) 1993-11-25
EP0641290A1 (en) 1995-03-08
CA2135875A1 (en) 1993-11-25
JP3314935B2 (ja) 2002-08-19
DE69304695T2 (de) 1997-03-20
DE69304695D1 (de) 1996-10-17
US5441718A (en) 1995-08-15
JPH07507991A (ja) 1995-09-07
EP0641290B1 (en) 1996-09-11

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Legal Events

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