KR870007151A - 2-옥소-1,3-디옥솔란의 제조방법 - Google Patents
2-옥소-1,3-디옥솔란의 제조방법 Download PDFInfo
- Publication number
- KR870007151A KR870007151A KR870000137A KR870000137A KR870007151A KR 870007151 A KR870007151 A KR 870007151A KR 870000137 A KR870000137 A KR 870000137A KR 870000137 A KR870000137 A KR 870000137A KR 870007151 A KR870007151 A KR 870007151A
- Authority
- KR
- South Korea
- Prior art keywords
- group
- ether
- weight
- delglycol
- epoxy
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D317/34—Oxygen atoms
- C07D317/36—Alkylene carbonates; Substituted alkylene carbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/14—Polycondensates modified by chemical after-treatment
- C08G59/1405—Polycondensates modified by chemical after-treatment with inorganic compounds
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Epoxy Compounds (AREA)
- Epoxy Resins (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Polyurethanes Or Polyureas (AREA)
- Plural Heterocyclic Compounds (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (10)
- 에폭사이드를 알칼리 요다이드의 존재하에 이산화탄소와 반응시켜 2-옥소-1,3-디옥솔란을 제조하는 방법에 있어서, 적어도 하나의 에폭시 화합물을 불활성 용매를 사용하거나 사용하지 않고 상압 또는 약간 상승된 압력하에 이산화탄소를 도입시키면서 40내지 180℃의 온도에서, (A)적어도 하나의 알칼리 요다이드 및 (B) 폴리올과 다음 일반식(Ba) 및 (Bb)의 폴리에테르 또는 에테르로 이루어진 화합물 적어도 하나의 혼합물과 반응시키거나, 에폭시 화합물이 이미 화합물(Ba) 및 (Bb)의 구조적 특징을 갖고 있다면 알칼리 요다이드 (A)와 만 반응시켜 상응하는 유기 카보네이트를 생성시킴을 특징으로 하는 방법.상기식에서,R은 동일하거나 다르며, 각각의 경우에 알킬그룹의 탄소수가 1내지 10개인 알킬 또는 아르알킬, 또는 아릴이고 ;R1및 R2는 동일하거나 다르며, 각각 독립적으로 수소, 또는 탄소수 1 내지 10의 알킬이고 ;R3는 R과 동일하지만, 또한 수소일 수도 있다.
- 제 1 항에 있어서, 1 내지 10바아, 바람직하게는 1 내지 5 바아, 특히 바람직하게는 1 내지 3바아의 압력을 사용하는 방법.
- 제 1 항 또는 2항에 있어서, 알칼리 요다이드로서 요드화 칼륨 또는 요드화나트륨을 에폭시 성분에 대해 0.01내지 1중량%, 바람직하게는 0.05내지 1중량%, 특히 바람직하게는 0.05내지 0.5중량%의 양으로 사용하는 방법.
- 제 1 항에 있어서, 디-, 트리-또는 폴리-글리콜, 또는 모노-및/또는 디에테르를 폴리올(Ba) 또는 에테르(Bb)로서 사용하는 방법.
- 제 4 항에 있어서, 디에틸렌, 트리에틸렌, 테트라에틸렌 및 디프로필렌글리콜, 에틸렌글리콜 모노메틸 및 모노부틸에테르, 디메톡시에탄, 디에틸델글리콜모노메틸 및 모노부틸에테르, 디에틸델글리콜디메틸 및 디에틸에테르, 트리에틸델글리콜모노메틸 및 디메틸 에테르, 프로필델글리콜모노부틸에테르, 및 에틸델프로필델글리콜모노부틸에테르를 사용하는 방법.
- 제 1 항에 있어서, 화합물(Ba) 및 (Bb)를 에폭시 성분에 대해 1내지 95중량%, 바람직하게는 1내지 50중량%, 특히 바람직하게는 10내지 30중량%의 양으로 사용하는 방법.
- 제 1 항에 있어서, 에폭시 화합물의 반응을 이산화탄소에 의해 부분적으로만 수행하는 방법.
- 제 1 항에 있어서, 적어도 하나의 말단 에폭시 그룹을 함유하며, 적어도 6개의 탄소원자를 갖는 지방족 에폭사이드, 또는 일반식(2)의 글리시돌 또는 에피할로 히드린인 에폭시 화합물, 평균적으로 적어도 하나의 일반식(3)의 치환되거나 비치환된 글리시딜 에테르그룹 또는 일반식(4)의 치환되거나 비치환된 글리시딜 에스테르 그룹을 함유하는 에폭시 화합물, 에폭시화 다중불포화 화합물, 또는 아미드 또는 우레탄 그룹을 함유하는 에폭사이드를 반응시키는 방법.상기식에서,Z는 수소원자, 메틸그룹 또는 에틸그룹이고,X는 할로겐원자 또는 OH 그룹이다.
- 제 8 항에 있어서, (폴리)글리시딜 에테르, 말단 에폭시그룹을 갖는 가소화 에폭시 수지, 또는 포화 또는 에틸렌성 불포화(폴리)카복실산의 글리시딜 에스테르를 반응시키는 방법.
- 우레탄 그룹을 함유하는 합성 수지를 피복물 또는 성형체의 형태로 제조하기 위한, 제 1 항 내지 9항중의 어느 한 항의 방법에 따라 수득된 2-옥소-1,3-디옥솔란의 용도.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEP3600602.5 | 1986-01-11 | ||
DE19863600602 DE3600602A1 (de) | 1986-01-11 | 1986-01-11 | Verfahren zur herstellung von 2-oxo-1,3-dioxolanen |
Publications (2)
Publication Number | Publication Date |
---|---|
KR870007151A true KR870007151A (ko) | 1987-08-17 |
KR950003498B1 KR950003498B1 (ko) | 1995-04-13 |
Family
ID=6291668
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019870000137A KR950003498B1 (ko) | 1986-01-11 | 1987-01-10 | 2-옥소-1,3-디옥솔란의 제조방법 |
Country Status (18)
Country | Link |
---|---|
US (1) | US4835289A (ko) |
EP (1) | EP0229622B1 (ko) |
JP (1) | JP2561654B2 (ko) |
KR (1) | KR950003498B1 (ko) |
CN (1) | CN1016870B (ko) |
AR (1) | AR243878A1 (ko) |
AT (1) | ATE54664T1 (ko) |
AU (1) | AU589732B2 (ko) |
BR (1) | BR8700097A (ko) |
CA (1) | CA1335736C (ko) |
DE (2) | DE3600602A1 (ko) |
DK (1) | DK10287A (ko) |
ES (1) | ES2016807B3 (ko) |
FI (1) | FI90074C (ko) |
MX (1) | MX168442B (ko) |
NO (1) | NO870076L (ko) |
PT (1) | PT84087B (ko) |
ZA (1) | ZA87138B (ko) |
Families Citing this family (55)
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JPH064620B2 (ja) * | 1987-12-22 | 1994-01-19 | 日本ポリウレタン工業株式会社 | グリセロールカーボネートの製造方法 |
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US5095124A (en) * | 1990-09-10 | 1992-03-10 | Isp Investments Inc. | Process for the preparation of alk-1-enyl ether cyclocarbonate |
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US5182290A (en) * | 1991-08-27 | 1993-01-26 | Neurogen Corporation | Certain oxazoloquinolinones; a new class of GABA brain receptor ligands |
DE4129753C2 (de) * | 1991-09-04 | 1995-05-04 | Dainippon Ink & Chemicals | Verfahren zur Herstellung von Cyclocarbonatverbindungen |
DE4129752C2 (de) * | 1991-09-04 | 1994-01-05 | Dainippon Ink & Chemicals | Verfahren zur Herstellung von 2-Oxo-1,3-dioxolanen |
DE4225870A1 (de) * | 1992-08-05 | 1994-02-10 | Basf Ag | Verfahren zur Herstellung von Glycerincarbonat |
US5712363A (en) * | 1993-01-06 | 1998-01-27 | Akzo Nobel Nv | Oligomeric sterically hindered polyamine crosslinkers and coating compositions containing the same |
DE4344510A1 (de) * | 1993-12-24 | 1995-06-29 | Hoechst Ag | Flüssige Zweikomponenten-Überzugsmittel |
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JPH11513063A (ja) * | 1996-06-25 | 1999-11-09 | ヘルバーツ・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング | アミノウレタン硬化剤、エポキシベース塗料及びそれらの使用 |
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CN100369910C (zh) * | 2006-05-12 | 2008-02-20 | 中国科学院山西煤炭化学研究所 | 一种使用天然可再生资源生成环状碳酸酯的方法 |
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WO2010089264A1 (de) | 2009-02-05 | 2010-08-12 | Basf Se | Verfahren zur herstellung von biscarbonaten |
FR2952933B1 (fr) * | 2009-11-20 | 2012-05-25 | Centre Nat Rech Scient | Precurseurs biscarbonates, leur procede de preparation et leurs utilisations |
JP5496750B2 (ja) * | 2010-04-07 | 2014-05-21 | 株式会社クラレ | α,β−不飽和エステルの製造方法 |
ES2585030T3 (es) | 2012-08-28 | 2016-10-03 | Covestro Deutschland Ag | Aglutinante con estructuras de carbonato cíclico |
JP6426091B2 (ja) | 2012-08-28 | 2018-11-21 | コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag | イソシアナート官能性環状カルボナート |
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JP2019515074A (ja) | 2016-04-29 | 2019-06-06 | ヘンケル・アクチェンゲゼルシャフト・ウント・コムパニー・コマンディットゲゼルシャフト・アウフ・アクチェンHenkel AG & Co. KGaA | アミン官能性ポリマーおよびそのようなポリマーの製造方法 |
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DE3529263A1 (de) * | 1985-08-16 | 1987-02-19 | Hoechst Ag | Verfahren zur herstellung von 2-oxo-1,3-dioxolanen |
-
1986
- 1986-01-11 DE DE19863600602 patent/DE3600602A1/de not_active Withdrawn
-
1987
- 1987-01-07 ES ES87100074T patent/ES2016807B3/es not_active Expired - Lifetime
- 1987-01-07 DE DE8787100074T patent/DE3763670D1/de not_active Expired - Fee Related
- 1987-01-07 AT AT87100074T patent/ATE54664T1/de not_active IP Right Cessation
- 1987-01-07 EP EP87100074A patent/EP0229622B1/de not_active Expired - Lifetime
- 1987-01-08 NO NO870076A patent/NO870076L/no unknown
- 1987-01-08 FI FI870068A patent/FI90074C/fi not_active IP Right Cessation
- 1987-01-08 US US07/001,349 patent/US4835289A/en not_active Expired - Fee Related
- 1987-01-08 AR AR87306424A patent/AR243878A1/es active
- 1987-01-09 AU AU67448/87A patent/AU589732B2/en not_active Ceased
- 1987-01-09 CA CA000527001A patent/CA1335736C/en not_active Expired - Fee Related
- 1987-01-09 PT PT84087A patent/PT84087B/pt not_active IP Right Cessation
- 1987-01-09 ZA ZA87138A patent/ZA87138B/xx unknown
- 1987-01-09 JP JP62001972A patent/JP2561654B2/ja not_active Expired - Lifetime
- 1987-01-09 MX MX004902A patent/MX168442B/es unknown
- 1987-01-09 DK DK010287A patent/DK10287A/da not_active Application Discontinuation
- 1987-01-10 KR KR1019870000137A patent/KR950003498B1/ko not_active IP Right Cessation
- 1987-01-10 CN CN87100052A patent/CN1016870B/zh not_active Expired
- 1987-01-12 BR BR8700097A patent/BR8700097A/pt not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
NO870076D0 (no) | 1987-01-08 |
EP0229622A3 (en) | 1988-07-06 |
AU6744887A (en) | 1987-07-16 |
AR243878A1 (es) | 1993-09-30 |
FI90074B (fi) | 1993-09-15 |
PT84087A (en) | 1987-02-01 |
BR8700097A (pt) | 1987-12-01 |
DK10287D0 (da) | 1987-01-09 |
CA1335736C (en) | 1995-05-30 |
NO870076L (no) | 1987-07-13 |
ES2016807B3 (es) | 1990-12-01 |
FI90074C (fi) | 1993-12-27 |
JPS62175477A (ja) | 1987-08-01 |
ATE54664T1 (de) | 1990-08-15 |
DE3600602A1 (de) | 1987-07-16 |
CN87100052A (zh) | 1987-08-05 |
FI870068A0 (fi) | 1987-01-08 |
ZA87138B (en) | 1987-09-30 |
EP0229622B1 (de) | 1990-07-18 |
AU589732B2 (en) | 1989-10-19 |
EP0229622A2 (de) | 1987-07-22 |
PT84087B (pt) | 1989-07-31 |
US4835289A (en) | 1989-05-30 |
MX168442B (es) | 1993-05-25 |
DE3763670D1 (de) | 1990-08-23 |
JP2561654B2 (ja) | 1996-12-11 |
DK10287A (da) | 1987-07-12 |
FI870068A (fi) | 1987-07-12 |
CN1016870B (zh) | 1992-06-03 |
KR950003498B1 (ko) | 1995-04-13 |
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