KR20100095967A - Cosmetic composition and preparation of peel-off nutrition mask pack containing loess powder and herb extracts - Google Patents

Cosmetic composition and preparation of peel-off nutrition mask pack containing loess powder and herb extracts Download PDF

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KR20100095967A
KR20100095967A KR1020090015039A KR20090015039A KR20100095967A KR 20100095967 A KR20100095967 A KR 20100095967A KR 1020090015039 A KR1020090015039 A KR 1020090015039A KR 20090015039 A KR20090015039 A KR 20090015039A KR 20100095967 A KR20100095967 A KR 20100095967A
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ocher
pack
skin
peel
powder
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최중소
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/042Gels
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

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  • Cosmetics (AREA)

Abstract

PURPOSE: A composition of yellow soil nutritious pack of peel-off type is provided to ensure treatment of skin defect. CONSTITUTION: A peel-off yellow soil nutritious pack composition contains: 30wt% of yellow soil powder, 25wt% of herb extract(Dictamni Radicis Cortx/Houttuynia cordata/Ginkgonis folium/mulberry/Phaseoli radiati Semen/seaweeds/herb/aloe), 15wt% of coating agent, 5wt% of moisturizer(1,3-butyleneglycol/glycerin/alantoin/oat meal/sodium hyaluronate/rice bran), 10wt% of oil, and 5wt% of emulsifying agent(glyceryl stearate/polysolvate-60).

Description

황토분말 및 한방추출물을 함유하는 필-오프 황토영양팩의 조성물 및 제조방법{Cosmetic composition and preparation of peel-off nutrition mask pack containing loess powder and herb extracts}Composition and preparation method of peel-off ocher nutrient pack containing ocher powder and herbal extracts {{Cosmetic composition and preparation of peel-off nutrition mask pack containing loess powder and herb extracts}

발명이 속하는 기술 및 그 분야의 종래기술 The technology to which the invention belongs and the prior art in the field

황토분말을 이용하여 미용팩을 제조하기 위한 조성물 및 제조방법에 관한 종래의 기술은 다양하게 개발되어져 왔다.   Conventional techniques related to compositions and methods for preparing cosmetic packs using ocher powder have been developed in various ways.

사용방법을 기준으로 황토분말을 이용한 미용팩을 분류하면 피부에 적용된 후에 씻어내는 워시오프(wash-off)형과 떼어내는 필-오프(peel-off)형으로 나뉘어 진다. 이러한 분류에 따라 워시오프(wash-off)형 황토미용팩에 관련한 종래의 기술들은 황토를 주원료로 하여 다양한 식물추출물, 국내에서 생산되는 토종 액상 및 분말 원료, 천연 광물, 천연오일, 보습제, 각종 영양성분 등을 서로 다른 형태로 혼합한 후 물을 추가하여 겔화(gelation)시켜 피부에 도포하였다가 씻어 내는 타입으로 제조하여 피부개선효과가 뛰어나다고 각기 주장하여 왔다.   If you classify the cosmetic pack using ocher powder based on the method of use, it is divided into wash-off type and peel-off type that are washed off after being applied to the skin. According to this classification, the related arts related to the wash-off type ocher cosmetic packs have various plant extracts, native liquid and powder raw materials produced in Korea, natural minerals, natural oils, humectants, and various nutritional ingredients based on ocher. Each of them has been insisted on having excellent skin improvement effects by mixing gels by mixing water in different forms, gelling the gel by applying water, and then applying it to the skin.

상기에서 설명한 바와 같이 워시오프(wash-off)형의 황토미용팩은 발명자 각각의 아이디어만 있으면 전문기술이 부족하여도 누구나 쉽게 제조하여 발명 효과를 누릴 수 있는 장점이 있는 반면에, 황토미용팩이 얼굴에 도포된 후 일정시간 후에 씻어낼 때는 모공에 빠진 미세한 황토입자가 씻겨지지 않고 그대로 남아 피부로 흡수되어 피부트러블의 원인이 될 수도 있고, 피부를 세척한 장소의 황토 물은 청소해야하는 번거로움의 단점을 가지고 있다.     As described above, the washing-off type ocher cosmetic pack has the advantage that anyone can easily manufacture and enjoy the invention effect even if they lack the expertise if each of the inventors have ideas, while the ocher cosmetic pack has a face. When the product is washed after a certain time after application, the fine ocher particles in the pores remain unwashed and absorbed into the skin, which may cause skin trouble, and the ocher water in the place where the skin is washed has the disadvantage of having to clean. Have.

이러한 단점을 해결할 수 있는 대안이 필-오프(peel-off)형의 황토미용팩이다. 이는 워시오프(wash-off)형의 황토미용팩에 비하여 제조의 난이도가 높다. 특허등록번호 10-085324[문헌1]은 황토분말 과 소디움 알기네이트(Na-Alginate)분말을 주요성분으로 하여 여기에 물을 부어 반죽으로 하여 소디움 알기네이트(Na-Alginate)분말이 물과 혼합이 되면 이온중합 반응이 일어나 이온중합 특성상 속경화 되어 고무와 같은 탄성체가 되는 성질을 이용하였다. 이온중합 반응이 너무 빠르게 진행되어 반응속도조절을 하기 위하여 지연제로 인산나트륨을 사용하고 있으며, 부드러움을 부여하기 위하여 연화제로 탄산나트륨을 사용하였다. 이렇게 제조된 황토분말과 소디움 알기네이트(Na-Alginate) 분말 혼합물에 물을 부어 페이스트 형상의 황토혼합물을 얼굴에 두껍게 도포한 후 일정시간 후에 떼어내는 필-오프 황토팩을 제조하여 발명의 효과로서 일반적인 황토의 효과를 제시한 바 있었다.   An alternative solution to this drawback is the peel-off type ocher cosmetology pack. This is a difficulty of manufacturing compared to the wash-off type ocher cosmetology pack. Patent registration No. 10-085324 [Patent 1] is made of ocher powder and sodium alginate (Na-Alginate) powder as main ingredients, and water is poured into it to make the sodium-alginate powder mixed with water. In this case, the ion polymerization reaction occurs, and the ionic polymerization property is used to rapidly harden and to become an elastomer such as rubber. Sodium phosphate was used as a retarder to control the reaction rate because the ion polymerization reaction proceeded too fast, and sodium carbonate was used as a softener to impart softness. The ocher powder and sodium alginate (Na-Alginate) powder mixture thus prepared are poured into the ocher mixture thickly on the face, and then peeled off after a certain time to prepare a peel-off ocher pack. The effect of ocher was presented.

발명이 이루고자 하는 기술적 과제Technical problem to be invented

상기에서 설명한 바와 같이 워시-오프(wash-off)형의 황토미용팩을 제조하는 특허는 다수가 존재하고 있지만 필-오프(wash-off)형의 황토미용팩에 관한 등록특허는 특허등록번호 10-0853204[문헌1] 만이 존재하나 이 또한 사용 전에 황토팩 혼 합물에 물을 부어 반죽으로 만들어 가능하면 빠른 시간 내에 사용해야하는 불편함이 있다.    As described above, there are a number of patents for manufacturing the wash-off type ocher cosmetic pack, but the registered patent for the wash-off type ocher cosmetic pack is patent registered number 10-0853204. [1] only exists, but this also has the inconvenience of using the ocher pack mixture to pour water into the dough to use as soon as possible.

상기에서 설명한 바와 같이 워시-오프(wash-off)형의 황토미용팩을 제조하는 특허는 다수가 존재하고 있지만 이러한 특허들은 워시-오프(wash-off)형의 황토미용팩 단점인 모공으로의 미세한 황토입자의 박힘 현상, 사용 후 청소의 번거로움의 문제를 해소할 수가 없었고, 피부개선효과를 얻기 위한 필-오프(wash-off)형의 황토미용팩에 관한 등록특허번호 10-0853204[문헌1]은 유일하게 황토분말과 소디움알기네이트(Na-Alginate)분말 혼합물이 물과 만나 이온중합을 시킴으로서 두껍게 피막이 형성되어 떼어내는 제품을 제조하는 방법은 있었으나 이 또한 사용 전에 황토팩 혼합물에 물을 부어 반죽으로 만들어 사용해야하고, 피부에 바르는 시간이 지연되면 경화되어 사용을 할 수 없는 불편함이 있다.    As described above, there are a number of patents for manufacturing a wash-off type ocher cosmetology pack, but these patents are fine ocher particles into pores, which are disadvantages of the wash-off type ocher cosmetology pack. The problem of nailing phenomenon and the trouble of cleaning after use could not be solved, and Patent No. 10-0853204 [Patent 1] relates to a wash-off type ocher cosmetic pack for obtaining skin improvement effect. There has been a method of manufacturing a product in which a mixture of ocher powder and sodium alginate powder meets with water and undergoes ion polymerization to form a thick film, and then, before use, pour water into the ocher pack mixture to make a dough. And, if the time to apply to the skin is delayed there is an inconvenience that can not be used.

본 발명에서는 워시오프형 황토미용팩의 단점을 해결하고, 발열반응을 하는 이온중합반응의 단시간 반응문제로 단시간에 얼굴에 도포해야만 하는 기존의 필오프형의 황토미용팩의 문제점을 개선하여 새로운 발명 제품을 제조하고자 황토분말, 피막제, 한방추출물, 천연보습제, 천연오일, 기능성영양성분 등을 함유하고 있으면서 이 혼합물을 유화방법으로 균일 황토 점성액체(황토영양팩)으로 제조하여 이를 얼굴에 도포하였다가 일정시간 후에 떼어낼 수 있는 필-오프형의 황토영양팩을 발명하여 피부개선효과를 이루고자 한다.   The present invention solves the shortcomings of the washoff type ocher cosmetic pack and improves the problem of the existing peel-off type ocher cosmetic pack which has to be applied to the face in a short time due to the short time reaction problem of the ion polymerization reaction exothermic. It contains ocher powder, coating film, herbal extract, natural moisturizer, natural oil, functional nutritional ingredients, etc., and this mixture is prepared as an ocher viscous liquid (ocher nutrition pack) by emulsification method and applied to the face. Invented a peel-off type ocher nutrition pack that can be removed to achieve skin improvement.

발명의 구성Composition of the Invention

본 발명은 피부개선효과를 발휘해 주는 황토영양팩 조성물 및 제조방법에 관한 것으로, 더욱 상세하게는 황토분말, 한방추출물, 피막제, 천연보습제, 천연오일, 천연영양성분으로 구성된 혼합액이 피부개선 효과를 나타낼 수 있도록 황토분말의 원적외선, 음이온, 미네랄성분 등의 특성을 이용하였고, 한방추출물의 항균 및 보습 특징을 이용하였고, 피막제의 점착 특성을 이용하였고, 천연보습제, 천연오일, 천연영양성분의 유수분 균형 유지 및 기능성 특성을 이용하였다.    The present invention relates to a loess nutrient pack composition and a method for producing the skin improvement effect, and more particularly, a mixture consisting of ocher powder, herbal extracts, coating agent, natural moisturizing agent, natural oil, and natural nutrients may exhibit skin improvement effect. It uses the characteristics of far-infrared, anion, and minerals of ocher powder, antibacterial and moisturizing properties of herbal extracts, adhesive properties of coatings, maintenance of oil and moisture balance of natural moisturizers, natural oils, and natural nutrients. Functional properties were used.

더욱 상세하게는 황토는 저준위 에너지를 갖는 원적외선을 방사하여 진피에 에너지를 전달하여 발한작용, 모세혈관의 혈행 개선, 신진대사촉진 효과를 나타내 주고, 피지를 녹여 모공을 통하여 노폐물을 배출시키고, 발생된 음이온은 몸속의 활성산소와 결합하여 피부의 스트레스를 감소시켜주고, 각종 미네랄 성분(Na, Mg, Ca 등)은 천연보습인자로 작용하는 효과를 발휘하는 성분으로 작용하였고, 한방추출물은 항균 및 보습효과가 있어 피부기생충을 다스려 손상된 피부의 재생을 돕는 성분으로 작용하여주었고, 천연보습제 및 천연오일은 피부의 유수분 균형유지 성분으로 작용하여주었고, 천연영양성분은 재생된 피부에 영양을 보충해주는 성분으로 작용하여 본 발명품은 피부개선 효과를 극대화 시켜주었다.   More specifically, ocher transmits energy to the dermis by radiating far-infrared rays with low-level energy, thus exhibiting sweating, improving blood circulation in capillaries, promoting metabolism, and dissolving sebum to discharge waste products through pores. Negative ions combine with active oxygen in the body to reduce skin stress, and various mineral components (Na, Mg, Ca, etc.) act as a natural moisturizing factor. Herbal extracts are antibacterial and moisturizing. It is effective in controlling skin parasites and helping to regenerate damaged skin.Natural moisturizers and natural oils act as skin oil and moisture balance components, and natural nutrients supplement nutrition to regenerated skin. By acting as the present invention maximized the skin improvement effect.

일반적으로 대부분의 황토미용팩은 황토분말에 각종 천연재료로 된 분말을 배합하여 물과 일정비율로 혼합하여 피부에 바르거나 황토분말에 피부에 영양을 줄 수 있는 액상원료를 배합하여 습식형태로 제조한 후 이를 피부에 바르고 건조되면 물 로 씻어내는 워시-오프형 형태로 제조하여 사용하고 있다.  In general, most ocher cosmetology packs are prepared in a wet form by mixing powders of various natural ingredients with ocher powder and mixing them with water at a certain ratio and applying liquid ingredients that can nourish the skin with ocher powder. After it is applied to the skin and dried and washed with water wash-off form is used.

또한 황토미용팩이 간편성을 갖추기 위하여 보조기구로 얼굴모양의 부직포에 상기에서 제조된 황토미용팩 혼합물을 침투시켜 피부에 일정시간 붙였다가 떼어내도록 제조하여 사용하기도 한다.  In addition, the ocher cosmetology pack may be used to infiltrate the ocher cosmetology pack mixture prepared in the above into the face-shaped nonwoven fabric as an auxiliary device to attach to the skin for a certain time and then remove it.

그러나 워시-오프 형태이든 부직포 형태이든 팩에 황토분말을 이용하였다면 미세한 황토입자가 모공을 통하여 금속산화물 형태로 흡수되어 박혀 계속 축적이 되면 때로는 피부트러블의 원인이 될 수도 있다. 이러한 문제점을 해결하기 위해서는 황토입자가 피부표면에서만 머물러 황토 고유의 독특한 기능으로 피부개선 작용을 하고, 황토 속의 천연 보습인자인 미네랄 성분만이 피부에 흡수되어 피부미용의 개선효과만 얻을 수 있고, 간편하게 떼어내는 필-오프 형의 황토미용팩을 제조하는 기술을 필요로 하고 있다.  However, if ocher powder is used in the pack, whether in the wash-off or non-woven form, the fine ocher particles are absorbed into the metal oxide form through the pores and accumulate continuously, which may sometimes cause skin problems. In order to solve this problem, the ocher particles stay on the skin surface to improve the skin with the unique function of ocher, and only the mineral component, which is a natural moisturizing factor in the ocher, is absorbed by the skin, and only the improvement of skin beauty can be obtained. There is a need for a technique for producing a peel-off type ocher cosmetic pack.

종래기술의 문헌정보Literature Information of the Prior Art

[문헌1] 특허등록번호 10-0853204 A 2008.08.13.[Document 1] Patent Registration No. 10-0853204 A 2008.08.13.

본 발명에서 제조한 필-오프형 황토영양팩은 무기물인 황토분말이 에멀젼화된 유기물인 화장료 조성물에 함유되어 균일하게 분산되어 피부에 도포되어 건조 후에 팩이 찢어지지 않고 균일하게 떼어져야 하며, 피부에 도포되어 있을 때 피부에 자 극을 주지 않을 정도로 부드러워야 하고, 영양팩 속의 황토는 물론이거니와 한방추출물, 보습제, 천연오일, 기능성 영양성분 등의 각종 피부개선 성분이 피부에 흡수되어 피부개선 효과를 발휘하도록 황토영양팩을 제조하는 데 그 목적이 있다.  Peel-off type ocher nutrition pack prepared in the present invention is contained in the cosmetic composition of the emulsified organic soil ocher powder is uniformly dispersed and applied to the skin to be peeled off evenly without drying the pack after drying, When applied, it should be soft enough to not irritate the skin, and not only ocher in the nutrition pack, but also various skin improvement ingredients such as herbal extracts, moisturizers, natural oils, and functional nutritional ingredients are absorbed by the skin to exert skin improvement effects. Its purpose is to produce ocher nutrition pack.

본 발명에서는 상기의 목적을 달성하기 위하여 황토분말, 한방추출물, 피막제, 보습제, 천연오일, 기능성 영양성분 등을 함유하면서 피부개선효과를 나타내는 필-오프형 황토미용팩을 제조하기 위하여 다음과 같은 실시단계를 거쳤다.  In the present invention, to achieve the above object to prepare a peel-off type ocher beauty pack containing the ocher powder, herbal extracts, coatings, moisturizers, natural oils, functional nutritional ingredients, etc. and showing the skin improvement effect Went through.

실시 예 1. - 황토분말의 준비단계Example 1 Preparation of Loess Powder

본 발명에서 사용된 황토분말은 원토를 채취하여 건조 및 볼밀에 의한 분쇄과정을 거쳐 325 메쉬(mesh)로 1차 분급되고, 325 메쉬 이상의 황토분말을 채취하여 다시 사이클론을 통과시켜 8,000 메쉬(평균직경 1.6 마이크로미터) 망을 통과한 분말만을 채취하여 사용하였다.    The ocher powder used in the present invention is first classified into 325 mesh through pulverization process by drying and ball mill after collecting raw soil, and after collecting ocher powder of 325 mesh or more and passing through a cyclone again, 8,000 mesh (average diameter) 1.6 micrometers) only the powder that passed through the net was used.

실시 예 2. - 한방추출물의 준비 단계Example 2 Preparation of Herbal Extracts

본 발명에서는 황토영양팩이 항균효과 및 보습효과를 나타내주는 한방재료를 선정하기 위하여 [동의보감] 등에서 추출물을 피부에 발라 상처가 나았다거나 천연보습제로 추천이 되고 있는 다양한 천연재료 중에서 문헌에 근거하여 항균효과와 보습효과가 뛰어난 백선피/어성초/은행잎/뽕나무/녹두/해초/쑥/로즈마리/알로에 등 을 선정하여 9종류로 구성된 한방재료를 준비하였다. 9종의 한방재료는 따로따로 정제수/한방재의 비율을 50/50 wt%로 하여 추출조에 넣고 50로 48시간 이상을 진공 농축하여 추출되며, 농축된 한방추출물은 여과과정을 거쳐 황토영양팩을 제조하는 원료로 사용하였다.    In the present invention, in order to select a herbal material showing the antimicrobial and moisturizing effect of the ocher nutrition pack, the antimicrobial effect is based on the literature among various natural materials that have been applied to the skin by the extracts from [agreement bogam], etc. Also, 9 kinds of herbal ingredients were prepared by selecting white pine, fish vinegar, ginkgo biloba, mulberry, green bean, seaweed, mugwort, rosemary, and aloe. Nine kinds of herbal materials are separately extracted into 50/50 wt% ratio of purified water / herbal materials in an extraction tank and extracted by vacuum concentration for more than 48 hours at 50. The concentrated herbal extracts are filtered to produce ocher nutrition packs. Used as a raw material.

실시 예 3. - 피막제의 최적 배합비 결정 단계Example 3-Determination of the optimum blending ratio of the coating agent

본 발명에서는 황토분말 및 한방추출물을 함유한 혼합물의 피막이 찢어지지 않는 최적의 조건을 찾기 위하여 상기에서 사전 준비한 8000 메쉬 이상의 입도분포를 갖는 황토분말을 사용하였고, 피막제로는 점착성능이 우수하며 피부에 적용되어 해가 없는 폴리비닐알콜(PVA)과 폴리비닐피롤리돈(PVP)을 선정하였고, 황토/PVA/PVP 간의 함량비를 변화시켜가며 건조 후에 피막의 찢김을 조사하여 그 결과를 표 1.에 나타내었다.   In the present invention, in order to find the optimal condition that the coating of the mixture containing ocher powder and herbal extracts does not tear, ocher powder having a particle size distribution of 8000 mesh or more prepared in advance was used. The selected polyvinyl alcohol (PVA) and polyvinylpyrrolidone (PVP) were applied to each other, and the tearing of the film after drying was performed by changing the content ratio between ocher / PVA / PVP. Shown in

단위 : wt %Unit: wt% 황토ocher PVAPVA PVPPVP 피막 찢김Tear film 100100 00 00 Yes 8585 1010 55 Yes 7070 2020 1010 아니오no 5555 3030 1515 아니오no 4040 4040 2020 아니오no 2525 5050 2525 아니오no 1010 6060 3030 아니오no

상기의 표 1.에서 보는 바와 같이 피막 찢어짐이 없는 황토분말/PVA/PVP 간의 함량비는 70/20/10 으로 나타나 이를 황토영양팩을 제조하기 위한 최적의 피막제 함량비로 결정하였으며, 더욱 상세하게는 55/30/15 의 함량비로 피막을 제조할 때가 최적이라는 결과로 나타났다.    As shown in Table 1 above, the content ratio between the ocher powder / PVA / PVP without tearing of the film was 70/20/10, which was determined as an optimal coating agent content ratio for preparing the ocher nutrition pack, and more specifically, 55. The optimum results were obtained when the film was prepared with a content ratio of / 30/15.

상기에서 결정된 조성물은 피부에 도포되고 건조되면 피부에 너무 강하게 점착이 되어 떼어낼 때 피부가 통증을 느끼거나 심지어는 피부를 상하게 할 수도 있다. 이러한 문제를 해결하기 위하여 상기 피막을 부보습제로 1,3-브틸렌글리콜을 결정하였다. 이의 최적함량 비율을 찾기 위하여 황토/PVA/PVP의 함량비를 55/30/15 로 고정시킨 후 이를 한 성분으로 간주하고 1,3-브틸렌글리콜을 0.5~10.0 wt% 범위에서 변화시켰고, 더욱 상세하게는 황토영양팩 전체 조성물 대비 1.0~2.0 wt% 범위에서 이를 첨가하여 반복실험에 의하여 황토영양팩 피막에 유연성 및 촉촉함을 부여하였다.    The composition determined above may be too strongly adhered to the skin when applied to the skin and dried, causing the skin to feel pain or even hurt the skin when peeled off. In order to solve this problem, 1,3-butylene glycol was determined as the moisturizing agent. In order to find the optimal content ratio, the content ratio of ocher / PVA / PVP was fixed to 55/30/15, and this was regarded as one component, and 1,3-butylene glycol was changed in the range of 0.5 to 10.0 wt%, Specifically, it was added in the range of 1.0 to 2.0 wt% of the ocher nutrition pack total composition to give flexibility and moisture to the ocher nutrition pack film by repeated experiments.

실시 예 4. - Example 4.- 황토영양팩의Ocher Nutrition Pack 제조 단계 Manufacturing steps

상기 비율로 결정된 황토/피막제의 함량비에 맞추어 황토분말 30wt%, 피막제 드럽게 해주는 성분으로 연화제 겸 25wt%(폴리비닐알콜/폴리비닐피롤리돈), 보습제 5 wt% (1,3-브틸렌글리콜/글리세린/알란토인/오트밀/소디움 히아루로네이트/디판테놀/쌀겨), 한방추출물 25wt%를 진공아지믹서에 혼합시킨 후 70까지 승온시켜 교반하여 완전히 용해시켰고, 또한 오일 용해조에 오일상으로 10wt% (호호바오일/올리브오일/새서미오일/스쿠알란/세틸알콜/스테아린산/피이지-60 경피자유), 유화제 함량 5wt%(글리세릴 스테아레이트/폴리솔베이트-60)를 넣고, 70로 유지하여 교반하여 완전히 용해시킨다.   According to the content ratio of ocher / coating agent determined by the above ratio, ocher powder 30wt%, softening agent and 25wt% (polyvinyl alcohol / polyvinylpyrrolidone) as a component to soften the coating agent, moisturizing agent 5 wt% (1,3- butylene glycol / Glycerin / Allantoin / Oatmeal / Sodium Hyaluronate / Difanthenol / Rice Bran), 25wt% of herbal extracts were mixed in a vacuum agitator, heated to 70, and completely dissolved by stirring. Jojoba oil / olive oil / sasumi oil / squalane / cetyl alcohol / stearic acid / figure-60 transdermal oil) and 5 wt% of emulsifier (glyceryl stearate / polysorbate-60) are added and kept at 70 and stirred Dissolve completely.

상기의 용해된 수상혼합물에 오일혼합물을 배합하고 5분간 5000 rpm으로 고속 교반한다. 이어서 30까지 냉각하고, 콜라겐, 엘라스틴, 코엔자임Q-10, 알부틴, 향료 등의 기능성 영양성분을 미량씩 첨가하고 교반한 후 탈포를 하여 용기에 주입을 한다.   The oil mixture is blended with the dissolved aqueous phase mixture and stirred at 5000 rpm at high speed for 5 minutes. Subsequently, the mixture is cooled to 30, and a small amount of functional nutrients such as collagen, elastin, coenzyme Q-10, arbutin, and fragrance are added, stirred, and defoamed to be injected into a container.

실시 예 5. - Example 5. 황토영양팩의Ocher Nutrition Pack 필- Phil 오프off 기능 확인 단계 Feature Verification Steps

본 발명에서 상기의 방법으로 제조된 황토영양팩의 필-오프의 기능 유지여부를 확인하기 위하여 실제의 인물에 적용시켰고, 도 1.에는 황토영양팩을 얼굴에 바르는 모습을, 도 2.에는 떼어낸 황토영양팩을 나타내었다. 도 1. 및 도 2. 에서 보는 바와 같이 상기 제조과정을 통하여 제조된 황토영양팩은 얼굴에 도포되어 건조 후에 1mm 이하의 얇은 막으로 떼어지는 결과를 얻었다.    The present invention was applied to a real person to check whether the ocher nutrient pack prepared by the above method maintains the peel-off function, Figure 1. Figure of applying the ocher nutrient pack on the face, Figure 2. A nutrition pack was shown. As shown in Figure 1 and Figure 2. The ocher nutrient pack prepared through the manufacturing process was applied to the face and obtained a result of peeling off a thin film of less than 1mm after drying.

실시 예 6. - 황토영양 팩의 관능평가 단계Example 6 sensory evaluation step of ocher nutrition pack

상기 방법으로 제조된 황토영양팩에 대하여 19~50세의 여성 50명을 대상으로 3회/주 이상 사용하도록 하고 2개월 동안 피부반응에 대한 관능평가를 실시하여 사용 중 및 사용 후로 구분하여 순서대로 다음 표 2.에 나타내었다.   For ocher nutrition packs prepared by the above method, 50 women aged 19 to 50 should be used more than 3 times / week, and sensory evaluation of skin reactions for 2 months was carried out. Table 2 shows.

괄호안(%)In parentheses (%) 번호number 구 분division AA BB CC 1One 팩도포시 사용감Feel when using the pack 사용부위 아픔(10)Pain in use (10) 사용부위 시원함(70)Cooling Area (70) 감각 없음(20)No sense (20) 22 팩의 피부밀착성Skin adhesion of the pack 강함(10)Strong (10) 중간(80)Medium (80) 무응답(10)No Response (10) 33 팩후 피부보습상태Skin moisturizing condition after pack 끈적임(0)Sticky (0) 촉촉함(92)Moist (92) 건조함(8)Dry (8) 44 필-오프 사용감Feel-off feeling 뗄때 아픔(8)Sick pain (8) 뗄때 적당함(90)Suitable for removing (90) 무응답(2)No Response (2) 55 팩후 화장효과Makeup effect after pack 화장안됨(5)No makeup (5) 화장 잘됨(86)Good Makeup (86) 무응답(10)No Response (10) 66 미백(맑음)효과Whitening effect 높음(20)High (20) 적당(60)Fitness (60) 약함(20)Weak (20) 77 주름개선효과Wrinkle improvement effect 높음(4)High (4) 적당(64)Fitness (64) 약함(32)Weak (32) 88 피부잡티개선효과Skin Blemish Improvement 높음(40)High (40) 적당(50)Fitness (50) 약함(10)Weak (10) 99 팩의 건조시간Pack drying time 20-30분(30)20-30 minutes (30) 10-20분(70)10-20 minutes (70) 1-10분(0)1-10 minutes (0)

상기 표 2.에서 보는 바와 같이 본 발명에서 제조한 황토영양팩을 무작위 50명 여성에게 사용하도록 하여 관능 평가한 결과를 살펴보면, 팩을 도포하였을 때 사용부위가 시원하다고 답하였고, 피부에 대한 황토영양팩의 밀착성은 좋았다 라고 답하였고, 팩을 사용한 후의 피부의 보습상태는 촉촉하였다는 의견이 지배적이었고, 팩이 건조된 후 떼어낼 때 약간 아픈 감이 있거나 대부분 적당하다고 답하였으며, 팩을 한 후에 화장효과는 잘 된다 라는 의견이 지배적이었고, 팩을 한 후에 미백(맑음), 주름개선, 피부잡티개선 효과는 적당하다는 의견이었으며, 팩이 건조되어 떼어내는 시간까지는 10-20분 정도 소요된 것으로 나타났다.  Looking at the results of sensory evaluation by using the ocher nutrition pack prepared in the present invention to 50 random women as shown in Table 2. When the pack was applied, the use site was cool, and the ocher nutrition pack for the skin It was said that the adhesiveness was good, and the opinion that the moisturizing condition of the skin was moist after using the pack was dominant, and that it was slightly painful or mostly appropriate when peeling off after the pack was dried. Opinion was predominant, and after the pack, the effect of whitening (clear), wrinkle improvement and skin blemishes was moderate, and it took 10-20 minutes for the pack to dry out.

본 발명에서는 황토분말, 한방추출물, 피막제, 보습제, 오일, 기능성 영양성분을 함유하는 필-오프형 황토영양팩을 제조한 결과, 황토분말 30wt%, 한방추출물 25wt%, 피막제 25wt%, 보습제 5 wt%, 오일 10wt%, 유화제 함량 5wt%, 기능성 영양성분 미량 등을 함유하는 황토영양팩 조성물이 두께 1mm 이하로 되어도 충분한 필-오프 기능을 발휘하였고, 이를 무작위 50명을 선정하여 관능평가를 실시한 결과, 상기 표2. 와 같은 피부개선 효과를 가진 결과로 나타났다.  In the present invention, as a result of preparing a peel-off loess nutrient pack containing ocher powder, herbal extract, coating agent, humectant, oil, functional nutritional ingredients, ocher powder 30wt%, herbal extract 25wt%, coating agent 25wt%, moisturizer 5wt% The ocher nutrient pack composition containing 10 wt% oil, 5 wt% emulsifier content, trace amount of functional nutrients, and the like exhibited sufficient peel-off function even when the thickness was 1 mm or less. Table 2. The result was a skin improvement effect such as

이는 황토의 고유 특성인 원적외선 흡수에 의한 노폐물 제거, 음이온 발생에 의한 몸속의 활성산소 감소, 미네랄에 의한 피부보습, 피부윤기, 피부결 개선이 이루어진 것으로 추정되며, 여기에 추가로 한방추출물, 보습제, 천연오일 등은 황토와 함께 피부개선을 위한 충분한 효과를 발휘 하였다고 할 수 있다.  It is estimated that the intrinsic properties of ocher are the removal of waste products by absorption of far infrared rays, the reduction of free radicals in the body by the generation of negative ions, skin moisturization by minerals, skin gloss, and skin texture improvement. Natural oil, etc., can be said to exert sufficient effects for skin improvement along with ocher.

본 발명에서 제조한 황토영양팩은 피막이 얇으면서도 피부에 도포되어 건조 후에 떼어낼 때 찢어지지 않고 적당히 부드러워 떼어내는 통증이 없으며, 피부개선용으로 사용된 원재료의 측면에서 황토의 효능을 충분히 감지할 수 있었고, 한방추출물은 피부의 결함을 개선시켜주는 충분한 효과를 발휘함을 감지할 수 있었고, 유수분 평형유지에 의한 피부의 보습도도 잘 이루어지고 있는 특징을 가지고 있는 것으로 나타났다.  The ocher nutrient pack prepared in the present invention was applied to the skin even though the film was thin, there was no tearing and not peeling moderately when peeling off after drying, and it was possible to sufficiently sense the efficacy of ocher in terms of raw materials used for skin improvement. In addition, it was found that herbal extracts exhibited sufficient effects to improve skin defects, and the moisture retention of the skin due to oil and moisture balance was well established.

본 발명에서는 다음 표 3.과 같은 조성을 가진 황토영양팩을 제조하여 1mm 이하의 두께를 갖는 필-오프 황토영양팩을 제조할 수 있으며, 이를 사용하여 피부개선효과를 발휘할 수 있다. In the present invention, the ocher nutrient pack having a composition as shown in Table 3 may be prepared to produce a peel-off ocher nutrient pack having a thickness of 1 mm or less, and the skin improvement effect may be exhibited using the same.

단위 : wt%Unit: wt% 번호number 성분ingredient 본 발명Invention 1One 황토분말Ocher powder 3030 22 한방추출물Herbal Extract 2525 33 피막제Film 2525 44 보습제Moisturizer 55 55 오일oil 1010 66 유화제Emulsifier 55 77 기능성영양성분Functional Nutrition Ingredients 미량a very small amount

본 발명에서 제조한 황토영양팩은 도1. 및 도 2. 에서 보는 바와 같이 얼굴에 도포한 후 15-20분 동안의 건조시간을 거쳐 1 mm 이하의 피막으로 떼어낼 수 있고, 도 3.의 황토영양팩의 제조공정을 나타낸 흐름도에서와 같이 제품화될 수 있기 때문에 산업상 이용가능성은 충분한 것으로 판단된다.  The ocher nutritional pack prepared in the present invention is shown in Figure 1. And after applying to the face as shown in Figure 2. After drying for 15-20 minutes can be peeled off to a film of 1 mm or less, as shown in the flow chart showing the manufacturing process of the ocher nutrition pack of Figure 3. Industrial availability is considered to be sufficient.

도 1은 황토영양팩을 얼굴에 바르는 모습    Figure 1 is the appearance of applying the ocher nutritional pack on the face

도 2은 황토영양팩을 얼굴에서 떼어낸 모습     Figure 2 shows the ocher nutritional pack removed from the face

도 3은 황토영양팩의 제조공정을 나타낸 흐름도     Figure 3 is a flow chart showing a manufacturing process of ocher nutrition pack

Claims (2)

황토분말 30 wt%, 한방추출물 25wt%( 백선피/어성초/은행잎/뽕나무/녹두/해초/쑥/허브/알로에), 피막제 15wt%(PVA/PVP), 보습제 5wt% (1,3-브틸렌글리콜/글리세린/ 알란토인/오트밀/소디움 히아루로네이트/디판테놀/쌀겨), 오일 10 wt%(호호바오일/올리브오일/새서미오일/스쿠알란/세틸알콜/스테아린산), 유화제 5wt%(글리세릴 스테아레이트/폴리솔베이트-60) 등으로 이루어진 것을 특징으로 하는 필-오프 황토영양팩의 조성물 및 제조방법  Loess powder 30 wt%, Herbal extract 25wt% (Birthday skin, Echo, Ginkgo leaf, Mulberry, Mung bean, Seaweed, Mugwort, Herb, Aloe), 15 wt% of coating agent (PVA / PVP), Moisturizing agent 5wt% (1,3-butylene Glycol / Glycerin / Allantoin / Oatmeal / Sodium Hyaluronate / Dipanthenol / Rice Bran), Oil 10 wt% / Polysorbate-60) composition of the peel-off ocher nutrition pack, characterized in that consisting of 제1항에 있어서, 8,000메쉬 이하의 입도분포를 갖는 황토분말을 함유하면서 건조 후에 1 mm 이하의 두께를 갖는 특징으로 하는 필-오프 황토영양팩의 제조방법 The method for preparing a peel-off loess nutrient pack according to claim 1, wherein the method comprises a loess powder having a particle size distribution of 8,000 mesh or less and has a thickness of 1 mm or less after drying.
KR1020090015039A 2009-02-23 2009-02-23 Cosmetic composition and preparation of peel-off nutrition mask pack containing loess powder and herb extracts KR101112716B1 (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102648941A (en) * 2011-02-28 2012-08-29 中国医学科学院药用植物研究所 New application for antioxidation action of cortex dictamni extract
KR20190000816A (en) * 2017-06-23 2019-01-03 주식회사 글로원 Mask pack with improved elasticity manufactured by using biodegradable polymer and loess, and the method for manufacturing the mask pack
CN109481729A (en) * 2018-11-23 2019-03-19 南京华开生物科技有限公司 A kind of low molecular weight sodium hyaluronate isotonic liquid dressing and preparation method thereof
KR102622864B1 (en) * 2023-03-13 2024-01-09 한국콜마주식회사 Cosmetics composition of peel-off type pack

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010088600A (en) * 2001-08-09 2001-09-28 최상구 Peel off type loess pack
KR20050062473A (en) * 2005-04-28 2005-06-23 방계룡 Jellied pack contained yellow soil.

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102648941A (en) * 2011-02-28 2012-08-29 中国医学科学院药用植物研究所 New application for antioxidation action of cortex dictamni extract
KR20190000816A (en) * 2017-06-23 2019-01-03 주식회사 글로원 Mask pack with improved elasticity manufactured by using biodegradable polymer and loess, and the method for manufacturing the mask pack
CN109481729A (en) * 2018-11-23 2019-03-19 南京华开生物科技有限公司 A kind of low molecular weight sodium hyaluronate isotonic liquid dressing and preparation method thereof
KR102622864B1 (en) * 2023-03-13 2024-01-09 한국콜마주식회사 Cosmetics composition of peel-off type pack

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