JPWO2013080284A1 - 胡麻含有酸性液状調味料 - Google Patents
胡麻含有酸性液状調味料 Download PDFInfo
- Publication number
- JPWO2013080284A1 JPWO2013080284A1 JP2012516427A JP2012516427A JPWO2013080284A1 JP WO2013080284 A1 JPWO2013080284 A1 JP WO2013080284A1 JP 2012516427 A JP2012516427 A JP 2012516427A JP 2012516427 A JP2012516427 A JP 2012516427A JP WO2013080284 A1 JPWO2013080284 A1 JP WO2013080284A1
- Authority
- JP
- Japan
- Prior art keywords
- liquid seasoning
- sesame
- acid
- fragrance
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000011194 food seasoning agent Nutrition 0.000 title claims abstract description 97
- 239000007788 liquid Substances 0.000 title claims abstract description 96
- 235000003434 Sesamum indicum Nutrition 0.000 title claims abstract description 95
- 230000002378 acidificating effect Effects 0.000 title abstract description 25
- 244000000231 Sesamum indicum Species 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 104
- 241000207961 Sesamum Species 0.000 claims abstract description 94
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims abstract description 56
- UHEPJGULSIKKTP-UHFFFAOYSA-N sulcatone Chemical compound CC(C)=CCCC(C)=O UHEPJGULSIKKTP-UHFFFAOYSA-N 0.000 claims abstract description 50
- WWZKQHOCKIZLMA-UHFFFAOYSA-N Caprylic acid Natural products CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims abstract description 28
- GONOPSZTUGRENK-UHFFFAOYSA-N benzyl(trichloro)silane Chemical compound Cl[Si](Cl)(Cl)CC1=CC=CC=C1 GONOPSZTUGRENK-UHFFFAOYSA-N 0.000 claims abstract description 28
- FUZZWVXGSFPDMH-UHFFFAOYSA-N n-hexanoic acid Natural products CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims abstract description 28
- OHEFFKYYKJVVOX-UHFFFAOYSA-N sulcatol Natural products CC(O)CCC=C(C)C OHEFFKYYKJVVOX-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000000796 flavoring agent Substances 0.000 claims description 23
- 235000019634 flavors Nutrition 0.000 claims description 23
- 238000000034 method Methods 0.000 claims description 19
- 102000002322 Egg Proteins Human genes 0.000 claims description 18
- 108010000912 Egg Proteins Proteins 0.000 claims description 18
- 235000013345 egg yolk Nutrition 0.000 claims description 18
- 210000002969 egg yolk Anatomy 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims description 11
- 239000004334 sorbic acid Substances 0.000 claims description 11
- 235000010199 sorbic acid Nutrition 0.000 claims description 11
- 229940075582 sorbic acid Drugs 0.000 claims description 11
- 150000003839 salts Chemical class 0.000 claims description 7
- ZIIUUSVHCHPIQD-UHFFFAOYSA-N 2,4,6-trimethyl-N-[3-(trifluoromethyl)phenyl]benzenesulfonamide Chemical compound CC1=CC(C)=CC(C)=C1S(=O)(=O)NC1=CC=CC(C(F)(F)F)=C1 ZIIUUSVHCHPIQD-UHFFFAOYSA-N 0.000 claims description 5
- 102000015439 Phospholipases Human genes 0.000 claims description 5
- 108010064785 Phospholipases Proteins 0.000 claims description 5
- 239000007790 solid phase Substances 0.000 claims description 5
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 claims description 3
- 239000003205 fragrance Substances 0.000 abstract description 54
- 238000003860 storage Methods 0.000 abstract description 11
- 230000007774 longterm Effects 0.000 abstract description 9
- 230000000694 effects Effects 0.000 description 11
- 239000003921 oil Substances 0.000 description 9
- 235000019198 oils Nutrition 0.000 description 9
- 238000002156 mixing Methods 0.000 description 8
- 239000004278 EU approved seasoning Substances 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 7
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 239000003925 fat Substances 0.000 description 6
- 235000019197 fats Nutrition 0.000 description 6
- 238000004128 high performance liquid chromatography Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 5
- 150000007524 organic acids Chemical class 0.000 description 5
- 235000019482 Palm oil Nutrition 0.000 description 4
- 235000014113 dietary fatty acids Nutrition 0.000 description 4
- 235000021186 dishes Nutrition 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 229930195729 fatty acid Natural products 0.000 description 4
- 239000000194 fatty acid Substances 0.000 description 4
- 229940093915 gynecological organic acid Drugs 0.000 description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 4
- 235000005985 organic acids Nutrition 0.000 description 4
- 239000002540 palm oil Substances 0.000 description 4
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 4
- 238000002470 solid-phase micro-extraction Methods 0.000 description 4
- -1 sucrose fatty acid ester Chemical class 0.000 description 4
- 229930006000 Sucrose Natural products 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 235000012000 cholesterol Nutrition 0.000 description 3
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 description 3
- 230000001804 emulsifying effect Effects 0.000 description 3
- 238000002372 labelling Methods 0.000 description 3
- 230000014759 maintenance of location Effects 0.000 description 3
- 238000004949 mass spectrometry Methods 0.000 description 3
- 235000013923 monosodium glutamate Nutrition 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 229940073490 sodium glutamate Drugs 0.000 description 3
- 235000012424 soybean oil Nutrition 0.000 description 3
- 239000003549 soybean oil Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000005720 sucrose Substances 0.000 description 3
- 239000003760 tallow Substances 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241000287828 Gallus gallus Species 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 2
- 244000070406 Malus silvestris Species 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 235000019484 Rapeseed oil Nutrition 0.000 description 2
- 240000003768 Solanum lycopersicum Species 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 235000014121 butter Nutrition 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- 235000015165 citric acid Nutrition 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000013505 freshwater Substances 0.000 description 2
- 235000015203 fruit juice Nutrition 0.000 description 2
- JHHZQADGLDKIPM-UHFFFAOYSA-N hept-3-en-2-one Chemical compound CCCC=CC(C)=O JHHZQADGLDKIPM-UHFFFAOYSA-N 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 239000004310 lactic acid Substances 0.000 description 2
- 235000014655 lactic acid Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000691 measurement method Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 235000011803 sesame oil Nutrition 0.000 description 2
- 239000008159 sesame oil Substances 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229920001285 xanthan gum Polymers 0.000 description 2
- 239000000230 xanthan gum Substances 0.000 description 2
- 229940082509 xanthan gum Drugs 0.000 description 2
- 235000010493 xanthan gum Nutrition 0.000 description 2
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 description 1
- ASWBNKHCZGQVJV-UHFFFAOYSA-N (3-hexadecanoyloxy-2-hydroxypropyl) 2-(trimethylazaniumyl)ethyl phosphate Chemical compound CCCCCCCCCCCCCCCC(=O)OCC(O)COP([O-])(=O)OCC[N+](C)(C)C ASWBNKHCZGQVJV-UHFFFAOYSA-N 0.000 description 1
- WSWCOQWTEOXDQX-MQQKCMAXSA-M (E,E)-sorbate Chemical compound C\C=C\C=C\C([O-])=O WSWCOQWTEOXDQX-MQQKCMAXSA-M 0.000 description 1
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 1
- 235000009434 Actinidia chinensis Nutrition 0.000 description 1
- 235000009436 Actinidia deliciosa Nutrition 0.000 description 1
- 235000019489 Almond oil Nutrition 0.000 description 1
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Natural products OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 1
- 244000056139 Brassica cretica Species 0.000 description 1
- 235000003351 Brassica cretica Nutrition 0.000 description 1
- 240000007124 Brassica oleracea Species 0.000 description 1
- 235000003899 Brassica oleracea var acephala Nutrition 0.000 description 1
- 235000011301 Brassica oleracea var capitata Nutrition 0.000 description 1
- 235000001169 Brassica oleracea var oleracea Nutrition 0.000 description 1
- 235000003343 Brassica rupestris Nutrition 0.000 description 1
- 235000002566 Capsicum Nutrition 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 235000011201 Ginkgo Nutrition 0.000 description 1
- 235000008100 Ginkgo biloba Nutrition 0.000 description 1
- 244000194101 Ginkgo biloba Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 235000003228 Lactuca sativa Nutrition 0.000 description 1
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 1
- YBHQCJILTOVLHD-YVMONPNESA-N Mirin Chemical compound S1C(N)=NC(=O)\C1=C\C1=CC=C(O)C=C1 YBHQCJILTOVLHD-YVMONPNESA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 235000019483 Peanut oil Nutrition 0.000 description 1
- 239000006002 Pepper Substances 0.000 description 1
- 235000016761 Piper aduncum Nutrition 0.000 description 1
- 240000003889 Piper guineense Species 0.000 description 1
- 235000017804 Piper guineense Nutrition 0.000 description 1
- 235000008184 Piper nigrum Nutrition 0.000 description 1
- 235000019485 Safflower oil Nutrition 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 241000271567 Struthioniformes Species 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 235000019486 Sunflower oil Nutrition 0.000 description 1
- 235000006468 Thea sinensis Nutrition 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 239000008168 almond oil Substances 0.000 description 1
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 description 1
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 235000021016 apples Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000007961 artificial flavoring substance Substances 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- 235000021302 avocado oil Nutrition 0.000 description 1
- 239000008163 avocado oil Substances 0.000 description 1
- 239000000022 bacteriostatic agent Substances 0.000 description 1
- 235000013527 bean curd Nutrition 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 1
- QKSKPIVNLNLAAV-UHFFFAOYSA-N bis(2-chloroethyl) sulfide Chemical compound ClCCSCCCl QKSKPIVNLNLAAV-UHFFFAOYSA-N 0.000 description 1
- 235000007215 black sesame Nutrition 0.000 description 1
- 235000020279 black tea Nutrition 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 235000013351 cheese Nutrition 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 235000005687 corn oil Nutrition 0.000 description 1
- 239000002285 corn oil Substances 0.000 description 1
- 235000012343 cottonseed oil Nutrition 0.000 description 1
- 239000002385 cottonseed oil Substances 0.000 description 1
- 235000015140 cultured milk Nutrition 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 235000021323 fish oil Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000012041 food component Nutrition 0.000 description 1
- 235000012027 fruit salads Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 235000021552 granulated sugar Nutrition 0.000 description 1
- 239000008169 grapeseed oil Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000000752 ionisation method Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- TYQCGQRIZGCHNB-JLAZNSOCSA-N l-ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(O)=C(O)C1=O TYQCGQRIZGCHNB-JLAZNSOCSA-N 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 238000004811 liquid chromatography Methods 0.000 description 1
- 239000001630 malic acid Substances 0.000 description 1
- 235000011090 malic acid Nutrition 0.000 description 1
- 235000010746 mayonnaise Nutrition 0.000 description 1
- 239000008268 mayonnaise Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 150000004667 medium chain fatty acids Chemical class 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 235000010460 mustard Nutrition 0.000 description 1
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 description 1
- 125000004365 octenyl group Chemical group C(=CCCCCCC)* 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 239000008601 oleoresin Substances 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 238000004987 plasma desorption mass spectroscopy Methods 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 235000015277 pork Nutrition 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 150000003216 pyrazines Chemical class 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 235000021067 refined food Nutrition 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 229940075554 sorbate Drugs 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 235000013555 soy sauce Nutrition 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 235000012033 vegetable salad Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L25/00—Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof
- A23L25/30—Mashed or comminuted products, e.g. pulp, pastes, meal, powders; Products made therefrom, e.g. blocks, flakes, snacks; Liquid or semi-liquid products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Seasonings (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
(a)ブタン酸:0.0001〜0.02
(b)ヘキサン酸:0.0001〜0.05
(c)6−メチル−5−ヘプテン−2−オン:0.00001〜0.005
のいずれか一つ以上を満たすことが好ましい。
本発明の液状調味料は、胡麻と、酢酸と、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンからなる群から選択される少なくとも1種とを含んでなるものである。ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンからなる群から選択される少なくとも2種を含むことが好ましく、3種を含むことがより好ましい。液状調味料は、酢酸を配合することで、pHが、好ましくは6.5以下、より好ましくは4.6以下となっている酸性液状調味料である。胡麻を含有し、かつ酢酸を配合することで、作り立ては大変美味しいものの、長期保管後において胡麻特有の芳香が経時的に消失し易い問題があったが、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンからなる群から選択される少なくとも1種を含有することでこの問題を解決することができた。
(a)ブタン酸:0.0001〜0.02
(b)ヘキサン酸:0.0001〜0.05
(c)6−メチル−5−ヘプテン−2−オン:0.00001〜0.005
のいずれか一つ以上を満たすことが好ましく、
(a)ブタン酸:0.0005〜0.01
(b)ヘキサン酸:0.001〜0.02
(c)6−メチル−5−ヘプテン−2−オン:0.00003〜0.0015
のいずれか一つ以上を満たすことがより好ましく、
(a)ブタン酸:0.0007〜0.005
(b)ヘキサン酸:0.0015〜0.01
(c)6−メチル−5−ヘプテン−2−オン:0.00005〜0.001
のいずれか一つ以上を満たすことが特に好ましい。
酢酸のピーク面積に対する、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンの各ピーク面積の比が上記範囲程度であれば、胡麻特有の芳香をより強く感じることができる。
本発明の液状調味料中の酢酸の含有量の測定方法は、「栄養表示のための成分分析のポイント」(財団法人日本食品分析センター編、2007年10月20日発行)に開示されている、高速液体クロマトグラフ法(HPLC法)に基づいて行う。具体的には、例えば、有機酸類を最終濃度が0.5質量%となるように加えた過塩素酸で抽出し、有機酸類の紫外部吸収を利用して高速液体クロマトグラフ法(HPLC法)で分別定量する。
(1)香気成分の分離濃縮方法
SPMEファイバーと揮発性成分抽出装置を用い、以下の条件に従って、固相マイクロ抽出法で香気成分の分離濃縮を行う。
<固相マイクロ抽出条件>
・SPMEファイバー StableFlex 50/30μm,DVB/Carboxen/PDMS(Sigma−Aldrich社製)
・揮発性成分抽出装置 Combi PAL、CTC Analitics製
・予備加温 40℃,15min
・攪拌速度 300rpm
・揮発性成分抽出 40℃,20min
・脱着時間 10min
(2)香気成分の測定方法
ガスクロマトグラフ法及び質量分析法を用い、以下の条件に従って、液状調味料中の酢酸のピーク面積に対する、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンの各ピーク面積の比を測定する。
<ガスクロマトグラフ条件>
・測定機器 Agilent 6890N(Agilent Technologies社製)
・カラム SOLGEL−WAX(SGE社製)
長さ30m,口径0.25mm,膜厚0.25μm
・温度条件 35℃(5min)保持→120℃まで5℃/min昇温
→220℃まで15℃/min昇温→ 6min保持
・キャリアー Heガス、 ガス流量1.0mL/min
<質量分析条件>
・質量分析計 Agilent 5973N(Agilent Technologies社製)
・スキャン質量 m/z 29.0〜350.0
・イオン化方式 EI(イオン化電圧70eV)
まず、撹拌タンクに、すり胡麻3質量%、酢酸0.9質量%、グラニュ糖5質量%、グルタミン酸ナトリウム0.5質量%、ホスフォリパーゼA処理された卵黄(キユーピー(株)製)0.2質量%、キサンタンガム0.1質量%、胡麻風味香料(ジボダン社製、Nature identical flavor)0.1質量%、及び清水70.2質量%を投入して均一に混合後、撹拌しながら大豆油10質量%及びパーム油10質量%を注加して乳化処理を施し、液状調味料(水中油型乳化液状調味料)を調製した。次に、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンからなる群から選択される少なくとも1種をそれぞれ添加混合して、例1〜25の25種類の胡麻含有酸性液状調味料を調製した。各胡麻含有酸性液状調味料の香気成分を上記の固相マイクロ抽出−ガスクロマトグラフ質量分析法で測定し、酢酸、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンのピーク面積、並びに、酢酸のピーク面積に対する、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンの各ピーク面積の比を表1〜4に示した。また、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンのいずれも添加していない上記の液状調味料を対照品(例26)とした。
5:胡麻特有の芳香が対照品に比べて大変強い。
4:胡麻特有の芳香が対照品に比べてかなり強い。
3:胡麻特有の芳香が対照品に比べて強い。
2:胡麻特有の芳香が対照品に比べてやや強い。
1:胡麻特有の芳香が対照品に比べて少し強い。
Claims (8)
- 胡麻と、酢酸と、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンからなる群から選択される少なくとも1種とを含んでなる、液状調味料。
- 前記液状調味料の香気成分を固相マイクロ抽出−ガスクロマトグラフ質量分析法で測定した場合に、酢酸のピーク面積に対する、ブタン酸、ヘキサン酸、及び6−メチル−5−ヘプテン−2−オンの各ピーク面積の比が、下記の条件(a)〜(c):
(a)ブタン酸:0.0001〜0.02
(b)ヘキサン酸:0.0001〜0.05
(c)6−メチル−5−ヘプテン−2−オン:0.00001〜0.005
のいずれか一つ以上を満たす、請求項1に記載の液状調味料。 - 前記酢酸の含有量が、前記液状調味料の全量に対して、0.1〜2質量%である、請求項1又は2に記載の液状調味料。
- ソルビン酸及び/又はその塩をさらに含んでなる、請求項1〜3のいずれか一項に記載の液状調味料。
- 胡麻風味香料をさらに含んでなる、請求項1〜4のいずれか一項に記載の液状調味料。
- 水中油型乳化液状調味料である、請求項1〜5のいずれか一項に記載の液状調味料。
- 卵黄をさらに含んでなる、請求項1〜6のいずれか一項に記載の液状調味料。
- 前記卵黄がホスフォリパーゼA処理された卵黄である、請求項1〜7のいずれか一項に記載の液状調味料。
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/JP2011/077410 WO2013080284A1 (ja) | 2011-11-28 | 2011-11-28 | 胡麻含有酸性液状調味料 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP5048170B1 JP5048170B1 (ja) | 2012-10-17 |
JPWO2013080284A1 true JPWO2013080284A1 (ja) | 2015-04-27 |
Family
ID=47189441
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012516427A Active JP5048170B1 (ja) | 2011-11-28 | 2011-11-28 | 胡麻含有酸性液状調味料 |
Country Status (3)
Country | Link |
---|---|
JP (1) | JP5048170B1 (ja) |
CN (1) | CN103260435B (ja) |
WO (1) | WO2013080284A1 (ja) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2015039351A (ja) * | 2013-08-22 | 2015-03-02 | キユーピー株式会社 | 乳化状調味料 |
JP2015100335A (ja) * | 2013-11-27 | 2015-06-04 | キユーピー株式会社 | 酸性水中油型乳化調味料 |
RU2746605C1 (ru) * | 2017-08-31 | 2021-04-16 | Кьюпай Корпорейшн | Жидкая приправа |
JP6518363B1 (ja) * | 2018-06-05 | 2019-05-22 | キユーピー株式会社 | 液状調味料 |
JP6684955B1 (ja) * | 2019-10-30 | 2020-04-22 | キユーピー株式会社 | 調理ソース |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS57163461A (en) * | 1981-04-02 | 1982-10-07 | Takeshi Nishinakayama | Preparation of vineger containing favorite seasoning and spice |
JP3198383B2 (ja) * | 1997-07-03 | 2001-08-13 | 亀田鋼材株式会社 | 覆工板用外枠材 |
JPH11290036A (ja) * | 1998-04-10 | 1999-10-26 | Nakano Vinegar Co Ltd | 練りゴマ含有食品 |
JP2000217539A (ja) * | 1999-01-27 | 2000-08-08 | Kikkoman Corp | ゴマ含有液状調味料の製造方法 |
KR101255360B1 (ko) * | 2004-11-12 | 2013-04-17 | 카오카부시키가이샤 | 액체 조미료 |
JP4944662B2 (ja) * | 2007-04-24 | 2012-06-06 | 小川香料株式会社 | 低級脂肪酸を添加することを特徴とする飲食品の香味増強方法及び香味増強された飲食品並びに香味料組成物 |
CN101999624A (zh) * | 2009-09-01 | 2011-04-06 | 上海太太乐食品有限公司 | 一种液体调味料及其制备工艺 |
JP5164960B2 (ja) * | 2009-11-13 | 2013-03-21 | キユーピー株式会社 | 容器入り酸性液状食品の製造方法 |
JP5731987B2 (ja) * | 2009-11-27 | 2015-06-10 | キユーピー株式会社 | ゴマ含有酸性乳化液状調味料 |
-
2011
- 2011-11-28 WO PCT/JP2011/077410 patent/WO2013080284A1/ja active Application Filing
- 2011-11-28 JP JP2012516427A patent/JP5048170B1/ja active Active
- 2011-11-28 CN CN201180023904.0A patent/CN103260435B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN103260435B (zh) | 2014-08-13 |
CN103260435A (zh) | 2013-08-21 |
WO2013080284A1 (ja) | 2013-06-06 |
JP5048170B1 (ja) | 2012-10-17 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP6165138B2 (ja) | 胡麻含有酸性液状調味料 | |
JP5048170B1 (ja) | 胡麻含有酸性液状調味料 | |
JP6633368B2 (ja) | 酸性液状調味料 | |
TWI733041B (zh) | 液狀調味料 | |
JP6270733B2 (ja) | 胡麻含有酸性液状調味料 | |
JPWO2014083663A1 (ja) | マヨネーズ様食品 | |
JP2017099307A (ja) | 酸性液状調味料 | |
JPWO2016175323A1 (ja) | 香料組成物 | |
JP6276903B1 (ja) | 酸性水中油型乳化調味料及びその製造方法 | |
JP5738579B2 (ja) | 液体調味料 | |
JP6563620B1 (ja) | 液状調味料及びその製造方法 | |
JP2013111014A (ja) | 酸性水中油型乳化液状調味料 | |
JP2019088338A (ja) | 酸性水中油型乳化液状調味料の製造方法 | |
JP7084562B1 (ja) | 酸性液状調味料 | |
TWI593357B (zh) | Flavored acidic liquid seasoning containing flax | |
JP2016135148A (ja) | 酸性水中油型乳化液状調味料 | |
TWI598045B (zh) | Flax acid-containing liquid seasoning | |
JP6518363B1 (ja) | 液状調味料 | |
JP2012235721A (ja) | 酸性液状調味料 | |
JP2021090468A (ja) | 酸性水中油型乳化液状調味料の製造方法 | |
JP4902695B2 (ja) | 酸性水中油型乳化状調味料 | |
JP2017112889A (ja) | 常温喫食用レトルト食品用ゲル状香味料組成物 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20120619 |
|
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20120718 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20150727 Year of fee payment: 3 |
|
R150 | Certificate of patent or registration of utility model |
Ref document number: 5048170 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |