JPH0146495B2 - - Google Patents
Info
- Publication number
- JPH0146495B2 JPH0146495B2 JP62254888A JP25488887A JPH0146495B2 JP H0146495 B2 JPH0146495 B2 JP H0146495B2 JP 62254888 A JP62254888 A JP 62254888A JP 25488887 A JP25488887 A JP 25488887A JP H0146495 B2 JPH0146495 B2 JP H0146495B2
- Authority
- JP
- Japan
- Prior art keywords
- acid ester
- triphenylphosphine
- reaction
- iodine
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- RIOQSEWOXXDEQQ-UHFFFAOYSA-N triphenylphosphine Chemical compound C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 RIOQSEWOXXDEQQ-UHFFFAOYSA-N 0.000 claims description 10
- 125000001931 aliphatic group Chemical group 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 6
- -1 sulfonic acid halide Chemical class 0.000 claims description 4
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 claims description 3
- 125000000962 organic group Chemical group 0.000 claims description 3
- BUUPQKDIAURBJP-UHFFFAOYSA-N sulfinic acid Chemical compound OS=O BUUPQKDIAURBJP-UHFFFAOYSA-N 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 150000003453 sulfinic acid esters Chemical class 0.000 claims description 2
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 12
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 4
- 239000003153 chemical reaction reagent Substances 0.000 description 4
- 239000011630 iodine Substances 0.000 description 4
- 229910052740 iodine Inorganic materials 0.000 description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- BLXSFCHWMBESKV-UHFFFAOYSA-N 1-iodopentane Chemical compound CCCCCI BLXSFCHWMBESKV-UHFFFAOYSA-N 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 150000007824 aliphatic compounds Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000003710 aryl alkyl group Chemical group 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000007810 chemical reaction solvent Substances 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- FIQMHBFVRAXMOP-UHFFFAOYSA-N triphenylphosphane oxide Chemical compound C=1C=CC=CC=1P(C=1C=CC=CC=1)(=O)C1=CC=CC=C1 FIQMHBFVRAXMOP-UHFFFAOYSA-N 0.000 description 1
- VYNGFCUGSYEOOZ-UHFFFAOYSA-N triphenylphosphine sulfide Chemical compound C=1C=CC=CC=1P(C=1C=CC=CC=1)(=S)C1=CC=CC=C1 VYNGFCUGSYEOOZ-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62254888A JPH0196142A (ja) | 1981-03-02 | 1987-10-09 | 脂肪族ヨウ化物の製法 |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2950481A JPS57144230A (en) | 1981-03-02 | 1981-03-02 | Production of aliphatic iodide |
JP62254888A JPH0196142A (ja) | 1981-03-02 | 1987-10-09 | 脂肪族ヨウ化物の製法 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2950481A Division JPS57144230A (en) | 1981-03-02 | 1981-03-02 | Production of aliphatic iodide |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH0196142A JPH0196142A (ja) | 1989-04-14 |
JPH0146495B2 true JPH0146495B2 (es) | 1989-10-09 |
Family
ID=26367713
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP62254888A Granted JPH0196142A (ja) | 1981-03-02 | 1987-10-09 | 脂肪族ヨウ化物の製法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH0196142A (es) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2811131B2 (ja) * | 1991-04-26 | 1998-10-15 | 三菱電機株式会社 | 半導体装置の配線接続構造およびその製造方法 |
EP0558304B1 (en) * | 1992-02-28 | 2000-01-19 | STMicroelectronics, Inc. | Method of forming submicron contacts |
JP4770202B2 (ja) * | 2005-03-08 | 2011-09-14 | ダイキン工業株式会社 | 含フッ素ハロゲン化物の製造方法 |
-
1987
- 1987-10-09 JP JP62254888A patent/JPH0196142A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPH0196142A (ja) | 1989-04-14 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CA1340549C (en) | Method of preparing sphingosine derivatives | |
JPH0146495B2 (es) | ||
CA1201118A (en) | Conjugate addition of organocuprates generated from copper (i) cyanide and vinyl stannanes useful in prostaglandin analog synthesis | |
JPS64932B2 (es) | ||
JP3091022B2 (ja) | グルタル酸誘導体の製造方法 | |
SU1643516A1 (ru) | Способ получени спиртов | |
JPS5944315B2 (ja) | 2−ペンチニルエ−テルの製造法 | |
Gilman et al. | Studies in the Benzosilacycloalkene Series. III. Reactions of (o-Chlorophenyl) alkyl Derivatives with Magnesium and Lithium | |
HU206189B (en) | Process for producing glutaric acid derivatives | |
JPH0142253B2 (es) | ||
JPS6366176A (ja) | ヒドロキノン誘導体の製造方法 | |
JP2003034676A (ja) | スチレンスルホン酸エステル類の製造方法 | |
US4052434A (en) | Prostaglandin intermediates | |
JP2864985B2 (ja) | トリ(第2級アルキル)シラン化合物の製造方法 | |
JP2521100B2 (ja) | ハロゲノアルキルフルフリルアルコ−ル類およびその製造法 | |
JPS58162545A (ja) | 化合物1−デシロキシ−4−〔(7−オキサ−4−オクチニル)オキシ〕ベンゼンの製造方法 | |
CN113527178A (zh) | 对称二杂二硫类化合物及其合成方法和应用 | |
SU407917A1 (ru) | Способ получения 2-окса- или 2-тиаалкилдифенилфосфиноксидов | |
JPS63258836A (ja) | エテン誘導体の製造方法 | |
JP2614108B2 (ja) | スルフェニルオキシムカーバメート誘導体の製造方法 | |
JPH0141144B2 (es) | ||
JPS58164536A (ja) | 化合物1−デシロキシ−4−〔(7−オキサ−4−オクチニル)オキシ〕ベンゼンの製造方法 | |
JPH0680616A (ja) | 3、3−ジフルオロ−2−プロペンアミド誘導体の製造方法 | |
JPS5933571B2 (ja) | ジヒドロラバンジユラ−ルの合成法 | |
JPS6024796B2 (ja) | ボラン錯化合物及びその製造法 |