JP6726095B2 - アレルゲン低減化組成物、それを含む噴霧剤と表面加工剤、アレルゲン低減化方法、アレルゲン低減化された繊維構造体と建築用内装材 - Google Patents
アレルゲン低減化組成物、それを含む噴霧剤と表面加工剤、アレルゲン低減化方法、アレルゲン低減化された繊維構造体と建築用内装材 Download PDFInfo
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- JP6726095B2 JP6726095B2 JP2016508755A JP2016508755A JP6726095B2 JP 6726095 B2 JP6726095 B2 JP 6726095B2 JP 2016508755 A JP2016508755 A JP 2016508755A JP 2016508755 A JP2016508755 A JP 2016508755A JP 6726095 B2 JP6726095 B2 JP 6726095B2
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- reducing
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- reducing composition
- zinc
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- JWZXKXIUSSIAMR-UHFFFAOYSA-N methylene bis(thiocyanate) Chemical compound N#CSCSC#N JWZXKXIUSSIAMR-UHFFFAOYSA-N 0.000 description 1
- 235000013384 milk substitute Nutrition 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 229920006173 natural rubber latex Polymers 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- LAIZPRYFQUWUBN-UHFFFAOYSA-L nickel chloride hexahydrate Chemical compound O.O.O.O.O.O.[Cl-].[Cl-].[Ni+2] LAIZPRYFQUWUBN-UHFFFAOYSA-L 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 150000002903 organophosphorus compounds Chemical class 0.000 description 1
- 235000010292 orthophenyl phenol Nutrition 0.000 description 1
- 239000004306 orthophenyl phenol Substances 0.000 description 1
- ADGFKRMKSIAMAI-UHFFFAOYSA-L oxygen(2-);zirconium(4+);chloride;hydroxide Chemical compound [OH-].[O-2].[Cl-].[Zr+4] ADGFKRMKSIAMAI-UHFFFAOYSA-L 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 description 1
- 229960000490 permethrin Drugs 0.000 description 1
- RLLPVAHGXHCWKJ-UHFFFAOYSA-N permethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OCC1=CC=CC(OC=2C=CC=CC=2)=C1 RLLPVAHGXHCWKJ-UHFFFAOYSA-N 0.000 description 1
- 229960000969 phenyl salicylate Drugs 0.000 description 1
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 239000011120 plywood Substances 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000656 polylysine Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 239000011970 polystyrene sulfonate Substances 0.000 description 1
- 229960002796 polystyrene sulfonate Drugs 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 description 1
- 229940070846 pyrethrins Drugs 0.000 description 1
- DWFZBUWUXWZWKD-UHFFFAOYSA-N pyridaben Chemical compound C1=CC(C(C)(C)C)=CC=C1CSC1=C(Cl)C(=O)N(C(C)(C)C)N=C1 DWFZBUWUXWZWKD-UHFFFAOYSA-N 0.000 description 1
- YBBJKCMMCRQZMA-UHFFFAOYSA-N pyrithione Chemical compound ON1C=CC=CC1=S YBBJKCMMCRQZMA-UHFFFAOYSA-N 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 239000005871 repellent Substances 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 description 1
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 description 1
- 229960003656 ricinoleic acid Drugs 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000002455 scale inhibitor Substances 0.000 description 1
- 150000003325 scandium Chemical class 0.000 description 1
- JXOHGGNKMLTUBP-HSUXUTPPSA-N shikimic acid Chemical compound O[C@@H]1CC(C(O)=O)=C[C@@H](O)[C@H]1O JXOHGGNKMLTUBP-HSUXUTPPSA-N 0.000 description 1
- JXOHGGNKMLTUBP-JKUQZMGJSA-N shikimic acid Natural products O[C@@H]1CC(C(O)=O)=C[C@H](O)[C@@H]1O JXOHGGNKMLTUBP-JKUQZMGJSA-N 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 229940047908 strontium chloride hexahydrate Drugs 0.000 description 1
- AMGRXJSJSONEEG-UHFFFAOYSA-L strontium dichloride hexahydrate Chemical compound O.O.O.O.O.O.Cl[Sr]Cl AMGRXJSJSONEEG-UHFFFAOYSA-L 0.000 description 1
- 159000000008 strontium salts Chemical class 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- ZZYSLNWGKKDOML-UHFFFAOYSA-N tebufenpyrad Chemical compound CCC1=NN(C)C(C(=O)NCC=2C=CC(=CC=2)C(C)(C)C)=C1Cl ZZYSLNWGKKDOML-UHFFFAOYSA-N 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- WJCNZQLZVWNLKY-UHFFFAOYSA-N thiabendazole Chemical compound S1C=NC(C=2NC3=CC=CC=C3N=2)=C1 WJCNZQLZVWNLKY-UHFFFAOYSA-N 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- ODBLHEXUDAPZAU-UHFFFAOYSA-N threo-D-isocitric acid Natural products OC(=O)C(O)C(C(O)=O)CC(O)=O ODBLHEXUDAPZAU-UHFFFAOYSA-N 0.000 description 1
- FRNOGLGSGLTDKL-UHFFFAOYSA-N thulium atom Chemical class [Tm] FRNOGLGSGLTDKL-UHFFFAOYSA-N 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- KPZSTOVTJYRDIO-UHFFFAOYSA-K trichlorocerium;heptahydrate Chemical compound O.O.O.O.O.O.O.Cl[Ce](Cl)Cl KPZSTOVTJYRDIO-UHFFFAOYSA-K 0.000 description 1
- HFEOHRWLEGXZHW-UHFFFAOYSA-K trichlorodysprosium;hexahydrate Chemical compound O.O.O.O.O.O.[Cl-].[Cl-].[Cl-].[Dy+3] HFEOHRWLEGXZHW-UHFFFAOYSA-K 0.000 description 1
- UJBPGOAZQSYXNT-UHFFFAOYSA-K trichloroerbium;hexahydrate Chemical compound O.O.O.O.O.O.[Cl-].[Cl-].[Cl-].[Er+3] UJBPGOAZQSYXNT-UHFFFAOYSA-K 0.000 description 1
- PNYPSKHTTCTAMD-UHFFFAOYSA-K trichlorogadolinium;hexahydrate Chemical compound O.O.O.O.O.O.[Cl-].[Cl-].[Cl-].[Gd+3] PNYPSKHTTCTAMD-UHFFFAOYSA-K 0.000 description 1
- BUQFCXABQYNXLP-UHFFFAOYSA-K trichloroholmium;hexahydrate Chemical compound O.O.O.O.O.O.Cl[Ho](Cl)Cl BUQFCXABQYNXLP-UHFFFAOYSA-K 0.000 description 1
- TXVNDKHBDRURNU-UHFFFAOYSA-K trichlorosamarium;hexahydrate Chemical compound O.O.O.O.O.O.[Cl-].[Cl-].[Cl-].[Sm+3] TXVNDKHBDRURNU-UHFFFAOYSA-K 0.000 description 1
- 229920003176 water-insoluble polymer Polymers 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
- XNRYBAOKBQZJND-UHFFFAOYSA-N ytterbium(3+) trinitrate tetrahydrate Chemical compound O.O.O.O.[Yb+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O XNRYBAOKBQZJND-UHFFFAOYSA-N 0.000 description 1
- 150000003746 yttrium Chemical class 0.000 description 1
- XDWXRAYGALQIFG-UHFFFAOYSA-L zinc;propanoate Chemical compound [Zn+2].CCC([O-])=O.CCC([O-])=O XDWXRAYGALQIFG-UHFFFAOYSA-L 0.000 description 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1
- 229930007845 β-thujaplicin Natural products 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/22—Phase substances, e.g. smokes, aerosols or sprayed or atomised substances
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/14—Disinfection, sterilisation or deodorisation of air using sprayed or atomised substances including air-liquid contact processes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/24—Heavy metals; Compounds thereof
- A61K33/30—Zinc; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/24—Heavy metals; Compounds thereof
- A61K33/34—Copper; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/18—Liquid substances or solutions comprising solids or dissolved gases
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/155—Halides of elements of Groups 2 or 12 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
- D06M11/42—Oxides or hydroxides of copper, silver or gold
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
Landscapes
- Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Chemical And Physical Treatments For Wood And The Like (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Building Environments (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Description
塩化セリウム七水和物(和光純薬工業株式会社製)
塩化サマリウム六水和物(和光純薬工業株式会社製)
塩化ガドリニウム六水和物(和光純薬工業株式会社製)
塩化ジスプロシウム六水和物(和光純薬工業株式会社製)
塩化ホルミウム六水和物(和光純薬工業株式会社製)
塩化エルビウム六水和物(和光純薬工業株式会社製)
塩化イッテルビウム六水和物(和光純薬工業株式会社製)
硝酸イッテルビウム四水和物(和光純薬工業株式会社製)
酸化ランタン(和光純薬工業株式会社製)
酸化ネオジム(和光純薬工業株式会社製)
グルコン酸亜鉛(ヘルシャスZn(登録商標)、扶桑化学工業株式会社製)
グルコン酸銅(和光純薬工業株式会社製)
塩化亜鉛(和光純薬工業株式会社製)
硫酸銅五水和物(和光純薬工業株式会社製)
塩化カルシウム二水和物(和光純薬工業株式会社製)
塩化ストロンチウム六水和物(和光純薬工業株式会社製)
塩化アルミニウム六水和物(和光純薬工業株式会社製)
硝酸ガリウムn水和物(n=7〜9)(和光純薬工業株式会社製)
塩化インジウム四水和物(稀産金属株式会社製)
塩化コバルト六水和物(OUTKUMPU社製)
塩化ニッケル六水和物(和光純薬工業株式会社製)
塩基性塩化ジルコニウム(約45%)(ジルコゾールZC−2(登録商標)、第一稀元素化学工業株式会社製)
90%乳酸(株式会社武蔵野化学研究所製)
リンゴ酸(DL−りんご酸:和光純薬工業株式会社製)
50%グルコン酸水溶液(和光純薬工業株式会社製)
タンニン酸(富士化学工業株式会社製)
玉入れ冷却管を取り付けた100mL容量の三角フラスコに、90%乳酸溶液4.5gとイオン交換水69.0gを混合し、さらに酸化ランタン1.2gを添加した。湯浴中で75℃に加温して撹拌を3時間継続し、酸化ランタンを溶解させた。放冷し、約4%の乳酸ランタンを含有する水溶液を得た。
玉入れ冷却管を取り付けた100mL容量の三角フラスコに、90%乳酸10.4gとイオン交換水29.4gを混合し、さらに酸化ネオジム4.2gを添加した。湯浴中で75℃に加温し、1時間撹拌後、硫酸1滴を添加した。さらに1時間撹拌を継続し、酸化ネオジムを溶解させた。冷却後に取り出してイオン交換水を用いて総量を120gに希釈し、約4%の乳酸ネオジムを含有する紫色の水溶液を得た。
玉入れ冷却管を取り付けた500mL容量の三角フラスコに、50%グルコン酸水溶液20.5gとイオン交換水300gを混合し、さらに酸化ネオジム2.2gを添加した。湯浴中で75℃に加温し、1時間撹拌後、硫酸1滴を添加した。さらに3時間撹拌を継続し、イオン交換水を用いて総量を480gに希釈し、酸化ネオジムを溶解させた。放冷し、約2%のグルコン酸ネオジムを含有する紫色の溶液を得た(比較例24)。
玉入れ冷却管を取り付けた300mL容量の三角フラスコに、リンゴ酸3.1gとイオン交換水200gを混合し、さらに酸化ランタン1.2gを添加した。湯浴中で75℃に加温し、2時間撹拌後、硫酸1滴を添加した。さらに3時間撹拌し、酸化ランタンを溶解させた。放冷し、約2%のリンゴ酸ランタンを含有する水溶液を得た(比較例39)。
玉入れ冷却管を取り付けた300mL容量の三角フラスコに、リンゴ酸3.1gとイオン交換水200gを混合し、さらに酸化ネオジム1.2gを添加した。湯浴中で75℃に加温し、2時間撹拌後、硫酸1滴を添加した。さらに3時間撹拌し、酸化ネオジムを溶解させた。放冷し、約2%のリンゴ酸ネオジムを含有する紫色の水溶液を得た(比較例40)。
アレルゲン低減化組成物によるダニアレルゲンの低減化効果の測定
ダニアレルゲンDer f2を含有する、タンパク質量として約900ng/1mL{リン酸緩衝液(pH7.2)}のアレルゲン液に対し、実施例1〜24、比較例1〜46を、それぞれ25μLを反応させた。これら試料について Der f2酵素免疫測定法(ELISA)のサンドイッチ法にてダニアレルゲン低減化効果の測定を行った。まず、リン酸緩衝液(pH7.4)で2μg/mLに希釈した抗Der f2 モノクローナル抗体15E11を、F16 MAXISORP NUNC−IMMUNO MODULEプレート(NUNC社製)の1ウェルあたり100μLずつ添加し、4℃にて3日以上感作させた。感作後、液を捨て、ブロッキング試薬{1重量%牛血清アルブミン+リン酸緩衝液(pH7.2)}を1ウェルあたり200μLずつ添加し、37℃、60分間反応させた。反応後、リン酸緩衝液(pH7.2)にてプレートを洗浄した。
アレルゲン低減化組成物によるスギ花粉アレルゲンの低減化効果の測定
スギ花粉アレルゲンCry j1として約12.5ng/1mL{リン酸緩衝液(pH7.2)}のアレルゲン液に対し、実施例1、7、8、10、11、12、14、15、16、18、19、24、比較例1、7、8、10、11、12、22、23、43、44、45、46を、それぞれ25μLを反応させた。これら試料についてCry j1酵素免疫測定法(ELISA)のサンドイッチ法にてスギ花粉アレルゲン低減化効果の測定を行った。まず、リン酸緩衝液(pH7.4、0.1重量%NaN3含有)で2μg/mLに希釈したCry j1 モノクローナル抗体013を、F16 MAXISORP NUNC−IMMUNO MODULEプレート(NUNC社製)の1ウェルあたり100μLずつ添加し、4℃にて1日以上感作させた。感作後、液を捨て、ブロッキング試薬{1重量%牛血清アルブミン+リン酸緩衝液(pH7.2、0.1重量%NaN3含有)}を1ウェルあたり200μLずつ添加し、37℃、60分間反応させた。反応後、リン酸緩衝液{pH7.2、0.1重量%ポリオキシエチレン(20)ソルビタンモノラウレート含有}にてプレートを洗浄した。
2%グルコン酸亜鉛水溶液(比較例10)と2%塩化ランタン七水和物水溶液(比較例1)を、表14に示すように1:9、3:7、7:3、9:1の比率で混合し、それぞれ実施例25〜28とした。なお、5:5の比率で混合したもの(実施例1)も表記した。これらの実施例について、試験例1と同様の方法でダニアレルゲンDer f2の低減化効果を測定した。結果を表14に示した。
2%グルコン酸亜鉛水溶液(比較例10)と2%塩化イッテルビウム六水和物水溶液(比較例8)を、表15に示すように1:9、3:7、7:3、9:1の比率で混合し、それぞれ実施例29〜32とした。なお、5:5の比率で混合したもの(実施例8)も表記した。これらの実施例について、試験例1と同様の方法でダニアレルゲンDer f2の低減化効果を測定した。結果を表15に示した。
[実施例33]
グルコン酸亜鉛4g、塩化ランタン七水和物4g、プロピレングリコール3.5gをイオン交換水に溶解し、総量を100gとした。
グルコン酸亜鉛8g、プロピレングリコール3.5gをイオン交換水に溶解し、総量を100gとした。
塩化ランタン七水和物8g、プロピレングリコール3.5gをイオン交換水に溶解し、総量を100gとした。
塩ビ壁紙表面層として、平均重合度700の塩ビ粉末(PQB83、新第一塩ビ株式会社製)100g、可塑剤ジイソノニルフタレート(DINP、田岡化学工業株式会社製)50g、安定剤としてアデカスタブ(登録商標)FL100(株式会社ADEKA製)3g、イソパラフィン(IPソルベント2028、出光興産株式会社製)7gを攪拌機を用いて混合した。基材層としてA4サイズのPPC用紙に、調製した表面層液を約200g/m2となるように塗布し、150℃にて1分間加熱し、塩ビ壁紙を得た。
表面加工剤としてウレタン系樹脂エマルジョン(スーパーフレックス500M(登録商標)、第一工業製薬株式会社製)を用い、これに実施例33、比較例47、比較例48をそれぞれ12%添加し、均一に混合した。この表面加工剤を、上記塩ビシートに10g/m2となるように塗布し、室温にて乾燥させてアレルゲン低減化壁紙を得た。
グルコン酸亜鉛0.8g、塩化ランタン七水和物0.4g、ポリエチレングリコール(分子量20000)0.8gをイオン交換水にて溶解し、総量を100gとして噴霧剤とした。
グルコン酸亜鉛1.6g、ポリエチレングリコール(分子量20000)0.8gをイオン交換水にて溶解し、総量を100gとして噴霧剤とした。
塩化ランタン七水和物0.8、ポリエチレングリコール(分子量20000)0.8gをイオン交換水にて溶解し、総量を100gとして噴霧剤とした。
噴霧剤によるアレルゲン低減化効果の測定
実施例34、比較例49、比較例50をそれぞれトリガー式噴霧容器に入れ、社内事務所の床カーペット0.5m2に約20gを噴霧した。4時間経過後、電気掃除機(日立製作所PV−H23:吸い込み仕事率240W)の吸引ホースに微細塵捕集装置「ごみ取り袋」(住化エンバイロメンタルサイエンス株式会社製)を取り付け、実施例34または比較例49、50を噴霧した部分と、噴霧していない部分(対照)それぞれ0.5m2の面積から1分間、ごみを吸引、採取した。ごみを採取したごみ取り袋をチャック付きビニル袋に入れ、リン酸緩衝5mLにてダニアレルゲンを抽出した。抽出液をダニアレルゲン量を測定試料として、Der f2酵素免疫測定法(ELISA)のサンドイッチ法にて[試験例1]と同様の方法を用いてダニアレルゲン量の測定を行った。結果を表17に示した。
加工不織布に対するアレルゲン低減化効果の測定
実施例27、比較例1、10をそれぞれイオン交換水で所定濃度に希釈した液50gに、80g/m2のポリプロピレン製不織布(20cm×15cm)を1分間浸漬し、しぼり率約200%で処理後、100℃で15分間乾燥させた。加工量は有効成分量として約0.15g/m2となるように希釈率を調製した。これらのアレルゲン低減化不織布の試料を5cm×5cmに切り取り、チャックつきポリ袋内に入れてさらにダニアレルゲン水溶液(Der f2含有、タンパク質濃度として900ng/mL)またはスギ花粉アレルゲン水溶液(Cry j1濃度12.5ng/mL)1mLを添加した。1時間、室温にて保管し、アレルゲン水溶液を、ピペットマンを用いて100μL回収し、[試験例1]または[試験例2]と同様の方法を用いてダニアレルゲン量またはスギ花粉アレルゲン量の測定を行った。結果を表18および表19に示した。
鉄による着色性試験
実施例1、14、18、比較例45を、それぞれ10mL容量のガラス製サンプル瓶に2mL採り、さらに鉄釘(長さ38mm)1本を入れた。経時的に外観を観察した。結果を表20に示す。タンニン酸を含有する比較例45は、鉄釘と接触直後から紫色に着色したが、実施例1、14、18の外観に着色は認められなかった。
Claims (16)
- (A)亜鉛塩および銅塩からなる群から選択される一種類以上の化合物と、
(B)希土類塩から選択される一種類以上の化合物を含有し、
亜鉛塩がヒドロキシ酸亜鉛であり、
銅塩がヒドロキシ酸銅である、アレルゲン低減化組成物。 - ヒドロキシ酸亜鉛がグルコン酸亜鉛である、請求項1に記載のアレルゲン低減化組成物。
- ヒドロキシ酸銅がグルコン酸銅である、請求項1または請求項2に記載のアレルゲン低減化組成物。
- 希土類塩は、ランタン塩、セリウム塩、ガドリニウム塩、エルビウム塩、および、イッテルビウム塩からなる群から選ばれる一種類以上の化合物である、請求項1から請求項3までのいずれか1項に記載のアレルゲン低減化組成物。
- 希土類塩は、ランタン塩またはセリウム塩である、請求項1から請求項3までのいずれか1項に記載のアレルゲン低減化組成物。
- (A)亜鉛塩および銅塩からなる群から選択される一種類以上の化合物と、(B)希土類塩から選択される一種類以上の化合物との混合比率は、重量比で1:9〜9:1である、請求項1から請求項5までのいずれか1項に記載のアレルゲン低減化組成物。
- (A)亜鉛塩および銅塩からなる群から選択される一種類以上の化合物と、(B)希土類塩から選択される一種類以上の化合物とを合計0.5〜70重量%含有する、請求項1から請求項6までのいずれか1項に記載のアレルゲン低減化組成物。
- 請求項1から請求項7までのいずれか1項に記載のアレルゲン低減化組成物と、水または水溶性溶剤を含有する噴霧剤。
- 請求項1から請求項7までのいずれか1項に記載のアレルゲン低減化組成物と、水または水溶性溶剤を含有する表面加工剤。
- 請求項1から請求項7までのいずれか1項に記載のアレルゲン低減化組成物をアレルゲンが存在する環境中に処理する、アレルゲン低減化方法。
- 請求項1から請求項7までのいずれか1項に記載のアレルゲン低減化組成物をアレルゲン低減化対象空間内に存在させる、アレルゲン低減化方法。
- 請求項8に記載の噴霧剤をアレルゲン低減化対象空間内に噴霧する、アレルゲン低減化方法。
- 請求項1から請求項7までのいずれか1項に記載のアレルゲン低減化組成物をアレルゲン低減化対象物の表面に存在させる、アレルゲン低減化方法。
- 請求項9に記載の表面加工剤をアレルゲン低減化対象物の表面に存在させる、アレルゲン低減化方法。
- 請求項1から請求項7までのいずれか1項に記載のアレルゲン低減化組成物を加工した繊維構造体。
- 請求項1から請求項7までのいずれか1項に記載のアレルゲン低減化組成物を加工した建築用内装材。
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