JP6715662B2 - 捺染布帛およびその製造方法 - Google Patents
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Landscapes
- Coloring (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Description
例えば、本発明は、以下の(1)〜(7)である。
ISO 20471:2013の5.1に準じて、分光測色計(CM−2500C(コニカミノルタ株式会社製))を用いて、Yxy表色系のY,x,yの測定を行い、判定した。また、輝度率βは、β=Y/100で求めた。なお、捺染布帛の色材を含むバインダー樹脂を付与した面を測定面とした。
JIS L1096 引裂強さ D法 ペンジュラム法に準じて試験を行い、捺染布帛のタテ方向及び/又はヨコ方向の引裂強さを測定した。
風合いは、得られた捺染布帛を手でさわって判断を行った。
難燃性は、ISO 15025:2000 A法(表面接炎)に準じて試験を行い、ISO 11612 cord letter A1にて合否を判定した。捺染布帛の色材を含むバインダー樹脂を付与した面を接炎面とした。
モダクリル繊維(商品名:プロテックスM 株式会社カネカ製)54質量%、綿35質量%、アラミド繊維(商品名:ケブラー デュポン社製)10質量%、導電糸1質量%の複合糸をタテ糸及びヨコ糸に用いた平織物(目付:225g/m2、密度:タテ×ヨコ=68本/2.54cm×58本/2.54cm)を、染料として、Kayacryl Brill. Yellow Flavine 10G−ED(日本化薬(株)製、カチオン染料)、Aizen Cathilon Pink BL−DP80(保土谷化学工業(株)製、カチオン染料)、MIKA ホワイト ATN(日本化薬(株)製、蛍光増白剤)およびハッコール BRK(昭和化学工業(株)、蛍光増白剤)を用いて、100℃で30分間染色し、湯洗および水洗し、120℃×30秒乾燥後、140℃×1分間熱セットすることで、オレンジ色に着色された繊維布帛を得た。
柔軟剤(アミノ変性シリコーンオイルのエマルジョン 固形分16質量%) 2質量%
水 98質量%
MASTUMIN グローカラー Orange MRS 16質量%
(顔料、蛍光を有する橙色の顔料、(株)松井色素製)
RYUDYE−W Orange RS−E 0.5質量%
(顔料、蛍光を有さない橙色の顔料、DIC(株)製)
紫外線吸収剤(ベンゾトリアゾール系) 2質量%
アクリル樹脂 15質量%
架橋剤(イソシアネート系架橋剤) 2質量%
増粘剤 1.5質量%
水 35質量%
繊維布帛に柔軟剤を含む処理液を付与しなかった以外は、実施例1と同様にし、蛍光オレンジレッドに着色された捺染布帛を得た。得られた捺染布帛の性能を表1に記載した。
色材を含むバインダー樹脂を繊維布帛に付与する前に繊維布帛に対して柔軟剤を含む処理液での処理は行わずに、色材を含むバインダー樹脂を繊維布帛に付着させた後、実施例1で用いた柔軟剤を含む処理液で繊維布帛を処理した以外は、実施例1と同様にし、蛍光オレンジレッドに着色された捺染布帛を得た。得られた捺染布帛の性能を表1に記載した。
実施例1で用いた色材を含むバインダー樹脂液に、柔軟剤としてその配合量が5質量%となるように、シリコーンオイル(ジメチルシリコーン)、脂肪酸エステル化合物、および非イオン系界面活性剤を15質量%含むエマルジョンを追加配合した以外は、実施例1と同様にして蛍光オレンジレッドに着色された捺染布帛を得た。得られた捺染布帛の性能を表1に記載した。
繊維布帛に柔軟剤を含む処理液の付与を行わなかった以外は、実施例2と同様にし、蛍光オレンジレッドに着色された捺染布帛を得た。得られた捺染布帛の性能を表1に記載した。
柔軟剤を含む処理液に用いた柔軟剤を、実施例2の色材を含むバインダー樹脂液に用いた柔軟剤に変更した以外は実施例2と同様にして捺染布帛を得た。得られた捺染布帛の性能を表1に記載した。
実施例1で用いた柔軟剤に替え、メチルハイドロジエンポリシロキサンを50質量%含むエマルジョンを1質量%用いた以外は、実施例1と同様にし、蛍光オレンジレッドに着色された捺染布帛を得た。得られた捺染布帛の性能を表1に記載した。
Claims (7)
- ISO 20471:2013の5.1 色に対する要求事項を満たす捺染布帛であって、繊維布帛の少なくとも片面の表面を構成する繊維の表面に柔軟剤が付着しており、前記柔軟剤の上に色材を含むバインダー樹脂が付着していることを特徴とする捺染布帛。
- 前記柔軟剤は、シリコーン樹脂を含むことを特徴とする請求項1に記載の捺染布帛。
- 前記捺染布帛は、JIS L1096 引裂強さ D法 ペンジュラム法でのタテ方向及び/又はヨコ方向の引裂強さが10N以上であることを特徴とする請求項1または2に記載の捺染布帛。
- 前記繊維布帛は、モダクリル繊維を含むことを特徴とする請求項1〜3のいずれか1項に記載の捺染布帛。
- 前記捺染布帛は、難燃性を有することを特徴とする請求項1〜4のいずれか1項に記載の捺染布帛。
- 請求項1〜5のいずれか一項に記載の捺染布帛の製造方法であって、繊維布帛の少なくとも片面に柔軟剤を含む処理液を付与する工程と、前記片面に色材を含むバインダー樹脂液を付与する工程とを有することを特徴とする捺染布帛の製造方法。
- 前記柔軟剤は、シリコーン樹脂を含むことを特徴とする請求項6に記載の捺染布帛の製造方法。
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