JP6491244B2 - 耐uv性超疎水性コーティング組成物 - Google Patents
耐uv性超疎水性コーティング組成物 Download PDFInfo
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- JP6491244B2 JP6491244B2 JP2016575029A JP2016575029A JP6491244B2 JP 6491244 B2 JP6491244 B2 JP 6491244B2 JP 2016575029 A JP2016575029 A JP 2016575029A JP 2016575029 A JP2016575029 A JP 2016575029A JP 6491244 B2 JP6491244 B2 JP 6491244B2
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- silicon dioxide
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- 239000008199 coating composition Substances 0.000 title claims description 137
- 230000003075 superhydrophobic effect Effects 0.000 title description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 120
- 239000004020 conductor Substances 0.000 claims description 102
- 239000004593 Epoxy Substances 0.000 claims description 78
- 239000002952 polymeric resin Substances 0.000 claims description 66
- 229920003002 synthetic resin Polymers 0.000 claims description 66
- 239000000203 mixture Substances 0.000 claims description 57
- 239000000377 silicon dioxide Substances 0.000 claims description 48
- 239000000758 substrate Substances 0.000 claims description 42
- 239000002491 polymer binding agent Substances 0.000 claims description 40
- 229920005596 polymer binder Polymers 0.000 claims description 39
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- 229910052782 aluminium Inorganic materials 0.000 claims description 27
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 27
- 238000000034 method Methods 0.000 claims description 19
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 17
- 239000011230 binding agent Substances 0.000 claims description 17
- 235000012239 silicon dioxide Nutrition 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims description 15
- 229910052982 molybdenum disulfide Inorganic materials 0.000 claims description 15
- 125000000524 functional group Chemical group 0.000 claims description 14
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- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 claims description 8
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- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 7
- 150000001875 compounds Chemical class 0.000 claims description 6
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 6
- LIKFHECYJZWXFJ-UHFFFAOYSA-N dimethyldichlorosilane Chemical compound C[Si](C)(Cl)Cl LIKFHECYJZWXFJ-UHFFFAOYSA-N 0.000 claims description 6
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- 229910000838 Al alloy Inorganic materials 0.000 claims description 4
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- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 4
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- YGZSVWMBUCGDCV-UHFFFAOYSA-N chloro(methyl)silane Chemical compound C[SiH2]Cl YGZSVWMBUCGDCV-UHFFFAOYSA-N 0.000 claims description 3
- 239000010949 copper Substances 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
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- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 3
- FPLYNRPOIZEADP-UHFFFAOYSA-N octylsilane Chemical compound CCCCCCCC[SiH3] FPLYNRPOIZEADP-UHFFFAOYSA-N 0.000 claims description 3
- ZPQAUEDTKNBRNG-UHFFFAOYSA-N 2-methylprop-2-enoylsilicon Chemical compound CC(=C)C([Si])=O ZPQAUEDTKNBRNG-UHFFFAOYSA-N 0.000 claims description 2
- AFUWHLXUBJOPNO-UHFFFAOYSA-N CCCCCCCCCCCCCCCC[SiH3] Chemical compound CCCCCCCCCCCCCCCC[SiH3] AFUWHLXUBJOPNO-UHFFFAOYSA-N 0.000 claims description 2
- 125000003545 alkoxy group Chemical group 0.000 claims description 2
- 125000005370 alkoxysilyl group Chemical group 0.000 claims description 2
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- 230000009477 glass transition Effects 0.000 claims description 2
- 125000001181 organosilyl group Chemical group [SiH3]* 0.000 claims description 2
- 125000004469 siloxy group Chemical group [SiH3]O* 0.000 claims description 2
- 239000004408 titanium dioxide Substances 0.000 claims 3
- WSPOQKCOERDWJQ-UHFFFAOYSA-N 2-methyl-1,3,5,7,2,4,6,8-tetraoxatetrasilocane Chemical compound C[SiH]1O[SiH2]O[SiH2]O[SiH2]O1 WSPOQKCOERDWJQ-UHFFFAOYSA-N 0.000 claims 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 claims 1
- 238000000576 coating method Methods 0.000 description 31
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- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 15
- 229910002012 Aerosil® Inorganic materials 0.000 description 13
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 description 10
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
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- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
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- HMMGMWAXVFQUOA-UHFFFAOYSA-N octamethylcyclotetrasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 HMMGMWAXVFQUOA-UHFFFAOYSA-N 0.000 description 2
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- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- VPWNQTHUCYMVMZ-UHFFFAOYSA-N 4,4'-sulfonyldiphenol Chemical compound C1=CC(O)=CC=C1S(=O)(=O)C1=CC=C(O)C=C1 VPWNQTHUCYMVMZ-UHFFFAOYSA-N 0.000 description 1
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 1
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- 102100030322 Ephrin type-A receptor 1 Human genes 0.000 description 1
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 1
- 101000938354 Homo sapiens Ephrin type-A receptor 1 Proteins 0.000 description 1
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- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 1
- 239000004841 bisphenol A epoxy resin Substances 0.000 description 1
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- 150000004985 diamines Chemical class 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical compound C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 1
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- SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 description 1
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- AFEQENGXSMURHA-UHFFFAOYSA-N oxiran-2-ylmethanamine Chemical compound NCC1CO1 AFEQENGXSMURHA-UHFFFAOYSA-N 0.000 description 1
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
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- C09D127/20—Homopolymers or copolymers of hexafluoropropene
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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- C08K3/36—Silica
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- C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
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- C09D127/12—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
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- C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
- C09D127/02—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
- C09D127/12—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
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- H01B3/44—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes vinyl resins; acrylic resins
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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Description
本出願は、2014年6月23日出願の米国仮特許出願第62/015771号、名称「耐UV性超疎水性コーティング組成物(UV‐Resistant Superhydrophobic Coating Compositions)」に対する優先権を主張するものであり、上記仮特許出願の開示全体は、参照により本出願に援用される。
Claims (24)
- 基材用のコーティング組成物であって、
フルオロポリマー又はエポキシポリマー樹脂を含むポリマーバインダ;
1つ又は複数の疎水性二酸化ケイ素組成物であって、二酸化ケイ素よりも高い疎水性を有する化合物を規定するように疎水性ポリマー官能基を結合させた二酸化ケイ素を含む前記疎水性二酸化ケイ素組成物;
二硫化モリブデン;並びに
酸化亜鉛及び二酸化チタンから選ばれる少なくとも一つのUV保護剤
を含む、前記コーティング組成物。 - 前記ポリマーバインダは、75℃〜350℃のガラス転移温度又は融点を有する、請求項1に記載のコーティング組成物。
- 前記バインダは、ポリテトラフルオロエチレン(PTFE)、ポリビニリデンジフルオリド(PVDF)及びポリヘキサフルオロプロピレン(PHFP)からなる群から選択される少なくとも1つのフルオロポリマーを含む、請求項1に記載のコーティング組成物。
- 前記バインダは、20℃〜27℃の温度及び硬化の開始前において、1センチポアズ〜25000センチポアズの粘度を有する少なくとも1つのエポキシポリマー樹脂を含む、請求項1に記載のコーティング組成物。
- 前記コーティング組成物は、少なくとも50重量%の前記ポリマーバインダ、0.5重量%〜15重量%の前記1つ又は複数の疎水性二酸化ケイ素組成物、0.1重量%〜15重量%の二硫化モリブデン、及び0.1重量%〜10重量%の前記1つ又は複数のUV保護剤を含む、請求項1に記載のコーティング組成物。
- 前記UV保護剤のうちの少なくとも1つは酸化亜鉛を含む、請求項1に記載のコーティング組成物。
- 前記1つ又は複数の疎水性二酸化ケイ素組成物は、アルキル、アルコキシ、シリル、アルコキシシリル及びシロキシからなる群から選択される少なくとも1つの官能基を含む、請求項1に記載のコーティング組成物。
- 前記1つ又は複数の疎水性二酸化ケイ素組成物は、メチルクロロシラン、ヘキサメチルジシラザン(HMDS)、ポリジメチルシロキサン(PDMS)、オクチルシラン、ヘキサデシルシラン、メタクリルシラン、ジメチルジクロロシラン(DDS)及びオクタメチルシクロテトラシロキサンからなる群から選択される少なくとも1つの官能基を含む、請求項1に記載のコーティング組成物。
- 請求項1に記載のコーティング組成物でコーティングされたコンダクタケーブル。
- 前記コンダクタケーブルは裸線架空コンダクタケーブルである、請求項9に記載のコンダクタケーブル。
- 前記コンダクタケーブルは、アルミニウム、鋼鉄、又は炭素繊維ポリマー複合材料を含む、請求項9に記載のコンダクタケーブル。
- 前記コンダクタケーブルの外側表面が、厚さ0.00001インチ〜0.030インチの前記コーティング組成物でコーティングされる、請求項9に記載のコンダクタケーブル。
- 前記コンダクタケーブルは接地裸線ワイヤである、請求項9に記載のコンダクタケーブル。
- 前記コンダクタは、銅、アルミニウム又はアルミニウム合金を含む剛性コンダクタ材料を含む、請求項9に記載のコンダクタ。
- 複数の素線ワイヤを含むコンダクタケーブルであって、少なくとも1つの前記素線ワイヤは、請求項1に記載のコーティング組成物でコーティングされる、前記コンダクタケーブル。
- 基材用のコーティング組成物であって、
バインダであって:
1つ若しくは複数のフルオロポリマー;又は
1つ若しくは複数のエポキシポリマー樹脂
を含む前記バインダ;
1つ又は複数の疎水性二酸化ケイ素組成物であって、二酸化ケイ素よりも高い疎水性を有する化合物を規定するように疎水性ポリマー官能基を結合させた二酸化ケイ素を含む前記疎水性二酸化ケイ素組成物;
二硫化モリブデン;及び
酸化亜鉛及び二酸化チタンから選ばれる少なくとも一つのUV保護剤
を含み、
前記コーティング組成物が少なくとも150時間の期間にわたって少なくとも1W/m2のUV照射で曝露された後の前記コーティング組成物上に形成された水滴の接触角が、少なくとも140°である、前記コーティング組成物。 - 前記コーティング組成物が少なくとも470時間の期間にわたって少なくとも1W/m2のUV照射で曝露された後の前記コーティング組成物上に形成された水滴の前記接触角が、少なくとも140°である、請求項16に記載のコーティング組成物。
- 基材表面にコーティング組成物を提供する方法であって、
ポリマーバインダ、
1つ又は複数の疎水性二酸化ケイ素組成物であって、二酸化ケイ素よりも高い疎水性を有する化合物を規定するように疎水性ポリマー官能基を結合させた二酸化ケイ素を含む前記疎水性二酸化ケイ素組成物、
二硫化モリブデン、並びに
酸化亜鉛及び二酸化チタンから選ばれる少なくとも一つのUV保護剤
の混合物を前記基材表面に塗布して、前記基板表面上に前記コーティング組成物を形成するステップを含み、
前記ポリマーバインダは、フルオロポリマー又はエポキシポリマー樹脂を含む、前記方法。 - 前記基材表面は、裸線架空コンダクタケーブルの外側表面の一部分を含む、請求項18に記載の方法。
- 前記混合物は、液体キャリア中で形成され、
前記混合物を前記基材表面に塗布する前記ステップは、さらに:
前記混合物を含む前記液体キャリアを前記基材表面に塗布するステップ
を含む、請求項19に記載の方法。 - 前記基材表面を乾燥させて、前記液体キャリアを除去することにより、前記基材表面に付着した前記混合物を含む前記コーティング組成物を形成するステップをさらに含む、請求項19に記載の方法。
- 前記ポリマーバインダは、1つ又は複数のエポキシポリマー樹脂を含み、さらに:
前記基材表面に塗布した前記液体キャリア中の前記1つ又は複数のエポキシポリマー樹脂を硬化させるステップ
を含む、請求項21に記載の方法。 - 前記混合物を前記基材表面に塗布するステップは、さらに:
前記混合物を乾燥粉体として前記基材表面に塗布するステップ;及び
前記基材表面を加熱して、前記基材表面に付着した前記混合物を含む前記コーティング組成物を形成するステップ
を含む、請求項18に記載の方法。 - 前記混合物を前記基材表面に塗布するステップは、前記混合物の塗布前に前記基材表面に対していずれの摩擦を実施することなく行われる、請求項18に記載の方法。
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PCT/US2015/036840 WO2015200146A1 (en) | 2014-06-23 | 2015-06-20 | Uv-resistant superhydrophobic coating compositions |
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CN106574173A (zh) | 2017-04-19 |
KR102133544B1 (ko) | 2020-07-13 |
CA2953510A1 (en) | 2015-12-30 |
CN106574173B (zh) | 2019-11-01 |
KR20170016946A (ko) | 2017-02-14 |
US20190338102A1 (en) | 2019-11-07 |
US20150368496A1 (en) | 2015-12-24 |
EP3158022A1 (en) | 2017-04-26 |
KR20190097311A (ko) | 2019-08-20 |
EP3158022A4 (en) | 2018-06-20 |
US10370514B2 (en) | 2019-08-06 |
US11001696B2 (en) | 2021-05-11 |
JP2017529409A (ja) | 2017-10-05 |
CA2953510C (en) | 2019-12-03 |
WO2015200146A1 (en) | 2015-12-30 |
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