JP6309012B2 - 偏光板およびこれを含む画像表示装置 - Google Patents
偏光板およびこれを含む画像表示装置 Download PDFInfo
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- JP6309012B2 JP6309012B2 JP2015534411A JP2015534411A JP6309012B2 JP 6309012 B2 JP6309012 B2 JP 6309012B2 JP 2015534411 A JP2015534411 A JP 2015534411A JP 2015534411 A JP2015534411 A JP 2015534411A JP 6309012 B2 JP6309012 B2 JP 6309012B2
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- polarizing plate
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- epoxy compound
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- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 150000002497 iodine compounds Chemical class 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- FOVRCVYQPBQVTL-UHFFFAOYSA-N isocyanatomethyl prop-2-enoate Chemical compound C=CC(=O)OCN=C=O FOVRCVYQPBQVTL-UHFFFAOYSA-N 0.000 description 1
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 238000003475 lamination Methods 0.000 description 1
- 150000007517 lewis acids Chemical class 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 230000028161 membrane depolarization Effects 0.000 description 1
- 125000004184 methoxymethyl group Chemical group [H]C([H])([H])OC([H])([H])* 0.000 description 1
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 1
- 125000002816 methylsulfanyl group Chemical group [H]C([H])([H])S[*] 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- SEEYREPSKCQBBF-UHFFFAOYSA-N n-methylmaleimide Chemical compound CN1C(=O)C=CC1=O SEEYREPSKCQBBF-UHFFFAOYSA-N 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 229920003986 novolac Polymers 0.000 description 1
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- LLEMOWNGBBNAJR-UHFFFAOYSA-N ortho-phenyl-phenol Natural products OC1=CC=CC=C1C1=CC=CC=C1 LLEMOWNGBBNAJR-UHFFFAOYSA-N 0.000 description 1
- 235000010292 orthophenyl phenol Nutrition 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- AHHWIHXENZJRFG-UHFFFAOYSA-N oxetane Chemical compound C1COC1 AHHWIHXENZJRFG-UHFFFAOYSA-N 0.000 description 1
- RPQRDASANLAFCM-UHFFFAOYSA-N oxiran-2-ylmethyl prop-2-enoate Chemical compound C=CC(=O)OCC1CO1 RPQRDASANLAFCM-UHFFFAOYSA-N 0.000 description 1
- UWJJYHHHVWZFEP-UHFFFAOYSA-N pentane-1,1-diol Chemical compound CCCCC(O)O UWJJYHHHVWZFEP-UHFFFAOYSA-N 0.000 description 1
- GTCCGKPBSJZVRZ-UHFFFAOYSA-N pentane-2,4-diol Chemical compound CC(O)CC(C)O GTCCGKPBSJZVRZ-UHFFFAOYSA-N 0.000 description 1
- 239000010702 perfluoropolyether Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 239000003504 photosensitizing agent Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229920001610 polycaprolactone Polymers 0.000 description 1
- 239000004632 polycaprolactone Substances 0.000 description 1
- 150000004291 polyenes Chemical class 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920005906 polyester polyol Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000307 polymer substrate Polymers 0.000 description 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- 229920005749 polyurethane resin Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000007870 radical polymerization initiator Substances 0.000 description 1
- 238000010526 radical polymerization reaction Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N tetraethylene glycol Chemical compound OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- TXEYQDLBPFQVAA-UHFFFAOYSA-N tetrafluoromethane Chemical compound FC(F)(F)F TXEYQDLBPFQVAA-UHFFFAOYSA-N 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- YRHRIQCWCFGUEQ-UHFFFAOYSA-N thioxanthen-9-one Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3SC2=C1 YRHRIQCWCFGUEQ-UHFFFAOYSA-N 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- DQZNLOXENNXVAD-UHFFFAOYSA-N trimethoxy-[2-(7-oxabicyclo[4.1.0]heptan-4-yl)ethyl]silane Chemical compound C1C(CC[Si](OC)(OC)OC)CCC2OC21 DQZNLOXENNXVAD-UHFFFAOYSA-N 0.000 description 1
- BPSIOYPQMFLKFR-UHFFFAOYSA-N trimethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CO[Si](OC)(OC)CCCOCC1CO1 BPSIOYPQMFLKFR-UHFFFAOYSA-N 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 239000013585 weight reducing agent Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- INRGAWUQFOBNKL-UHFFFAOYSA-N {4-[(Vinyloxy)methyl]cyclohexyl}methanol Chemical compound OCC1CCC(COC=C)CC1 INRGAWUQFOBNKL-UHFFFAOYSA-N 0.000 description 1
Classifications
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- G02B5/00—Optical elements other than lenses
- G02B5/30—Polarising elements
- G02B5/3025—Polarisers, i.e. arrangements capable of producing a definite output polarisation state from an unpolarised input state
- G02B5/3033—Polarisers, i.e. arrangements capable of producing a definite output polarisation state from an unpolarised input state in the form of a thin sheet or foil, e.g. Polaroid
- G02B5/3041—Polarisers, i.e. arrangements capable of producing a definite output polarisation state from an unpolarised input state in the form of a thin sheet or foil, e.g. Polaroid comprising multiple thin layers, e.g. multilayer stacks
- G02B5/305—Polarisers, i.e. arrangements capable of producing a definite output polarisation state from an unpolarised input state in the form of a thin sheet or foil, e.g. Polaroid comprising multiple thin layers, e.g. multilayer stacks including organic materials, e.g. polymeric layers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
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- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
- G02F1/133—Constructional arrangements; Operation of liquid crystal cells; Circuit arrangements
- G02F1/1333—Constructional arrangements; Manufacturing methods
- G02F1/1335—Structural association of cells with optical devices, e.g. polarisers or reflectors
- G02F1/133528—Polarisers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2457/00—Electrical equipment
- B32B2457/20—Displays, e.g. liquid crystal displays, plasma displays
- B32B2457/202—LCD, i.e. liquid crystal displays
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2457/00—Electrical equipment
- B32B2457/20—Displays, e.g. liquid crystal displays, plasma displays
- B32B2457/206—Organic displays, e.g. OLED
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/22—Di-epoxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/22—Di-epoxy compounds
- C08G59/226—Mixtures of di-epoxy compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
- C09J163/10—Epoxy resins modified by unsaturated compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2323/00—Functional layers of liquid crystal optical display excluding electroactive liquid crystal layer characterised by chemical composition
- C09K2323/05—Bonding or intermediate layer characterised by chemical composition, e.g. sealant or spacer
- C09K2323/055—Epoxy
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F2202/00—Materials and properties
- G02F2202/28—Adhesive materials or arrangements
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31511—Of epoxy ether
- Y10T428/31515—As intermediate layer
Landscapes
- Physics & Mathematics (AREA)
- Nonlinear Science (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Chemical & Material Sciences (AREA)
- Mathematical Physics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Chemistry (AREA)
- Polarising Elements (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Electroluminescent Light Sources (AREA)
- Coating Of Shaped Articles Made Of Macromolecular Substances (AREA)
- Laminated Bodies (AREA)
- Paints Or Removers (AREA)
Description
本発明で使用可能な偏光子は特に制限されるものではなく、当該技術分野で一般的に使用される偏光子、例えば、ポリビニルアルコール系フィルム、部分ホルマール化ポリビニルアルコール系フィルム、エチレン・酢酸ビニル共重合体の部分ケン化フィルムなどの親水性高分子フィルムに、ヨウ素や二色性染料などの偏光物質を吸着させ、延伸して一定方向に配向したフィルム、ポリビニルアルコールの脱水処理物やポリ塩化ビニルの脱塩酸処理物などのポリエン系配向フィルムなどであってよく、好ましくは、ヨウ素系化合物または二色性偏光物質を含む分子鎖が一定方向に配向されたポリビニルアルコール系偏光子であってよい。
本発明において、前記偏光子の少なくとも一面には、接着剤層およびプライマー層を介してポリエチレンテレフタレートフィルムが付着する。ポリエチレンテレフタレートフィルムは、透湿度水蒸気透過速度および含湿率含水率が低いため、偏光子保護フィルムとして使用される場合、偏光板の耐水性を向上させるだけでなく、熱および水分に対する抵抗性が高く、高温高湿下においても偏光板の光学物性を優れたものに維持することができる。また、ポリエチレンテレフタレートフィルムは、他の透明高分子フィルムに比べて生産価格が安価であるため、これを使用する場合、偏光板の製造コストを低減させることができる利点がある。
一方、本発明において、前記偏光子およびポリエチレンテレフタレートフィルムは、活性エネルギー線硬化型接着剤によって付着する。この時、活性エネルギー線硬化性接着剤は、活性エネルギー線の照射によって硬化される接着剤を意味する。
さらに、前記脂肪族多価カルボン酸としては、例えば、シュウ酸、マロン酸、コハク酸、グルタル酸、アジピン酸、ピメリン酸、スベリン酸、アゼライン酸、セバシン酸、ドデカン二酸、2−メチルコハク酸、2−メチルアジピン酸、3−メチルアジピン酸、3−メチルペンタン二酸、2−メチルオクタン二酸、3,8−ジメチルデカン二酸、3,7−ジメチルデカン二酸、1,20−エイコサメチレンジカルボン酸、1,2−シクロペンタンジカルボン酸、1,3−シクロペンタンジカルボン酸、1,2−シクロヘキサンジカルボン酸、1,3−シクロヘキサンジカルボン酸、1,4−シクロヘキサンジカルボン酸、1,4−ジカルボキシルメチレンシクロヘキサン、1,2,3−プロパントリカルボン酸、1,2,3,4−ブタンテトラカルボン酸、1,2,3,4−シクロブタンテトラカルボン酸などが例示できるが、これらに制限されるものではない。
本発明の偏光板は、接着剤層とポリエチレンテレフタレートフィルムとの間に、接着剤層とポリエチレンテレフタレートフィルムの接着力を向上させるためのプライマー層を含む。
ホモポリマーのガラス転移温度が190℃の3,4−エポキシシクロヘキシルメチル−3,4’−エポキシシクロヘキサンカルボキシレート25重量%(Diel社のCelloxide2021P)、ホモポリマーのガラス転移温度が25℃の1,2−シクロヘキサンジメタノールジグリシジルエーテル25重量%、3−エチル−3−[(3−エチルオキセタン−3−イル)メトキシメチル]オキセタン(東亜合成、アロンオキセタンDOX221)50重量%を入れて製造した樹脂組成物100重量部に、陽イオン開始剤のCPI100P(Sanapro社)5重量部を添加して、偏光板用接着剤組成物Aを製造した。製造された接着剤組成物Aの粘度は35cP、ガラス転移温度は102℃であった。
ポリエチレンテレフタレートフィルムの一面に、ポリエステル樹脂およびエポキシ系架橋剤を含むプライマー組成物(ポリエステル樹脂とエポキシ系架橋剤をブレンディングした樹脂組成物[製造会社:TAKAMATSU社、商品名:A115GE]40重量部、シリカ3重量部、および水57重量部)をコーティングして、プライマー層が形成されたポリエチレンテレフタレートフィルムを製造した。
プライマー層が形成されたポリエチレンテレフタレートフィルムの代わりに、コロナ処理されたトリアセチルセルロースフィルム(製造会社:富士フイルム、商品名:UZ TAC)を使用した点を除いては、実施例1と同様の方法で偏光板を製造した。製造された偏光板は、UZ TACフィルム/接着剤層/偏光子/接着剤層/NRTフィルムの構造からなる偏光板を製造した。
ポリエチレンテレフタレートフィルムの一面に、ポリエステル樹脂およびアクリル系架橋剤を含むプライマー組成物をコーティングして、プライマー層が形成されたポリエチレンテレフタレートフィルムを製造した。
プライマー層が形成されたポリエチレンテレフタレートフィルムの代わりに、コロナ処理されたトリアセチルセルロースフィルム(製造会社:富士フイルム、商品名:UZ TAC)を使用した点を除いては、比較例2と同様の方法で偏光板を製造した。製造された偏光板は、UZ TACフィルム/接着剤層/偏光子/接着剤層/NRTフィルムの構造からなる偏光板を製造した。
プライマー層を形成しないポリエチレンテレフタレートフィルムを使用した点を除いては、実施例1と同様の方法で偏光板を製造した。製造された偏光板は、PETフィルム/接着剤層/偏光子/接着剤層/NRTフィルムの構造であった。
ポリエステル樹脂およびエポキシ系架橋剤を含むプライマー組成物の代わりに、ポリエステル樹脂およびウレタン系架橋剤を添加したプライマー組成物を使用した点を除いては、実施例1と同様の方法で偏光板を製造した。
ポリエステル樹脂およびエポキシ系架橋剤を含むプライマー組成物の代わりに、ポリウレタン樹脂を含むプライマー組成物を使用した点を除いては、実施例1と同様の方法で偏光板を製造した。
前記実施例1および比較例1〜6により製造された偏光板のカール特性を肉眼で観察した。図1〜図7には、実施例1および比較例1〜6の偏光板のカール特性を示す写真が示されている。図1〜図7を通して、実施例1の偏光板は、カールが発生しないのに対し、比較例1〜6により製造された偏光板では、カールが発生したことが分かる。
実施例1により製造された偏光板と、比較例1により製造された偏光板を、60℃の温度の水に24時間浸漬させた後、偏光板の状態を肉眼で観察した。図8は、実施例1および比較例1の偏光板を24時間浸漬させた後の状態を示す写真である。図8を通して、実施例1の偏光板の場合、24時間浸漬後もほとんど変化がないのに対し、比較例1の偏光板は、4時間浸漬後に末端部分に脱色が発生しはじめ、24時間浸漬後に大きな偏光板の脱色が発生したことが分かる。
一面に1,1,1−トリフルオロエタンを混合したアクリル樹脂を塗布して形成された低屈折率層がコーティングされたポリエチレンテレフタレートフィルム上に、ポリエステル樹脂およびエポキシ系架橋剤を含むプライマー組成物(ポリエステル樹脂とエポキシ系架橋剤をブレンディングした樹脂組成物[製造会社:TAKAMATSU社、商品名:A115GE]40重量部、シリカ3重量部および水57重量部)をコーティングして、プライマー層が形成されたポリエチレンテレフタレートフィルムを製造した。
プライマー層が形成されたポリエチレンテレフタレートフィルムの代わりに、コロナ処理されたトリアセチルセルロースフィルム(製造会社:富士フイルム、商品名:NRT)を使用した点を除いては、実施例2と同様の方法で偏光板を製造した。製造された偏光板は、NRTフィルム/接着剤層/偏光子/接着剤層/プライマー層/アクリルフィルムの構造であった。
実施例2および比較例7により製造された偏光板の光学物性および色相(CIE表色系による色相値)を、JASCO−V−7100Spectrophotometerを用いて測定した。測定の結果は下記の表1に開示された通りである。
実施例2および比較例7により製造された偏光板を、80℃のオーブンに100時間入れてから、常温で12時間放置した後、光学物性および色相の変化の程度を測定した。測定の結果は表2に記載した。
Claims (16)
- 偏光子の少なくとも一面に、接着剤層、プライマー層、およびポリエチレンテレフタレートフィルムが当該順に備えられた偏光板であって、
前記接着剤層は、ホモポリマーのガラス転移温度が120℃以上の第1エポキシ化合物、ホモポリマーのガラス転移温度が60℃以下の第2エポキシ化合物、およびカチオン性光重合開始剤を含む活性エネルギー線硬化型接着剤により形成され、
前記プライマー層は、ポリエステルバインダー樹脂と、エポキシ系架橋剤とを含むプライマー組成物により形成され、
前記ポリエチレンテレフタレートフィルムは、少なくとも片面に、屈折率が1.4〜1.5の低屈折率層を有し、
前記低屈折率層を有するポリエチレンテレフタレートフィルムは、全体屈折率が1.48〜1.55であり、
前記ポリエチレンテレフタレートフィルムは、水蒸気透過速度が100g/m2・day以下であり、含水率が1重量%以下であり、
前記活性エネルギー線硬化型接着剤は、ホモポリマーのガラス転移温度が120℃以上の前記第1エポキシ化合物100重量部に対して、前記カチオン性光重合開始剤0.5〜20重量部を含み、
前記第1エポキシ化合物は、脂環式エポキシ化合物および芳香族エポキシ化合物からなる群より選択される1つ以上を含み、
前記第2エポキシ化合物は、脂環式エポキシ化合物および脂肪族エポキシ化合物からなる群より選択された1種以上であり、
前記第2エポキシ化合物は、グリシジルエーテル基を1つ以上含み、
前記活性エネルギー線硬化型接着剤は、前記第1エポキシ化合物と第2エポキシ化合物を1:1〜3:1の重量比で含み、
前記プライマー層表面の水接触角が40〜100度である
偏光板。 - 前記第1エポキシ化合物は、3,4−エポキシシクロヘキシルメチル−3,4’−エポキシシクロヘキサンカルボキシレート、ビニルシクロヘキサンジオキサイドジシクロペンタジエンジオキサイド、ビス(エポキシシクロペンチル)エーテル、ビスフェノールA系エポキシ化合物、およびビスフェノールF系エポキシ化合物からなる群より選択された1種以上である、請求項1に記載の偏光板。
- 前記第2エポキシ化合物は、1,4−シクロヘキサンジメタノールジグリシジルエーテル、1,4−ブタンジオールジグリシジルエーテル、1,6−ヘキサンジオールジグリシジルエーテル、ネオペンチルジグリシジルエーテル、レゾルシノールジグリシジルエーテル、ジエチレングリコールジグリシジルエーテル、エチレングリコールジグリシジルエーテル、トリメチロールプロパントリグリシジルエーテル、n−ブチルグリシジルエーテル、2−エチルヘキシルグリシジルエーテル、フェニルグリシジルエーテル、およびo−クレシル(Cresyl)グリシジルエーテルからなる群から選択された1つ以上を含む、請求項1または2に記載の偏光板。
- 前記活性エネルギー線硬化型接着剤は、分子内に少なくとも1個のオキセタニル基を有するオキセタン化合物100〜400重量部をさらに含む、請求項1〜3のいずれか一項に記載の偏光板。
- 前記活性エネルギー線硬化型接着剤は、ビニル系化合物を更に含み、前記ビニル系化合物の含有量は、接着剤全体の100重量部に対して、0.1〜10重量部である、請求項1〜4のいずれか一項に記載の偏光板。
- 前記ビニル系化合物は、ヒドロキシC1-6アルキルビニルエーテルおよびビニルアセテートからなる群から選択された少なくとも1つを含む、請求項5に記載の偏光板。
- 前記活性エネルギー線硬化型接着剤は、シランカップリング剤を更に含み、前記シランカップリング剤の含有量は、接着剤全体の100重量部に対して、0.1〜5重量部である、請求項1〜6のいずれか一項に記載の偏光板。
- 前記シランカップリング剤は、エポキシ基、ビニル基、およびラジカル基からなる群より選択されるカチオン重合性官能基を含む、請求項7に記載の偏光板。
- 前記活性エネルギー線硬化型接着剤は、ラジカル重合性モノマーを更に含み、前記ラジカル重合性モノマーの含有量は、接着剤全体の100重量部に対して、0超過40重量部以下である、請求項1〜8のいずれか一項に記載の偏光板。
- 前記活性エネルギー線硬化型接着剤は、光ラジカル重合開始剤を更に含み、前記光ラジカル重合開始剤の含有量は、接着剤全体の100重量部に対して、0.5〜20重量部である、請求項9に記載の偏光板。
- 前記活性エネルギー線硬化型接着剤は、硬化後のガラス転移温度が80℃〜120℃である、請求項1〜10のいずれか一項に記載の偏光板。
- 前記活性エネルギー線硬化型接着剤は、25℃での粘度が15cP〜50cPである、請求項1〜11のいずれか一項に記載の偏光板。
- 前記偏光子の片面にポリエチレンテレフタレートフィルムが配置され、
前記偏光子の他面に、トリアセチルセルロースフィルム、シクロオレフィンポリマーフィルム、ポリエステル系フィルム、ポリカーボネートフィルム、およびアクリルフィルムからなる群より選択される透明高分子フィルムが配置される、請求項1〜12のいずれか一項に記載の偏光板。 - 前記偏光子の他面に付着する透明高分子フィルムは、位相差を有する一軸配向フィルムまたは二軸配向フィルムである、請求項13に記載の偏光板。
- 請求項1〜14のいずれか1項に記載の偏光板を含む、画像表示装置。
- 前記画像表示装置は、液晶表示装置(LCD)または有機EL表示装置である、請求項15に記載の画像表示装置。
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