JP6099722B2 - 耐黒変性及び密着力に優れたZn‐Mg合金コーティング鋼板及びその製造方法 - Google Patents
耐黒変性及び密着力に優れたZn‐Mg合金コーティング鋼板及びその製造方法 Download PDFInfo
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- JP6099722B2 JP6099722B2 JP2015214095A JP2015214095A JP6099722B2 JP 6099722 B2 JP6099722 B2 JP 6099722B2 JP 2015214095 A JP2015214095 A JP 2015214095A JP 2015214095 A JP2015214095 A JP 2015214095A JP 6099722 B2 JP6099722 B2 JP 6099722B2
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- 229910009369 Zn Mg Inorganic materials 0.000 title claims description 79
- 229910007573 Zn-Mg Inorganic materials 0.000 title claims description 79
- 229910000831 Steel Inorganic materials 0.000 title claims description 55
- 239000010959 steel Substances 0.000 title claims description 55
- 229910045601 alloy Inorganic materials 0.000 title claims description 25
- 239000000956 alloy Substances 0.000 title claims description 25
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 239000011247 coating layer Substances 0.000 claims description 47
- 238000000034 method Methods 0.000 claims description 30
- 238000005229 chemical vapour deposition Methods 0.000 claims description 29
- 238000000576 coating method Methods 0.000 claims description 25
- 239000011248 coating agent Substances 0.000 claims description 24
- 229910000765 intermetallic Inorganic materials 0.000 claims description 23
- 239000010410 layer Substances 0.000 claims description 20
- 238000005240 physical vapour deposition Methods 0.000 claims description 15
- 230000008569 process Effects 0.000 claims description 15
- 229910044991 metal oxide Inorganic materials 0.000 claims description 11
- 150000004706 metal oxides Chemical class 0.000 claims description 11
- 238000002485 combustion reaction Methods 0.000 claims description 9
- 239000002243 precursor Substances 0.000 claims description 9
- 229910000861 Mg alloy Inorganic materials 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- 229910052814 silicon oxide Inorganic materials 0.000 claims description 4
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 3
- 239000010408 film Substances 0.000 description 34
- 239000011701 zinc Substances 0.000 description 22
- 239000000463 material Substances 0.000 description 11
- 238000012360 testing method Methods 0.000 description 9
- 229910052725 zinc Inorganic materials 0.000 description 8
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 230000007797 corrosion Effects 0.000 description 5
- 238000005260 corrosion Methods 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000004566 building material Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 230000005674 electromagnetic induction Effects 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 238000007747 plating Methods 0.000 description 3
- 239000000758 substrate Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000010960 cold rolled steel Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000009713 electroplating Methods 0.000 description 2
- 238000010828 elution Methods 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 239000001294 propane Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229910000077 silane Inorganic materials 0.000 description 2
- 238000001771 vacuum deposition Methods 0.000 description 2
- 230000008016 vaporization Effects 0.000 description 2
- 229910000640 Fe alloy Inorganic materials 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000005275 alloying Methods 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- UQEAIHBTYFGYIE-UHFFFAOYSA-N hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 238000009830 intercalation Methods 0.000 description 1
- 230000002687 intercalation Effects 0.000 description 1
- 230000005596 ionic collisions Effects 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 201000009240 nasopharyngitis Diseases 0.000 description 1
- 150000001282 organosilanes Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 238000005019 vapor deposition process Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
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- B32B15/01—Layered products comprising a layer of metal all layers being exclusively metallic
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- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/30—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer
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- C—CHEMISTRY; METALLURGY
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- C23C30/00—Coating with metallic material characterised only by the composition of the metallic material, i.e. not characterised by the coating process
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- C—CHEMISTRY; METALLURGY
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Description
Claims (5)
- 素地鋼板上にZn‐Mgコーティング層を形成する段階と、
燃焼化学気相蒸着(CCVD)処理を施して厚さ11〜40nmの酸化皮膜を形成する段階
とを含み、
前記CCVD処理時、素地鋼板の温度は330〜450℃である、Zn‐Mg合金コーティング鋼板の製造方法。 - 前記Zn‐Mgコーティング層を形成する段階は、PVD法で行われる、請求項1に記載のZn‐Mg合金コーティング鋼板の製造方法。
- 前記CCVD処理時、空気供給量に対する前駆体蒸気の投入比は前駆体流量:空気供給量=0.8:210〜2.1:210L/分である、請求項1又は2に記載のZn‐Mg合金コーティング鋼板の製造方法。
- 前記Zn‐Mg合金コーティング鋼板は、
素地鋼板と、
前記素地鋼板上に形成されたZn‐Fe金属間化合物層と、
前記Zn‐Fe金属間化合物層上に形成され、Znの含量が95重量%以上のZn‐Mg金属間化合物を含む第1のZn‐Mgコーティング層と、
前記第1のZn‐Mgコーティング層上に形成され、Znの含量が80〜95重量%のZn‐Mg金属間化合物を含む第2のZn‐Mgコーティング層と、
前記第2のZn‐Mgコーティング層上に形成され、金属酸化物を含む酸化皮膜
とを含む、請求項1〜3のいずれか1項に記載のZn‐Mg合金コーティング鋼板の製造方法。 - 前記酸化皮膜は、金属酸化物を含み、前記金属酸化物は、シリコン酸化物(SiO2)を含み、MgOを一部含む、請求項1〜4のいずれか1項に記載のZn‐Mg合金コーティング鋼板の製造方法。
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KR1020110143891A KR101359259B1 (ko) | 2011-12-27 | 2011-12-27 | 내흑변성 및 밀착력이 우수한 Zn-Mg 합금 코팅강판 및 그 제조방법 |
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EP3561147A4 (en) | 2016-12-26 | 2020-03-25 | Posco | STEEL PLATED WITH ZINC ALLOY WITH EXCELLENT WELDABILITY AND CORROSION RESISTANCE |
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