JP5511381B2 - 硬化性のシリル化されたポリウレタン組成物から誘導された接着剤樹脂成分を有する固体高分子基質 - Google Patents
硬化性のシリル化されたポリウレタン組成物から誘導された接着剤樹脂成分を有する固体高分子基質 Download PDFInfo
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- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
- Y10T428/31573—Next to addition polymer of ethylenically unsaturated monomer
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
- Y10T428/31573—Next to addition polymer of ethylenically unsaturated monomer
- Y10T428/31583—Nitrile monomer type [polyacrylonitrile, etc.]
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Description
a)化学量論的に過剰のポリエーテルポリオールとポリイソシアナートとの反応から誘導されるヒドロキシ末端ポリウレタンプレポリマー;
b)イソシアナトシラン;および、任意選択で、
c)充填剤、紫外線安定剤、酸化防止剤、触媒、接着促進剤、硬化促進剤、チクソトロープ剤、可塑剤、水分捕捉剤、顔料、染料、界面活性剤、消泡剤、溶媒、および殺虫剤からなる群から選択される少なくとも一つの付加的な成分
を含有する硬化性樹脂生成組成物の硬化から得られる樹脂を、表面の少なくとも一部分に接着させた固体高分子基質。
OCN−R1−Si(R2)m(OR3)3−m
式中、R1は2価の炭化水素基であり、R2は1〜4の炭素原子を持つアルキルであり、R3は1〜4の炭素原子を持つアルキルであり、そしてmは0から2までの整数である。R1基は、末端イソシアナート基とアルコキシシラン基との間の安定した架橋を形成する種々の任意の構造を有してよい。本発明の一つの実施態様において、R1は、約1〜約12の炭素原子を持つアリーレン、または直鎖、環状もしくは分岐の炭化水素である。別の実施態様において、R1基は、1〜6の炭素原子を持つ低級アルキレン基であり、そして別の実施態様において少なくとも3の炭素原子を持つ低級アルキレン基である。
STPU重合体の調製:実施例1および比較例2、3のSTPU重合体の調製用の物質を表3に示す。
実施例4および比較例5、6の一液型STPU系シーラント製剤を表5に表す。
Claims (12)
- 固体高分子基質であって、:
a)二つのヒドロキシ基を持ち、8,000から16,000までの数平均分子量を有し、かつジオールの1グラム当たり0.2ミリ当量未満である末端エチレン性不飽和を有するポリオキシプロピレンポリエーテルポリオールの化学量論的に過剰量と脂環式ジイソシアナートとの反応〔ここでイソシアナートに対するヒドロキシの当量比は1.05から3.3である〕から誘導されるヒドロキシ末端ポリウレタンプレポリマー;
b)ガンマ−イソシアナトプロピルトリメトキシシラン;
c)炭酸カルシウム充填剤、ならびに
d)N−2−アミノエチル−3−アミノプロピルトリメトキシシラン、N−2−アミノエチル−3−アミノプロピルトリエトキシシラン、1,3,5−トリス(トリメトキシシリルプロピル)イソシアヌラート、ガンマ−アミノプロピルトリエトキシシラン、ガンマ−アミノプロピルトリメトキシシラン、ビス−ガンマ−(トリメトキシシリルプロピル)アミン、N−フェニル−ガンマ−アミノプロピルトリメトキシシラン、トリアミノ官能性トリメトキシシラン、ガンマ−アミノプロピルメチルジエトキシシラン、ガンマ−アミノプロピルメチルジエトキシシラン、ガンマ−メタクリロキシプロピルトリメトキシシラン、ガンマ−メチルアミノプロピルトリメトキシシラン、ガンマ−グリシドキシプロピルエチルジメトキシシラン、ガンマ−グリシドキシプロピルトリメトキシシラン、ガンマ−グリシドキシエチルトリメトキシシラン、ベータ−(3,4−エポキシシクロヘキシル)プロピルトリメトキシシラン、ベータ−(3,4−エポキシシクロヘキシル)エチルトリメトキシシラン、ベータ−(3,4−エポキシシクロヘキシル)エチルトリエトキシシラン、ベータ−(3,4−エポキシシクロヘキシル)エチルメチルジメトキシシラン、ガンマ−イソシアナトプロピルトリエトキシシラン、アルファ−イソシアナトプロピルメチルジメトキシシラン、ベータ−シアノエチルトリメトキシシラン、ガンマ−アクリロキシプロピルトリメトキシシラン、ガンマ−メタクリロキシプロピルメチルジメトキシシラン、4−アミノ−3,3−ジメチルブチルトリメトキシシラン、およびN−エチル−3−トリメトキシシリル−2−メチルプロパンアミン、ならびにそれらの混合物からなる群より選択される接着促進剤
を含有する硬化性樹脂生成組成物の硬化から得られる樹脂を、その表面の少なくとも一部分に接着させた固体高分子基質であって、ここで前記固体高分子基質が、ポリスチレン、ナイロン、およびアクリロニトリル−ブタジエン−スチレンからなる群から選択される少なくとも一つである固体高分子基質。 - 請求項1に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記脂環式ジイソシアナートがイソホロンジイソシアナートである、固体高分子基質。
- 請求項1〜2のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記イソシアナートに対するヒドロキシの当量比が1.2から2.0であり、そして前記ヒドロキシ末端ポリウレタンプレポリマーが少なくとも一つのヒドロキシ官能基を有する、固体高分子基質。
- 請求項1〜3のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記固体高分子基質がナイロンである、固体高分子基質。
- 請求項1〜3のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記固体高分子基質がアクリロニトリル−ブタジエン−スチレン樹脂である、固体高分子基質。
- 請求項1〜3のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記固体高分子基質がポリスチレンである、固体高分子基質。
- 請求項1〜6のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記接着促進剤が、N−2−アミノエチル−3−アミノプロピルトリメトキシシラン、ガンマ−アミノプロピルトリメトキシシラン、ビス−ガンマ−トリメトキシシリルプロピル)アミン、トリアミノ官能性トリメトキシシラン、4−アミノ−3,3−ジメチルブチルトリメトキシシラン、およびN−エチル−3−トリメトキシシリル−2−メチルプロパンアミンからなる群から選択される少なくとも一つである、固体高分子基質。
- 請求項1〜7のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記炭酸カルシウム充填剤が0.07マイクロメートルから4マイクロメートルまでの粒径を有する処理された炭酸カルシウムである、固体高分子基質。
- 固体高分子基質であって、前記樹脂がシーラントとして供される、請求項1〜8のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質。
- 請求項1〜8のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記樹脂がコーティングとして供される、固体高分子基質。
- 請求項1〜8のいずれか一項に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記樹脂が接着剤として供される、固体高分子基質。
- 請求項8に記載の硬化性樹脂生成組成物の硬化から得られる樹脂をその表面の少なくとも一部分に接着させた固体高分子基質であって、前記処理された炭酸カルシウム充填剤が前記樹脂生成組成物の100部当たり80から150部までの量で存在する、固体高分子基質。
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US11/515,442 US8153261B2 (en) | 2006-09-01 | 2006-09-01 | Solid polymeric substrate having adherent resin component derived from curable silylated polyurethane composition |
US11/515,442 | 2006-09-01 | ||
PCT/US2007/019119 WO2008027499A2 (en) | 2006-09-01 | 2007-08-30 | Solid polymeric substrate having adherent resin component derived from curable silylated polyurethane composition |
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JP2010502477A JP2010502477A (ja) | 2010-01-28 |
JP5511381B2 true JP5511381B2 (ja) | 2014-06-04 |
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US (1) | US8153261B2 (ja) |
EP (1) | EP2064257B1 (ja) |
JP (1) | JP5511381B2 (ja) |
CN (1) | CN101535360B (ja) |
BR (1) | BRPI0716151A2 (ja) |
CA (1) | CA2661812C (ja) |
TW (1) | TWI437016B (ja) |
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GB0721958D0 (en) | 2007-11-08 | 2007-12-19 | Tremco Illbruck Internat Gmbh | Insulating glass sealant |
DE102007058483A1 (de) | 2007-12-04 | 2009-06-10 | Henkel Ag & Co. Kgaa | Härtbare Zusammensetzungen enthaltend silylierte Polyurethane |
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JPWO2010013653A1 (ja) * | 2008-07-28 | 2012-01-12 | 旭硝子株式会社 | 粘着体、粘着シートおよびその用途 |
CN102119182B (zh) * | 2008-08-08 | 2013-02-06 | 建筑研究和技术有限公司 | 甲硅烷基化聚氨酯和/或聚脲的制备 |
DE102008038488A1 (de) * | 2008-08-20 | 2010-02-25 | Henkel Ag & Co. Kgaa | Feuchtigkeitshärtende wasserfeste Beschichtung |
DE102008047362A1 (de) | 2008-09-15 | 2010-04-15 | Henkel Ag & Co. Kgaa | Zusammensetzung zur Hautaufhellung |
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DE102009026679A1 (de) * | 2009-06-03 | 2010-12-16 | Henkel Ag & Co. Kgaa | Kleb- und Dichtstoffe auf Basis silanterminierter Bindemittel zum Verkleben und Abdichten von flexiblen Solarfolien / Photovoltaikmodulen |
DE102010000881A1 (de) * | 2010-01-14 | 2011-07-21 | Henkel AG & Co. KGaA, 40589 | 1K- Kaschierklebstoff mit Silanvernetzung |
EP2588511B1 (en) | 2010-06-30 | 2020-03-18 | Dow Global Technologies LLC | Low viscosity silyl-modified polymers |
US9290607B2 (en) | 2010-12-20 | 2016-03-22 | Dow Global Technologies Llc | Curable compositions containing isocyanate functional components having improved durability |
FR2969621B1 (fr) * | 2010-12-22 | 2013-01-18 | Bostik Sa | Polyurethane a blocs polyether et polyester et groupe terminal alkoxysilane |
EP2484706A1 (de) * | 2011-02-03 | 2012-08-08 | Sika Technology AG | Haftvermittlerzusammensetzung |
US10308847B1 (en) | 2011-02-03 | 2019-06-04 | Carroll Benford Dickens | Pressure sensitive, waterproof adhesive compositions |
US9822288B2 (en) | 2011-02-03 | 2017-11-21 | Carroll Benford Dickens | Waterproof silane-end capped adhesive compositions |
US10161140B1 (en) | 2011-02-03 | 2018-12-25 | Carroll Benford Dickens | Polymeric primer compositions and methods of use in flooring applications to displace gases |
US9068103B2 (en) * | 2011-02-03 | 2015-06-30 | Carroll Benford Dickens | Waterproof silane-endcapped adhesive mixture |
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US8153261B2 (en) | 2012-04-10 |
JP2010502477A (ja) | 2010-01-28 |
US20080057316A1 (en) | 2008-03-06 |
BRPI0716151A2 (pt) | 2013-09-17 |
CN101535360B (zh) | 2012-05-09 |
TWI437016B (zh) | 2014-05-11 |
CN101535360A (zh) | 2009-09-16 |
TW200833726A (en) | 2008-08-16 |
CA2661812A1 (en) | 2008-03-06 |
WO2008027499A2 (en) | 2008-03-06 |
WO2008027499A3 (en) | 2008-04-17 |
EP2064257A2 (en) | 2009-06-03 |
CA2661812C (en) | 2014-12-30 |
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